An effervescence tablet-assisted microextraction based on the solidification of deep eutectic solvents for the determination of strobilurin fungicides in water, juice, wine, and vinegar samples by HPLC

Jia, Liyan; Huang, Xin; Zhao, Wenfei; Wang, Huihui; Jing, Xu

doi:10.1016/j.foodchem.2020.126424

Cited by 96Analytical chemistry methods developmentPesticide Residue Analysis and SafetyIonic liquids properties and applications

An effervescence tablet-assisted microextraction based on the solidification of deep eutectic solvents for the determination of strobilurin fungicides in water, juice, wine, and vinegar samples by HPLC

Jia, Liyan, Huang, Xin, Zhao, Wenfei, Wang, Huihui, Jing, Xu·2020·Food Chemistry

DOI 10.1016/j.foodchem.2020.126424

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Abstract

In this study, a simple, efficient, and green effervescence tablet-assisted microextraction method based on the solidification of deep eutectic solvent (ETA-ME-SDES) was developed to determine picoxystrobin, pyraclostrobin, and trifloxystrobin in water, juice, wine, and vinegar samples by HPLC. An eco-friendly, hydrophobic, deep eutectic solvent (DES, acting as the extraction solvent) was synthesized by thymol and octanoic acid in the molar ratio of 1:5. The extraction solvent dispersed in sample solutions with the assistance of pH adjustment and effervescence reaction, and was collected after solidification in an ice bath. Several essential conditions, including the type and the volume of DESs, the amount of ammonia hydroxide, and the components of effervescence tablets were optimized. The limits of detection ranged from 0.15 to 0.38 μg L-1. Extraction recovery ranged from 77.4 to 106.9%. The proposed method was successful in determining the amount of strobilurin fungicides in water, juice, wine, and vinegar samples.

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A DES consisting of thymol and octanoic acid was used for the preconcentration of strobilurin fungicides in water, juice, wine, and vinegar samples by HPLC [59], and high extraction recovery was observed (77-107%).
“A DES consisting of thymol and octanoic acid was used for the preconcentration of strobilurin fungicides in water, juice, wine, and vinegar samples by HPLC [59], and high extraction recovery was observed (77-107%).”
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Authors: Jia, L., Huang, X., Zhao, W., Wang, H., & Jing, X.
Affiliations: Shanxi Agricultural University (CN)
Corresponding author: Jing, Xu
ORCID: Huang, Xin
Zhao, Wenfei
Wang, Huihui
Jing, Xu
Venue: Food Chemistry
Publisher: Elsevier BV
Published: 2020-07
Volume: 317
Pages: 126424
ISSN: 0308-8146 (ISSN-L)
DOI: 10.1016/j.foodchem.2020.126424
OpenAlex: W3007086530
Cited by: 96
References: 37
Citations by year: 2026: 27 · 2025: 12 · 2024: 11 · 2023: 11 · 2022: 15 · 2021: 14 · 2020: 6
FWCI: 5.96
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
www.elsevier.com/legal/tdmrep-license (tdm)
Locations: Food Chemistry (publishedVersion)
PubMed (publishedVersion)
Funders: ShanXi Science and Technology Department
Shanxi Agricultural University
Topics: Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Life Sciences › Agricultural and Biological Sciences › Food Science › Pesticide Residue Analysis and Safety
Physical Sciences › Chemical Engineering › Catalysis › Ionic liquids properties and applications
Keywords: deep eutectic solvents, strobilurin fungicides, picoxystrobin, pyraclostrobin, trifloxystrobin, food and beverage analysis, wine, vinegar, juice, water
MeSH terms: Fruit and Vegetable Juices, Strobilurins, Acetates, Chromatography, High Pressure Liquid, Fungicides, Industrial, Hydrogen-Ion Concentration, Imines, Salts, Water Pollutants, Chemical, Wine, Acetic Acid, Limit of Detection, Liquid Phase Microextraction

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An effervescence tablet-assisted microextraction based on the solidification of deep eutectic solvents for the determination of strobilurin fungicides in water, juice, wine, and vinegar samples by HPLC

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