Cited by 178Analytical chemistry methods developmentAnalytical Chemistry and ChromatographyPesticide Residue Analysis and Safety

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Solid-phase extraction combined with dispersive liquid–liquid microextraction-ultra preconcentration of chlorophenols in aqueous samples

Fattahi, Nazir, Samadi, Soheila, Assadi, Yaghoub, Hosseini, Mohammad Reza Milani·2007·Journal of Chromatography A

DOI 10.1016/j.chroma.2007.09.002

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Abstract

The solid-phase extraction (SPE) joined with the dispersive liquid-liquid microextraction (DLLME) has been developed as an ultra preconcentration technique for the determination of chlorophenols in water samples. Chlorophenols (CPs) were employed as model compounds to assess the extraction procedure and were determined by gas chromatography-electron-capture detection (GC-ECD). In solid-phase extraction-dispersive liquid-liquid microextraction (SPE-DLLME), CPs were adsorbed from a large volume of aqueous samples (100 mL) into 100 mg functionalized styrene-divinylbenzene polymer (PPL) sorbent. After the elution of the desired compounds from the sorbent by using acetone, DLLME technique was performed on the obtained solution. Some important extraction parameters, such as sample solution flow rate, breakthrough volume, sample pH, type and volume of the elution solvent as well as the salt addition, were studied and optimized. The new method (SPE-DLLME) provided an ultra enrichment factor (4390-17,870) for 19 CPs. The calibration graphs were linear in the range of 0.001-20 microg L(-1) and the limits of detection (LODs) ranged from 0.0005 to 0.1 microg L(-1). The relative standard deviations (RSDs, for 10.0 microg L(-1) of MCPs, 5.00 microg L(-1) of DCPs, 0.200 microg L(-1) of TCPs, 0.100 microg L(-1) of TeCPs and PCP) with and without the internal standard varied from 1.1 to 6.4% (n=7) and 2.5-9.7% (n=7), respectively. The relative recoveries of the well, tap and river water sampl…

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Authors: Fattahi, N., Samadi, S., Assadi, Y., & Hosseini, M. R. M.
Affiliations: Iran University of Science and Technology (IR)
Corresponding author: Assadi, Yaghoub
ORCID: Fattahi, Nazir
Samadi, Soheila
Hosseini, Mohammad Reza Milani
Venue: Journal of Chromatography A
Publisher: Elsevier BV
Published: 2007-10
Volume: 1169
Issue: 1-2
Pages: 63-69
ISSN: 0021-9673 (ISSN-L)
DOI: 10.1016/j.chroma.2007.09.002
OpenAlex: W2087588327
Cited by: 178
References: 48
Citations by year: 2026: 1 · 2025: 2 · 2024: 1 · 2023: 2 · 2022: 3 · 2021: 1 · 2020: 6 · 2019: 6 · 2018: 9 · 2017: 8 · 2016: 10 · 2015: 8 · 2014: 24 · 2013: 14 · 2012: 13
FWCI: 17.35
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Journal of Chromatography A (publishedVersion)
PubMed (publishedVersion)
Funders: Iran University of Science and Technology
Topics: Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Physical Sciences › Chemistry › Analytical Chemistry › Analytical Chemistry and Chromatography
Life Sciences › Agricultural and Biological Sciences › Food Science › Pesticide Residue Analysis and Safety
Keywords: chlorophenols, solid-phase extraction, dispersive liquid-liquid microextraction, water analysis, extraction optimization, electron capture detection
MeSH terms: Adsorption, Chlorophenols, Chromatography, Gas, Chemical Fractionation, Polystyrenes, Reference Standards, Sensitivity and Specificity, Specimen Handling, Spectrophotometry, Atomic, Water Pollutants, Chemical, Water Supply, Reproducibility of Results, Rivers, Solid Phase Extraction

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Solid-phase extraction combined with dispersive liquid–liquid microextraction-ultra preconcentration of chlorophenols in aqueous samples

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