The DOI matches its Crossref record; 31 of the 31 references it cites were found in a registry or an index.
Magnetite Nanocrystals: Nonaqueous Synthesis, Characterization, and Solubility
Abstract
A novel nonaqueous route has been applied for the preparation of nanocrystalline magnetite. In a simple one-pot reaction process, iron(III) acetylacetonate was dissolved in benzyl alcohol and treated in an autoclave between 175 and 200 °C. This approach leads to monocrystalline magnetite particles with sizes ranging from 12 to 25 nm, as evidenced by X-ray analysis, HRTEM, and Raman and Mössbauer spectroscopy. The isolated particles can be redispersed either in polar or nonpolar solvents by coating them just after synthesis with undecanoic acid or dopamine. Simple sedimentation after redispersion in hexane can be used to lower the polydispersity of the sample.
Overview
The claims and statistics of this paper haven’t been checked yet.
Run the check — free, no account needed. It reads the open-access text and checks the sources it cites.
Integrity signals
Registry
Cites
Statistics
Verification
Claims the paper makes
The claims and statistics of this paper haven’t been checked yet.
Run the check — free, no account needed. It reads the open-access text and checks the sources it cites.
Self-check
Percentages, sums and reported differences re-computed from the paper’s own numbers.
The self-check needs the paper’s full text.
Citations
Cites
Monodisperse MFe2O4 (M = Fe, Co, Mn) Nanoparticles
Sun, S., Zeng, H., Robinson, D. B., Raoux, S., Rice, P. M., Wang, S. X., & Li, G. (2004) · Journal of the American Chemical Society · doi:10.1021/ja0380852 · Cited by 3,441
Raman microspectroscopy of some iron oxides and oxyhydroxides
de Faria, D. L. A., Venâncio Silva, S., & de Oliveira, M. T. (1997) · Journal of Raman Spectroscopy · doi:10.1002/(sici)1097-4555(199711)28:11<873::aid-jrs177>3.0.co;2-b · Cited by 3,238
Size-Controlled Synthesis of Magnetite Nanoparticles
Sun, S., & Zeng, H. (2002) · Journal of the American Chemical Society · doi:10.1021/ja026501x · Cited by 2,829
Hyeon, T., Lee, S. S., Park, J., Chung, Y., & Na, H. B. (2001) · Journal of the American Chemical Society · doi:10.1021/ja016812s · Cited by 2,040
Bean, C. P., & Livingston, J. D. (1959) · Journal of Applied Physics · doi:10.1063/1.2185850 · Cited by 1,773
Magnetic Properties of Nanostructured Materials
Leslie-Pelecky, D. L., & Rieke, R. D. (1996) · Chemistry of Materials · doi:10.1021/cm960077f · Cited by 1,721
Functionalisation of magnetic nanoparticles for applications in biomedicine
Berry, C. C., & Curtis, A. S. G. (2003) · Journal of Physics D: Applied Physics · doi:10.1088/0022-3727/36/13/203 · Cited by 1,588
Synthesis and Characterization of Nanometer-Size Fe3O4 and γ-Fe2O3 Particles
Kang, Y. S., Risbud, S., Rabolt, J. F., & Stroeve, P. (1996) · Chemistry of Materials · doi:10.1021/cm960157j · Cited by 1,068
Raman spectroscopic study of magnetite (FeFe2O4): a new assignment for the vibrational spectrum
Shebanova, O. N., & Lazor, P. (2003) · Journal of Solid State Chemistry · doi:10.1016/s0022-4596(03)00294-9 · Cited by 905
Rockenberger, J., Scher, E. C., & Alivisatos, A. P. (1999) · Journal of the American Chemical Society · doi:10.1021/ja993280v · Cited by 736
Formation of uniform spherical magnetite particles by crystallization from ferrous hydroxide gels
Sugimoto, T., & Matijević, E. (1980) · Journal of Colloid and Interface Science · doi:10.1016/0021-9797(80)90187-3 · Cited by 643
Raman study of magnetite (Fe3O4): laser‐induced thermal effects and oxidation
Shebanova, O. N., & Lazor, P. (2003) · Journal of Raman Spectroscopy · doi:10.1002/jrs.1056 · Cited by 622
Commercial applications of ferrofluids
Raj, K., & Moskowitz, R. (1990) · Journal of Magnetism and Magnetic Materials · doi:10.1016/0304-8853(90)90058-x · Cited by 583
Polyol-Mediated Preparation of Nanoscale Oxide Particles
Feldmann, C., & Jungk, H.-O. (2001) · Angewandte Chemie International Edition · doi:10.1002/1521-3773(20010119)40:2<359::aid-anie359>3.0.co;2-b · Cited by 435
Niederberger, M., Bartl, M. H., & Stucky, G. D. (2002) · Chemistry of Materials · doi:10.1021/cm021203k · Cited by 419
Self-citationOrdered Two-Dimensional Arrays of Ferrite Nanoparticles
