Effects of crystallization condition of poly (butylene succinate) component on the crystallization of poly (ethylene oxide) component in their miscible blends
Abstract
The crystallization behavior of the poly(ethylene oxide) (PEO) component in poly(butylene succinate) (PBS)/PEO blends with the middle PEO content was investigated as a function of isothermal crystallization temperature of the PBS component ( T IC,PBS ) using differential scanning calorimetry (DSC). It is found that the crystallization behavior of the PEO component in these blends is significantly affected by T IC,PBS . Small-angle X-ray diffraction (SAXS) measurements were performed to explore the origin of the T IC,PBS dependence of crystallization of PEO component. On the basis of the SAXS measurements and the results of our previous work [ Macromolecules 2004, 37, 3337−3345], it is suggested that T IC,PBS controls the location distribution of the PEO component in the blends after the crystallization of the PBS component and thus significantly affects the crystallization behavior of PEO.
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In PBS/PEO blends, three fractionated exothermic peaks appear for the blend with weight composition 70/30.
“Three fractionated exothermic peaks appear for the blend with the weight composition of 70/30.”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [69]
With further decreasing PEO content in PBS/PEO blends, the degree of confinement is stronger and a single crystallization peak at very low temperature is observed for PEO.
“With further decreasing the content of PEO the degree of confinement is stronger and a single crystallization peak at very low temperature is observed for this polymer.”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [69]
In PBS/PEO blends, when PBS crystallizes first, the amorphous PEO chains are isolated within PBS interfibrillar/interlamellar regions.
“In this case, when PBS crystallizes first, the amorphous PEO chains are isolated within PBS interfibrillar/interlamellar regions.”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [69]
In PBS/PEO blends, up to a 60/40 composition, only a high-temperature exotherm is observed for PEO crystallization.
“Up to a 60/40 composition, only a high-temperature exotherm is observed for PEO crystallization.”
From Fractionated crystallization in semicrystalline polymers (2021) · cites this paper as [69]
Lateral contraction of the PLLA unit cell and local melting by rearrangement of the lamellar structure was reported for L60C40, L44C56, and L32C68.
“In fact, lateral contraction of the PLLA unit cell and local melting by rearrangement of the lamellar structure was reported for L60C40 21 , L44C56 25 , and L32C68 22 .”
From Crystallization Kinetics and Morphology of Biodegradable Double Crystalline PLLA- <i>b</i> -PCL Diblock Copolymers (2010) · cites this paper as [21]
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Miscibility, crystallization and properties of polyamide 6/MXD6 blendsPreprint
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- Authors
- He, Y., Zhu, B., Kai, W., & Inoue, Y.
- Affiliations
- Tokyo Institute of Technology (JP)
- Corresponding author
- Inoue, Yoshio
- Venue
- Macromolecules
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-09-23
- Volume
- 37
- Issue
- 21
- Pages
- 8050-8056
- ISSN
- 0024-9297 (ISSN-L)
- 1520-5835
- OpenAlex
- W2006709605
- Cited by
- 67
- References
- 38
- Citations by year
- 2025: 2 · 2023: 2 · 2022: 4 · 2021: 4 · 2020: 2 · 2019: 2 · 2018: 4 · 2017: 4 · 2016: 4 · 2015: 1 · 2014: 5 · 2013: 3 · 2012: 8
- FWCI
- 2.31
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Macromolecules (publishedVersion)
- Tokyo Tech Research Repository (Tokyo Institute of Technology) (submittedVersion)
- Topics
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer crystallization and properties
- Physical Sciences › Materials Science › Biomaterials › biodegradable polymer synthesis and properties
- Physical Sciences › Materials Science › Materials Chemistry › Block Copolymer Self-Assembly
- Keywords
- poly(butylene succinate), poly(ethylene oxide), polymer blends, miscible polymer blends, crystallization behavior, blend morphology
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