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Sulfur Vacancy-Rich O-Doped 1T-MoS2 Nanosheets for Exceptional Photocatalytic Nitrogen Fixation over CdS

Sun, Benteng, Liang, Zhangqian, Qian, Yeye, Xu, Xuesong, Han, Ye, Tian, Jian·2020·ACS Applied Materials & Interfaces

DOI 10.1021/acsami.9b20767

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Abstract

Here, we reported that sulfur vacancy-rich O-doped 1T-MoS 2 nanosheets (denoted as SV-1T-MoS 2 ) can surpass the activity of Pt as cocatalysts to assist in the photocatalytic nitrogen fixation of CdS nanorods. SV-1T-MoS 2 cocatalysts exhibit sulfur vacancies, O-doping, more metallic 1T phase, and high electronic conductivity, thus leading to the exposure of more active edge sites, high Brunauer–Emmett–Teller surface area, enhanced visible light absorption, and improved electron separation and transfer, which are beneficial for photocatalytic nitrogen fixation. Consequently, the optimized 30 wt % SV-1T-MoS 2 -/CdS composites exhibit an outstanding nitrogen fixation rate of 8220.83 μmol L –1 h –1 g –1 and long-term stability under simulated solar light irradiation, significantly higher than pure CdS nanorods, CdS–Pt (0.1 wt %), and 30 wt % 1T-MoS 2 /CdS composites. The catalytic mechanism of photocatalytic nitrogen fixation on SV-1T-MoS 2 is discussed by density functional theory calculations.

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Authors: Sun, B., Liang, Z., Qian, Y., Xu, X., Han, Y., & Tian, J.
Venue: ACS Applied Materials & Interfaces
Publisher: American Chemical Society (ACS)
Published: 2020-01-17
Volume: 12
Issue: 6
Pages: 7257-7269
ISSN: 1944-8244 (ISSN-L)
1944-8252
DOI: 10.1021/acsami.9b20767
OpenAlex: W2999823694
Cited by: 284
References: 65
FWCI: 8.82
Type: journal article
Language: en
Open access: closed

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Sulfur Vacancy-Rich O-Doped 1T-MoS2 Nanosheets for Exceptional Photocatalytic Nitrogen Fixation over CdS

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