Cited by 147Pesticide Residue Analysis and SafetyAnalytical chemistry methods developmentAnalytical Chemistry and Chromatography

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Determination of pesticide residues in coconut water by liquid–liquid extraction and gas chromatography with electron-capture plus thermionic specific detection and solid-phase extraction and high-performance liquid chromatography with ultraviolet detection

Brito, N.M., Navickiene, S., Polese, L., Jardim, E.F.G., Abakerli, R.B., Ribeiro, M.L.·2002·Journal of Chromatography A

DOI 10.1016/s0021-9673(02)00351-5

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Abstract

Two simple methods were developed to determine 11 pesticides in coconut water, a natural isotonic drink rich in salts, sugars and vitamins consumed by the people and athletes. The first procedure involves solid-phase extraction using Sep-Pak Vac C18 disposable cartridges with methanol for elution. Isocratic analysis was carried out by means of high-performance liquid chromatography with ultraviolet detection at 254 nm to analyse captan, chlorothalonil, carbendazim, lufenuron and diafenthiuron. The other procedure is based on liquid-liquid extraction with hexane-dichloromethane (1:1, v/v), followed by gas chromatographic analysis with effluent splitting to electron-capture detection for determination of endosulfan, captan, tetradifon and trichlorfon and thermionic specific detection for determination of malathion, parathion-methyl and monocrotophos. The methods were validated with fortified samples at different concentration levels (0.01-12.0 mg/kg). Average recoveries ranged from 75 to 104% with relative standard deviations between 1.4 and 11.5%. Each recovery analysis was repeated at least five times. Limits of detection ranged from 0.002 to 2.0 mg/kg. The analytical procedures were applied to 15 samples and no detectable amounts of the pesticides were found in any samples under the conditions described.

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Authors: Brito, N. M., Navickiene, S., Polese, L., Jardim, E. F. G., Abakerli, R. B., & Ribeiro, M. L.
Affiliations: Universidade Estadual Paulista (Unesp) (BR)
Embrapa (BR)
Corresponding author: Ribeiro, M.L.
ORCID: Brito, N.M.
Navickiene, S.
Polese, L.
Ribeiro, M.L.
Venue: Journal of Chromatography A
Publisher: Elsevier BV
Published: 2002-05
Volume: 957
Issue: 2
Pages: 201-209
ISSN: 0021-9673 (ISSN-L)
DOI: 10.1016/s0021-9673(02)00351-5
OpenAlex: W1974982552
Cited by: 147
References: 12
Citations by year: 2026: 1 · 2025: 1 · 2024: 1 · 2023: 7 · 2022: 9 · 2021: 9 · 2020: 8 · 2019: 5 · 2018: 6 · 2017: 9 · 2016: 10 · 2015: 4 · 2014: 6 · 2013: 6 · 2012: 7
FWCI: 5.68
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Journal of Chromatography A (publishedVersion)
PubMed (publishedVersion)
Acervo Digital da Universidade Estadual Paulista (Universidade Estadual Paulista) (submittedVersion)
UNESP Institutional Repository (São Paulo State University) (submittedVersion)
Topics: Life Sciences › Agricultural and Biological Sciences › Food Science › Pesticide Residue Analysis and Safety
Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Physical Sciences › Chemistry › Analytical Chemistry › Analytical Chemistry and Chromatography
Keywords: pesticide residues, coconut water, solid-phase extraction, liquid-liquid extraction, electron capture detection, HPLC-UV, gas chromatography, captan, chlorothalonil, carbendazim, lufenuron, diafenthiuron, endosulfan, tetradifon, trichlorfon, malathion, methyl parathion, monocrotophos, food safety
MeSH terms: Chromatography, Gas, Chromatography, High Pressure Liquid, Cocos, Pesticide Residues, Sensitivity and Specificity, Spectrophotometry, Ultraviolet, Reproducibility of Results

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Determination of pesticide residues in coconut water by liquid–liquid extraction and gas chromatography with electron-capture plus thermionic specific detection and solid-phase extraction and high-performance liquid chromatography with ultraviolet detection

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