Combination of ionic liquid-based dispersive liquid–liquid micro-extraction with stopped-flow spectrofluorometry for the pre-concentration and determination of aluminum in natural waters, fruit juice and food samples

Abdolmohammad-Zadeh, H.; Sadeghi, G.H.

doi:10.1016/j.talanta.2010.01.012

Cited by 86Analytical chemistry methods developmentElectrochemical Analysis and ApplicationsAnalytical Chemistry and Chromatography

Combination of ionic liquid-based dispersive liquid–liquid micro-extraction with stopped-flow spectrofluorometry for the pre-concentration and determination of aluminum in natural waters, fruit juice and food samples

Abdolmohammad-Zadeh, H., Sadeghi, G.H.·2010·Talanta

DOI 10.1016/j.talanta.2010.01.012

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Abstract

In this research, we combined ionic liquid-based dispersive liquid-liquid micro-extraction (IL-based DLLME) with stopped-flow spectrofluorometry (SFS) to evaluate the concentration of aluminum in different real samples at trace level. 1-Hexylpyridinium hexafluorophosphate [Hpy][PF(6)] ionic liquid and 8-hydroxyquinoline (oxine), which forms a highly fluorescent complex with Al(3+), were chosen as the extraction solvent and chelating agent, respectively. The hydrophobic Al-oxine complex was extracted into the [Hpy][PF(6)] and separated from the aqueous phase. Then, the concentration of the enriched aluminum in the sediment phase was determined by SFS. Some effective parameters that influence the SFS signals and the micro-extraction efficiency, such as the suction and sending time, the concentration of the chelating agent, pH, the amount of the ionic liquid, the type of disperser solvent and diluting agent, ionic strength, extraction time, equilibration temperature and centrifugation time were investigated and optimized. In the optimum experimental conditions, the limit of detection (3s) and enrichment factor were 0.05microgL(-1) and 100, respectively. The relative standard deviation (RSD) for six replicate determinations of 6microgL(-1) Al was 1.7%. The calibration graph using the pre-concentration system was linear in the range of 0.06-15microgL(-1) with a correlation coefficient of 0.9989. The developed method was validated by the analysis of certified reference materials and applied successfully to the determination of aluminum in several water, fruit juice and food samples.

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DLLME is an attractive tool for the miniaturized sample pretreatment of a wide range of sample matrices.
“Dispersive liquid–liquid microextraction (DLLME) is an attractive tool for the miniaturized sample pretreatment of a wide range of sample matrices (water samples,2 biological fluids,3 foods,4etc) introduced in 2006 by Rezaee et al.5”
From Deep eutectic solvents as a new kind of dispersive solvent for dispersive liquid–liquid microextraction (2018) · cites this paper as [4]

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Authors: Abdolmohammad-Zadeh, H., & Sadeghi, G. H.
Affiliations: Azarbaijan Shahid Madani University (IR)
Venue: Talanta
Publisher: Elsevier BV
Published: 2010-05
Volume: 81
Issue: 3
Pages: 778-785
ISSN: 0039-9140 (ISSN-L)
DOI: 10.1016/j.talanta.2010.01.012
OpenAlex: W2025031598
Cited by: 86
References: 38
Citations by year: 2024: 2 · 2023: 3 · 2022: 5 · 2021: 2 · 2020: 1 · 2019: 4 · 2018: 3 · 2017: 6 · 2016: 6 · 2015: 5 · 2014: 8 · 2013: 9 · 2012: 16
FWCI: 13.02
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
www.elsevier.com/legal/tdmrep-license (tdm)
Locations: Talanta (publishedVersion)
PubMed (publishedVersion)
Funders: Azarbaijan Shahid Madani University
Topics: Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Physical Sciences › Chemistry › Electrochemistry › Electrochemical Analysis and Applications
Physical Sciences › Chemistry › Spectroscopy › Analytical Chemistry and Chromatography
Keywords: aluminum determination, 8-hydroxyquinoline, natural waters, fruit juice, food samples, extraction optimization
MeSH terms: Aluminum, Beverages, Chelating Agents, Chemistry Techniques, Analytical, Food Analysis, Fruit, Hydrogen-Ion Concentration, Ions, Solvents, Spectrometry, Fluorescence, Temperature, Time Factors, Triticum, Reproducibility of Results, Solid Phase Microextraction

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Combination of ionic liquid-based dispersive liquid–liquid micro-extraction with stopped-flow spectrofluorometry for the pre-concentration and determination of aluminum in natural waters, fruit juice and food samples

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