Determination of Tetraethyllead and Inorganic Lead in Water by Solid Phase Microextraction/Gas Chromatography
Abstract
A new method for the determination of tetraethyllead (TEL) and ionic lead in water by SPME has been developed. TEL is extracted from the headspace over the sample. Inorganic lead is first derivatized with sodium tetraethylborate to form TEL, which is extracted in the same way as pure TEL samples. The analytical procedure was optimized with respect to pH, amount of derivatizing reagent added, stirring conditions, and extraction time. The detection limit obtained for TEL was found to be 100 ppt when using FID and 5 ppt when using ion trap MS (ITMS). The detection limit for Pb(2+), limited by the nonzero blank, was found to be 200 ppt. Linear calibration curves were obtained for both analytes when FID was used for detection. For lead they spanned over 4 orders of magnitude. ITMS offered excellent sensitivity and selectivity, but the calibration curves were nonlinear when the m/z = 295 ion was used for quantitation. The method has been verified on spiked tap water samples. An excellent agreement was found between the results obtained for standard solutions prepared using NANOpure water and spiked tap water samples.
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The sample volume is an important factor for obtaining a high preconcentration factor.
“The sample volume is an important factor for obtaining a high preconcentration factor [51,52,53,54,55,56,57,58].”
From Deep Eutectic Solvent-Based Microextraction of Lead(II) Traces from Water and Aqueous Extracts before FAAS Measurements (2020) · cites this paper as [58]
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de Castro, M. D. L., & García, J. L. L. (2002) · Techniques and instrumentation in analytical chemistry · doi:10.1016/s0167-9244(02)80006-3 · Cited by 1 · see citing works
Derivatization and vapor generation methods for trace element analysis and speciation
Cai, Y. Z. (2003) · Comprehensive analytical chemistry · doi:10.1016/s0166-526x(03)41019-2 · Cited by 1 · see citing works
Eisert, R., & Pawliszyn, J. B. (1999) · CRC Press eBooks · doi:10.1201/9781439832387.ch8 · Cited by 1 · see citing works
Self-citationGaschromatographische Techniken für die Speziationsanalytik
Rosenberg, E. (2001) · Nachrichten aus der Chemie · doi:10.1002/nadc.20010490215
- Authors
- Górecki, T., & Pawliszyn, J.
- Affiliations
- University of Waterloo (CA)
- Venue
- Analytical Chemistry
- Publisher
- American Chemical Society (ACS)
- Published
- 1996-09-01
- Volume
- 68
- Issue
- 17
- Pages
- 3008-3014
- ISSN
- 0003-2700 (ISSN-L)
- 1520-6882
- OpenAlex
- W1982095959
- Cited by
- 101
- References
- 23
- Citations by year
- 2023: 2 · 2021: 1 · 2020: 3 · 2016: 1 · 2015: 2 · 2014: 1 · 2013: 1 · 2012: 1
- FWCI
- 10.97
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Analytical Chemistry (publishedVersion)
- PubMed (publishedVersion)
- Topics
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Physical Sciences › Chemistry › Spectroscopy › Analytical Chemistry and Chromatography
- Physical Sciences › Environmental Science › Water Science and Technology › Environmental and Analytical Chemistry Studies
- Keywords
- tetraethyl lead, inorganic lead, solid-phase microextraction, headspace extraction, sodium tetraethylborate derivatization, tap water, ion trap mass spectrometry, flame ionization detection
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