Investigation of Deep Eutectic Solvent-Based Microwave-Assisted Extraction and Efficient Recovery of Natural Products
Abstract
A systematic study of the principles of deep eutectic solvent-based microwave-assisted extraction (DES-MAE) was performed. It was found that the heating rates of most DESs decreased (heat capacity increased) under microwave irradiation with increasing water content, allowing high-efficiency extraction for thermally sensitive compounds. In addition, DESs containing carboxylic acids reacted with hydroxyl groups of sugar and choline chloride, resulting in cell wall destruction and inhibition of cellulose, hemicellulose, and lignin reconnection in cell walls through hydrogen bonds, thus leading to better extraction performance. This was verified by extracting anthraquinones from Rheum palmatum using DES-MAE and optimizing extraction conditions. DES with citric acid as the hydrogen bonding donor gave the highest extraction efficiency under the optimized conditions. In addition, anthraquinones in the DES extract were recovered using three kinds of silica modified by different functional groups. The results showed that material containing a phenyl group is beneficial to the recovery of anthraquinones in acid-based DESs because it can facilitate strong hydrophobic and π–π interactions. This study showcases the green chemistry applications of DES-MAE in a laboratory and industry alike, and demonstrates the recovery of natural products from DES extracts. The findings also provide valuable information for green extraction, modification, and application of cellulose, hemicellulose, and lignin.
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Due to their ionic and polar nature, DESs can efficiently absorb microwave radiation, resulting in rapid heat generation and enhanced release of analytes from the sample matrix.
“Due to their ionic and polar nature, deep eutectic solvents can efficiently absorb microwave radiation, resulting in rapid heat generation and enhanced release of analytes from the sample matrix [34,35].”
From Eco-Friendly Deep Eutectic Solvent-Based Extraction Technologies: A Comprehensive Review of Principles, Applications, and Comparative Insights (2026) · cites this paper as [34]
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- Authors
- Wang, J., Jing, W., Tian, H., Liu, M., Yan, H., Bi, W., & Chen, D. D. Y.
- Affiliations
- Nanjing Normal University (CN)
- University of British Columbia (CA)
- Hebei University (CN)
- Corresponding author
- Bi, Wentao
- Chen, David Da Yong
- Venue
- ACS Sustainable Chemistry & Engineering
- Publisher
- American Chemical Society (ACS)
- Published
- 2020-07-17
- Volume
- 8
- Issue
- 32
- Pages
- 12080-12088
- ISSN
- 2168-0485 (ISSN-L)
- OpenAlex
- W3043696864
- Cited by
- 97
- References
- 31
- Citations by year
- 2026: 16 · 2025: 22 · 2024: 22 · 2023: 11 · 2022: 14 · 2021: 11 · 2020: 1
- FWCI
- 1.89
- Type
- journal article
- Language
- en
- Open access
- closed
- Licence
- Locations
- ACS Sustainable Chemistry & Engineering (publishedVersion)
- Funders
- Natural Science Foundation of Hebei Province (B2018201270)
- Major Basic Research Project of the Natural Science Foundation of the Jiangsu Higher Education Institutions (16KJB150022)
- National Natural Science Foundation of China (21475061, 21507062)
- Priority Academic Program Development of Jiangsu Higher Education Institutions
- Scientific Research Foundation for the Returned Overseas Chinese Scholars ([2015]1098)
- Jiangsu Collaborative Innovation Centre of Biomedical Functional Materials, Nanjing Normal University
- Topics
- Physical Sciences › Chemical Engineering › Catalysis › Ionic liquids properties and applications
- Physical Sciences › Chemistry › Organic Chemistry › Microwave-Assisted Synthesis and Applications
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
- Keywords
- deep eutectic solvents, microwave-assisted extraction, anthraquinones, Rheum palmatum, silica adsorbent, phenyl-functionalized silica, natural product recovery, cell wall damage, cellulose, hemicellulose and lignin, citric acid, choline chloride, green extraction
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