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Facile, scalable synthesis of edge-halogenated graphene nanoplatelets as efficient metal-free eletrocatalysts for oxygen reduction reaction
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A series of edge-selectively halogenated (X = Cl, Br, I) graphene nanoplatelets (XGnPs = ClGnP, BrGnP, IGnP) were prepared simply by ball-milling graphite in the presence of Cl2, Br2 and I2, respectively. High BET surface areas of 471, 579 and 662 m(2)/g were observed for ClGnP, BrGnP and IGnP, respectively, indicating a significant extent of delamination during the ball-milling and subsequent workup processes. The newly-developed XGnPs can be well dispersed in various solvents, and hence are solution processable. Furthermore, XGnPs showed remarkable electrocatalytic activities toward oxygen reduction reaction (ORR) with a high selectivity, good tolerance to methanol crossover/CO poisoning effects, and excellent long-term cycle stability. First-principle density-functional calculations revealed that halogenated graphene edges could provide decent adsorption sites for oxygen molecules, in a good agreement with the experimental observations.
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Metadata
- Authors
- Jeon, I.-Y., Choi, H.-J., Choi, M., Seo, J.-M., Jung, S.-M., Kim, M.-J., Zhang, S., Zhang, L., Xia, Z., Dai, L., Park, N., & Baek, J.-B.
- Venue
- Scientific Reports
- Published
- 2013-06-05
- Volume
- 3
- Issue
- 1
- Pages
- 1810-1810
- ISSN
- 2045-2322 (ISSN-L)
- OpenAlex
- W2150556972
- Cited by
- 353
- References
- 46
- FWCI
- 15.39
- Type
- journal article
- Language
- en
- Open access
- gold
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