A microextraction method based on precipitation for the simultaneous separation and preconcentration of cadmium and lead before their determination by FAAS: experimental design methodology
Abstract
A simple and rapid separation and preconcentration method based on precipitation combined with flame atomic absorption spectrometry for the determination of trace amounts of cadmium and lead ions has been introduced. Under the optimum conditions, the method exhibited linear dynamic ranges of 5–400 µg/L for cadmium and 8–500 µg/L for lead. The detection limits were 0.96 and 1.71 µg/L and the enhancement factors were 115 and 110 for cadmium and lead, respectively. The results revealed that the presented method is a good technique for the determination of target metal ions in natural water samples.
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The sample volume is an important factor for obtaining a high preconcentration factor.
“The sample volume is an important factor for obtaining a high preconcentration factor [51,52,53,54,55,56,57,58].”
From Deep Eutectic Solvent-Based Microextraction of Lead(II) Traces from Water and Aqueous Extracts before FAAS Measurements (2020) · cites this paper as [52]
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- Authors
- Koosha, E., Shamsipur, M., Salimi, F., & Ramezani, M.
- Affiliations
- Islamic Azad University, Arak (IR)
- Razi University (IR)
- Corresponding author
- Ramezani, Majid
- Venue
- Separation Science and Technology
- Publisher
- Informa UK Limited
- Published
- 2020-07-08
- Volume
- 56
- Issue
- 10
- Pages
- 1721-1729
- ISSN
- 0149-6395 (ISSN-L)
- 1520-5754
- OpenAlex
- W3041966478
- Cited by
- 26
- References
- 34
- Citations by year
- 2026: 1 · 2025: 1 · 2024: 4 · 2023: 6 · 2022: 8 · 2021: 4 · 2020: 2
- FWCI
- 2.59
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Separation Science and Technology (publishedVersion)
- Topics
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Physical Sciences › Environmental Science › Water Science and Technology › Environmental and Analytical Chemistry Studies
- Physical Sciences › Chemistry › Electrochemistry › Electrochemical Analysis and Applications
- Keywords
- cadmium, lead, preconcentration, simultaneous separation, trace metal analysis, natural water samples, flame atomic absorption spectrometry, experimental design optimization
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