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Cited by 248

The DOI matches its Crossref record; 2 of the 2 references it cites were found in a registry or an index.

Thiolysis−HPLC Characterization of Apple Procyanidins Covering a Large Range of Polymerization States

Guyot, Sylvain, Marnet, Nathalie, Drilleau, Jean-François·2001·Journal of Agricultural and Food Chemistry

Abstract

Procyanidins from the cortex of two cider apple varieties (Malus domestica; Kermerrien and Avrolles) were extracted by solvents. After a solid-phase extraction step, they were fractionated by normal- or reversed-phase HPLC at the semipreparative scale to obtain a series of purified fractions covering a wide range of polymerization states. Freeze-dried fractions were characterized by reversed-phase HPLC following thiolysis. Elution on normal-phase HPLC gave oligomeric procyanidins fractions with (average degree of polymerization) values varying from 2 to 8, whereas polymeric fractions ( values varying from 7 to 190) were obtained by reversed-phase HPLC. Constitutive units were mainly (-)-epicatechin with a proportion above 95% for all fractions. Thiolysis yields were wholly homogeneous with an average value of 75%, which indicates that the efficiency of the reaction did not depend on the polymerization state of the procyanidin fractions.

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Metadata

Authors
Guyot, S., Marnet, N., & Drilleau, J.-F.
Venue
Journal of Agricultural and Food Chemistry
Published
2000-12-06
Volume
49
Issue
1
Pages
14-20
ISSN
  • 0021-8561 (ISSN-L)
  • 1520-5118
OpenAlex
W2067308358
Cited by
248
References
2
FWCI
3.34
Type
journal article
Language
en
Open access
closed

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CoChat. (2026). Citation check: Thiolysis−HPLC Characterization of Apple Procyanidins Covering a Large Range of Polymerization States. https://app.cochat.ai/papers/10.1021/jf000814z
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Guyot, S., Marnet, N., & Drilleau, J.-F. (2001). Thiolysis−HPLC Characterization of Apple Procyanidins Covering a Large Range of Polymerization States. Journal of Agricultural and Food Chemistry. https://doi.org/10.1021/jf000814z

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