The DOI matches its Crossref record; 19 of the 19 references it cites were found in a registry or an index.
Surface Enhanced NMR Spectroscopy by Dynamic Nuclear Polarization
Open accessAbstract
It is shown that surface NMR spectra can be greatly enhanced using dynamic nuclear polarization. Polarization is transferred from the protons of the solvent to the rare nuclei (here carbon-13 at natural isotopic abundance) at the surface, yielding at least a 50-fold signal enhancement for surface species covalently incorporated into a silica framework.
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Citations
Cites
Silica‐Based Mesoporous Organic–Inorganic Hybrid Materials
Hoffmann, F., Cornelius, M., Morell, J., & Fröba, M. (2006) · Angewandte Chemie International Edition · doi:10.1002/anie.200503075 · Cited by 3,089
An Improved Broadband Decoupling Sequence for Liquid Crystals and Solids
Fung, B. M., Khitrin, A. K., & Ermolaev, K. (2000) · Journal of Magnetic Resonance · doi:10.1006/jmre.1999.1896 · Cited by 1,987
Marion, D., Ikura, M., Tschudin, R., & Bax, A. (1989) · Journal of Magnetic Resonance (1969) · doi:10.1016/0022-2364(89)90152-2 · Cited by 1,397
Direct Syntheses of Ordered SBA-15 Mesoporous Silica Containing Sulfonic Acid Groups
Margolese, D. I., Melero, J. A., Christiansen, S. C., Chmelka, B. F., & Stucky, G. D. (2000) · Chemistry of Materials · doi:10.1021/cm0010304 · Cited by 975
Dynamic nuclear polarization at high magnetic fields
Maly, T., Debelouchina, G. T., Bajaj, V. S., Hu, K.-N., Joo, C.-G., Mak–Jurkauskas, M. L., Sirigiri, J. R., van der Wel, P. C. A., Herzfeld, J., Temkin, R. J., et al. (2008) · The Journal of Chemical Physics · doi:10.1063/1.2833582 · Cited by 919
Polarization-Enhanced NMR Spectroscopy of Biomolecules in Frozen Solution
Hall, D. A., Maus, D. C., Gerfen, G. J., Inati, S. J., Becerra, L. R., Dahlquist, F. W., & Griffin, R. G. (1997) · Science · doi:10.1126/science.276.5314.930 · Cited by 553
TOTAPOL: A Biradical Polarizing Agent for Dynamic Nuclear Polarization Experiments in Aqueous Media
Song, C., Hu, K.-N., Joo, C.-G., Swager, T. M., & Griffin, R. G. (2006) · Journal of the American Chemical Society · doi:10.1021/ja061284b · Cited by 550
Macquarrie, D. J. (1996) · Chem. Commun. · doi:10.1039/cc9960001961 · Cited by 426
Solid-state dynamic nuclear polarization at 263 GHz: spectrometer design and experimental results
Rosay, M., Tometich, L., Pawsey, S., Bader, R., Schauwecker, R., Blank, M., Borchard, P. M., Cauffman, S. R., Felch, K. L., Weber, R. T., et al. (2010) · Physical Chemistry Chemical Physics · doi:10.1039/c003685b · Cited by 370
High-Field Dynamic Nuclear Polarization for Solid and Solution Biological NMR
Barnes, A. B., De Paëpe, G., van der Wel, P. C. A., Hu, K.-N., Joo, C.-G., Bajaj, V. S., Mak-Jurkauskas, M. L., Sirigiri, J. R., Herzfeld, J., Temkin, R. J., et al. (2008) · Applied Magnetic Resonance · doi:10.1007/s00723-008-0129-1 · Cited by 359
Cited by
Dynamic nuclear polarization for sensitivity enhancement in modern solid-state NMR
Lilly Thankamony, A. S., Wittmann, J. J., Kaushik, M., & Corzilius, B. (2017) · Progress in Nuclear Magnetic Resonance Spectroscopy · doi:10.1016/j.pnmrs.2017.06.002 · Cited by 544
Highly Efficient, Water‐Soluble Polarizing Agents for Dynamic Nuclear Polarization at High Frequency
Sauvée, C., Rosay, M., Casano, G., Aussenac, F., Weber, R. T., Ouari, O., & Tordo, P. (2013) · Angewandte Chemie International Edition · doi:10.1002/anie.201304657 · Cited by 503
Kachala, V. V., Khemchyan, L. L., Kashin, A. S., Orlov, N. V., Grachev, A. A., Zalesskiy, S. S., & Ananikov, V. P. (2013) · Russian Chemical Reviews · doi:10.1070/rc2013v082n07abeh004413 · Cited by 262
Mentink-Vigier, F., Marin-Montesinos, I., Jagtap, A. P., Halbritter, T., van Tol, J., Hediger, S., Lee, D., Sigurdsson, S. T., & De Paëpe, G. (2018) · Journal of the American Chemical Society · doi:10.1021/jacs.8b04911 · Cited by 171
Takahashi, H., Ayala, I., Bardet, M., De Paëpe, G., Simorre, J.-P., & Hediger, S. (2013) · Journal of the American Chemical Society · doi:10.1021/ja312501d · Cited by 149
Metadata
- Authors
- Lesage, A., Lelli, M., Gajan, D., Caporini, M. A., Vitzthum, V., Miéville, P., Alauzun, J., Roussey, A., Thieuleux, C., Mehdi, A., Bodenhausen, G., Coperet, C., & Emsley, L.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2010-09-10
- Volume
- 132
- Issue
- 44
- Pages
- 15459-15461
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W1965194735
- Cited by
- 585
- References
- 19
- FWCI
- 13.13
- Type
- journal article
- Language
- en
- Open access
- green
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- Lesage, A., Lelli, M., Gajan, D., Caporini, M. A., Vitzthum, V., Miéville, P., Alauzun, J., Roussey, A., Thieuleux, C., Mehdi, A., Bodenhausen, G., Coperet, C., & Emsley, L. (2010). Surface Enhanced NMR Spectroscopy by Dynamic Nuclear Polarization. Journal of the American Chemical Society. https://doi.org/10.1021/ja104771z
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