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Structural Features of Nanotubes Synthesized from NaOH Treatment on TiO2 with Different Post-Treatments
Abstract
We demonstrated that nanotubes synthesized from a NaOH treatment on TiO 2 with subsequent acid washing could proceed with repeatable crystalline-structure transformation through a simple acid−base washing step. By providing the unit cell parameters, we identified a divalent salt titanate (Na 2 Ti 2 O 5 ·H 2 O) with a layered structure as the structure formed after the NaOH treatment. With the increase in acidity during the post-treatment acid washing, the layered titaniate transformed into a nanotube through Na + −H + substitution, and eventually transformed into anatase TiO 2 . Crystalline-structure analysis has shown the feasibility of this titanate−titania transformation occuring through a simple structural rearrangement. A complete scheme for the formation and transformation of nanotubes induced by the NaOH treatment and the post-treatment washing was proposed.
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Metadata
- Authors
- Tsai, C.-C., & Teng, H.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2005-12-10
- Volume
- 18
- Issue
- 2
- Pages
- 367-373
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2950258454
- Cited by
- 486
- References
- 30
- FWCI
- 20.07
- Type
- journal article
- Language
- en
- Open access
- closed
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