Control of viscosity in starch and polysaccharide solutions with ultrasound after gelatinization
Abstract
Application of power ultrasound has immense potential for a wide variety of processes in the food industry which include sterilization, emulsification, extraction, crystallization, degassing, filtration, drying, and more. Controlling the viscosity of starch (polysaccharide) solutions is one of the most promising processes to be developed. Power ultrasound can effectively decrease the viscosity of starch solutions after gelatinization. At the high starch concentrations (20-30%), starch gel can be liquidized by sonication. The viscosity of the starch solution of moderate concentration (5-10%) can be reduced about two orders of magnitude to 100 mPa·s by the ultrasonic irradiation for 30 min. The treated solution can be efficiently powdered by a spray-dryer after the sonication. The effectiveness of the ultrasonic process has been evaluated by measuring the changes in viscosity. Granule disintegration was determined using a method which measures the swelling power of starch. Change in molecular weight of the starch was monitored by gel permeation chromatography and a static light scattering method. The depolymerization process of the starch has been also monitored by NMR spectroscopy. The elucidated merits of the ultrasonic process are: 1) the process does not require any chemicals and additives; 2) the process can be simple and rapid, which means that the process is cost effective; and 3) the process will not induce large changes in the chemical structure and in particular, the properties of starches. The ultrasonic process has been confirmed to be applicable for many kinds of starches (corn, potato, tapioca, and sweet potato) and polysaccharides. Industrial relevance: Starches and a variety of polysaccharides are used in a multitude of applications throughout the food industry. Ultrasonically assisted modification of their chemical and physical characters is an important process and has commercial potential. In this paper, the changes in their viscosity, molecular weight, and the NMR spectra have been measured to evaluate the effectiveness of the ultrasonic process for the depolymerization and the viscosity control of the starch and polysaccharide solutions after gelatinization.
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The average molecular weight of starch reduced from 3000 KDa to 500 KDa after ultrasonic treatment.
“the average molecular weight of starch exhibited a reduction from 3000KDa to 500KDa subsequent to undergoing ultrasonic treatment [41].”
From A comprehensive review of ultrasonic assisted extraction (UAE) for bioactive components: Principles, advantages, equipment, and combined technologies (2023) · cites this paper as [41]
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Shen, L., Pang, S., Zhong, M., Sun, Y., Qayum, A., Liu, Y., Rashid, A., Xu, B., Liang, Q., Ma, H., et al. (2023) · Ultrasonics Sonochemistry · doi:10.1016/j.ultsonch.2023.106646 · Cited by 892 · see citing works
“In another investigation, a comparable outcome was observed, as the average molecular weight of starch exhibited a reduction from 3000KDa to 500KDa subsequent to undergoing ultrasonic treatment [41].”
ResultKang, Q., Chen, S., Li, S., Wang, B., Liu, X., Hao, L., & Lu, J. (2019) · International Journal of Biological Macromolecules · doi:10.1016/j.ijbiomac.2018.11.215 · Cited by 150 · see citing works
- Authors
- Iida, Y., Tuziuti, T., Yasui, K., Towata, A., & Kozuka, T.
- Affiliations
- National Institute of Advanced Industrial Science and Technology (JP)
- Corresponding author
- Iida, Yasuo
- Venue
- Innovative Food Science & Emerging Technologies
- Publisher
- Elsevier BV
- Published
- 2008-04
- Volume
- 9
- Issue
- 2
- Pages
- 140-146
- ISSN
- 1466-8564 (ISSN-L)
- OpenAlex
- W2006765772
- Cited by
- 284
- References
- 22
- Citations by year
- 2026: 8 · 2025: 10 · 2024: 13 · 2023: 17 · 2022: 14 · 2021: 20 · 2020: 22 · 2019: 25 · 2018: 19 · 2017: 22 · 2016: 13 · 2015: 26 · 2014: 17 · 2013: 16 · 2012: 9
- FWCI
- 5.54
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Innovative Food Science & Emerging Technologies (publishedVersion)
- Funders
- U.S. Food and Drug Administration
- Topics
- Health Sciences › Nursing › Nutrition and Dietetics › Food composition and properties
- Life Sciences › Agricultural and Biological Sciences › Food Science › Polysaccharides Composition and Applications
- Physical Sciences › Materials Science › Materials Chemistry › Ultrasound and Cavitation Phenomena
- Keywords
- power ultrasound, starch solutions, polysaccharide solutions, viscosity reduction, sonication, starch depolymerization, molecular weight reduction, granule disintegration, starch swelling power, starch modification, corn starch, potato starch, cassava starch, sweet potato starch
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