Synthesis and crystallization behavior of poly( l -lactide)- block -poly(ϵ-caprolactone) copolymer
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The understanding of the complicated properties of double crystalline diblock copolymer systems is still at a nascent stage.
“Although there have been a number of prior reports on double crystalline diblock copolymer systems, the understanding of their complicated properties is still at a nascent stage. [5-16]”
The decrease in PCL peak crystallization temperature with increasing PLLA content could be a result of topological constraints because PLLA crystallizes first and forms spherulites regardless of composition.
“This could be a result of topological constraints since PLLA crystallizes first when the samples are cooled from the melt and in a break-out fashion whereby spherulites are formed regardless of composition. [6,16,21]”
Kim et al. found a rheological T_ODT of 220°C for two PLLA-b-PCL copolymers.
“They found a rheological T ODT of 220 8 C for two copolymers: one containing 32 wt.-% PCL with a M n ¼ 77000 g mol 1 and another with 46% PCL and M n ¼ 46000 g mol 1 .”
The mechanical properties and biodegradability of PLLA-b-PCL copolymers are affected by the crystallinity of the constituent blocks, which depends on the microdomain structure.
“The mechanical properties as well as biodegradability are very much affected by the crystallinity of the constituent blocks that in turn depends upon the microdomain structure. [6,20]”
Double-crystalline PLLA-b-PCL diblock copolymers have been reported as miscible or weakly segregated in the melt, depending on composition and molecular weight.
“The double-crystalline PLLAb -PCLdiblock copolymers have been reported as miscible or weakly segregated in the melt, depending on composition and molecular weight. 23 -29”
From Crystallization Kinetics and Morphology of Biodegradable Double Crystalline PLLA- <i>b</i> -PCL Diblock Copolymers (2010) · cites this paper as [24]
A detailed study of the crystallization kinetics and morphology of both blocks, and their dependence with composition in a wide range, has not been reported.
“Although these systems have been previously evaluated 30 -35 and morphological studies have been previously performed by SAXS, 24,27,28 a detailed study of the crystallization kinetics and morphology of both blocks, and their dependence with composition in a wide range has not been reported, as far as we are aware.”
From Crystallization Kinetics and Morphology of Biodegradable Double Crystalline PLLA- <i>b</i> -PCL Diblock Copolymers (2010) · cites this paper as [24]
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- Authors
- Kim, J. K., Park, D.-J., Lee, M.-S., & Ihn, K. J.
- Affiliations
- Pohang University of Science and Technology (KR)
- Kangwon National University (KR)
- Corresponding author
- Kim, Jin Kon
- Venue
- Polymer
- Publisher
- Elsevier BV
- Published
- 2001-08
- Volume
- 42
- Issue
- 17
- Pages
- 7429-7441
- ISSN
- 0032-3861 (ISSN-L)
- OpenAlex
- W2078444325
- Cited by
- 147
- References
- 37
- Citations by year
- 2026: 1 · 2025: 2 · 2024: 1 · 2023: 1 · 2022: 1 · 2021: 9 · 2020: 2 · 2019: 7 · 2018: 3 · 2017: 10 · 2016: 8 · 2015: 8 · 2014: 7 · 2013: 4 · 2012: 13
- FWCI
- 6.41
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Polymer (publishedVersion)
- Open Access System for Information Sharing (Pohang University of Science and Technology) (submittedVersion)
- Topics
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer crystallization and properties
- Physical Sciences › Materials Science › Biomaterials › biodegradable polymer synthesis and properties
- Physical Sciences › Materials Science › Materials Chemistry › Block Copolymer Self-Assembly
- Keywords
- block copolymer crystallization, semicrystalline block copolymers, microphase separation, ring-opening polymerization, chain folding, molecular weight effects
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