Fried, T., Shemer, G., & Markovich, G. (2001) · Advanced Materials · doi:10.1002/1521-4095(200108)13:15<1158::aid-adma1158>3.0.co;2-6 · Cited by 395
One-Pot Reaction to Synthesize Water-Soluble Magnetite Nanocrystals
Li, Z., Chen, H., Bao, H., & Gao, M. (2004) · Chemistry of Materials · doi:10.1021/cm035346y · Cited by 360
Niederberger, M., Bartl, M. H., & Stucky, G. D. (2002) · Journal of the American Chemical Society · doi:10.1021/ja027115i · Cited by 360
Self-citationIron in Soils and Clay Minerals
Olis, A. C. (1989) · Soil Science · doi:10.1097/00010694-198904000-00013 · Cited by 335
Nonaqueous Synthesis of Nanocrystalline Semiconducting Metal Oxides for Gas Sensing
Pinna, N., Neri, G., Antonietti, M., & Niederberger, M. (2004) · Angewandte Chemie International Edition · doi:10.1002/anie.200460610 · Cited by 332
Self-citationLevy, L., Sahoo, Y., Kim, K.-S., Bergey, E. J., & Prasad, P. N. (2002) · Chemistry of Materials · doi:10.1021/cm0203013 · Cited by 320
Niederberger, M., Pinna, N., Polleux, J., & Antonietti, M. (2004) · Angewandte Chemie International Edition · doi:10.1002/anie.200353300 · Cited by 305
Self-citationNiederberger, M., Garnweitner, G., Pinna, N., & Antonietti, M. (2004) · Journal of the American Chemical Society · doi:10.1021/ja0494959 · Cited by 284
Self-citationComplex Dynamics of Mesoscopic Magnets
Awschalom, D. D., & DiVincenzo, D. P. (1995) · Physics Today · doi:10.1063/1.881448 · Cited by 273
Niederberger, M., Garnweitner, G., Krumeich, F., Nesper, R., Cölfen, H., & Antonietti, M. (2004) · Chemistry of Materials · doi:10.1021/cm031108r · Cited by 234
Self-citationMagnetic recording beyond the first 100 Years
Speliotis, D. (1999) · Journal of Magnetism and Magnetic Materials · doi:10.1016/s0304-8853(98)00399-0 · Cited by 212
Kumar, R. V., Koltypin, Y., Cohen, Y. S., Cohen, Y., Aurbach, D., Palchik, O., Felner, I., & Gedanken, A. (2000) · Journal of Materials Chemistry · doi:10.1039/b000440p · Cited by 186
Non‐Aqueous Synthesis of High‐Purity Metal Oxide Nanopowders Using an Ether Elimination Process
Pinna, N., Garnweitner, G., Antonietti, M., & Niederberger, M. (2004) · Advanced Materials · doi:10.1002/adma.200400460 · Cited by 168
Self-citationSynthesis of Yttria‐Based Crystalline and Lamellar Nanostructures and their Formation Mechanism
Pinna, N., Garnweitner, G., Beato, P., Niederberger, M., & Antonietti, M. (2004) · Small · doi:10.1002/smll.200400014 · Cited by 130
Self-citationDetermination of particle size distributions with angström resolution
Cölfen, H., & Pauck, T. (1997) · Colloid & Polymer Science · doi:10.1007/s003960050068 · Cited by 98
A novel nonaqueous route to V2O3 and Nb2O5 nanocrystals
Pinna, N., Antonietti, M., & Niederberger, M. (2004) · Colloids and Surfaces A Physicochemical and Engineering Aspects · doi:10.1016/j.colsurfa.2004.04.078 · Cited by 92
Self-citation
Cited by
Oh, J. K., & Park, J. M. (2011) · Progress in Polymer Science · doi:10.1016/j.progpolymsci.2010.08.005 · Cited by 427
Mutin, P. H., & Vioux, A. (2009) · Chemistry of Materials · doi:10.1021/cm802348c · Cited by 296
Functionalized Magnetite Nanoparticles—Synthesis, Properties, and Bio-Applications
Majewski, P., & Thierry, B. (2007) · Critical Reviews in Solid State and Materials Sciences · doi:10.1080/10408430701776680 · Cited by 289
Cui, X., Antonietti, M., & Yu, S. (2006) · Small · doi:10.1002/smll.200600047 · Cited by 255
Self-citationMagnetic Nanoparticles as MRI Contrast Agents
Avasthi, A., Caro, C., Pozo-Torres, E., Leal, M. P., & García-Martín, M. L. (2020) · Topics in Current Chemistry · doi:10.1007/s41061-020-00302-w · Cited by 253
Metadata
- Authors
- Pinna, N., Grancharov, S., Beato, P., Bonville, P., Antonietti, M., & Niederberger, M.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2005-05-01
- Volume
- 17
- Issue
- 11
- Pages
- 3044-3049
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2087284917
- Cited by
- 355
- References
- 31
- FWCI
- 12.09
- Type
- journal article
- Language
- en
- Open access
- closed
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
Are you an author, or do you see a problem with this page? Request a review
Data sources
Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.