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Cited by 244

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Ruthenium Nanoparticles: Size, Shape, and Self-Assemblies

Viau, G., Brayner, R., Poul, L., Chakroune, N., Lacaze, E., Fiévet-Vincent, F., Fiévet, F.·2003·Chemistry of Materials
DOI 10.1021/cm0212109
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Abstract

Ruthenium nanoparticles were prepared by reduction of RuCl 3 in a liquid polyol. The mean particle size was restricted to the 1−6 nm range by appropriate choice of the reduction temperature and the acetate ion concentration in the solution. Very narrow particle diameter distributions were obtained. In some samples, among nearly isotropic particles, platelets with aspect ratios as low as 1/4 were detected. Colloidal solutions in toluene were obtained by coating the metal particles with dodecane thiol. Self-assemblies of 4-nm-sized coated particles were studied on a transmission electron microscope grid. The dodecane thiol concentration in the colloidal solution was found to determine, within the particle monolayer, the formation of either columnar units made up of edgewise stacked platelets, or a hexagonal network with a mean distance between the particles of 2 nm. The stacking of hexagonal arrays of particles was also studied, and both closed-packed and noncompact stackings were found. In the noncompact stacking, moiré images resulted from the twisting of the two hexagonal layers with respect to each other. Reconstructions of moiré patterns were observed to favor the 6-fold and 2-fold sites.

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Cited by

Metadata

Authors
Viau, G., Brayner, R., Poul, L., Chakroune, N., Lacaze, E., Fiévet-Vincent, F., & Fiévet, F.
Venue
Chemistry of Materials
Publisher
American Chemical Society (ACS)
Published
2002-12-13
Volume
15
Issue
2
Pages
486-494
ISSN
  • 0897-4756 (ISSN-L)
  • 1520-5002
DOI
10.1021/cm0212109
OpenAlex
W2045996022
Cited by
244
References
1
FWCI
8.89
Type
journal article
Language
en
Open access
closed

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