Solvent-surface interactions control the phase structure in laser-generated iron-gold core-shell nanoparticles
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This work highlights a strategy for the one-step synthesis of FeAu nanoparticles by the pulsed laser ablation of alloy targets in the presence of different solvents. This method allows particle generation without the use of additional chemicals; hence, solvent-metal interactions could be studied without cross effects from organic surface ligands. A detailed analysis of generated particles via transmission electron microscopy in combination with EDX elemental mapping could conclusively verify that the nature of the used solvent governs the internal phase structure of the formed nanoparticles. In the presence of acetone or methyl methacrylate, a gold shell covering a non-oxidized iron core was formed, whereas in aqueous media, an Au core with an Fe 3 O 4 shell was generated. This core-shell morphology was the predominant species found in >90% of the examined nanoparticles. These findings indicate that fundamental chemical interactions between the nanoparticle surface and the solvent significantly contribute to phase segregation and elemental distribution in FeAu nanoparticles. A consecutive analysis of resulting Fe@Au core-shell nanoparticles revealed outstanding oxidation resistance and fair magnetic and optical properties. In particular, the combination of these features with high stability magnetism and plasmonics may create new opportunities for this hybrid material in imaging applications.
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Wagener et al. observed that in the presence of acetone, Au shells overlap a non-oxidised iron core, and in water medium, an Au core with a Fe3O4 shell is generated, highlighting the crucial role of solvents in nanostructure formation.
“They observed that in the presence of acetone, the formation of Au shells overlaps a non-oxidised iron core, and in the water medium, an Au core with a Fe3O4 shell is generated, highlighting the crucial role of solvents in the formation of the nanostructure.”
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- Authors
- Wagener, P., Jakobi, J., Rehbock, C., Chakravadhanula, V. S. K., Thede, C., Wiedwald, U., Bartsch, M., Kienle, L., & Barcikowski, S.
- Affiliations
- University of Duisburg-Essen (DE)
- Christian-Albrechts-Universität zu Kiel (DE)
- Corresponding author
- Barcikowski, Stephan
- ORCID
- Venue
- Scientific Reports
- Published
- 2016-03-23
- Volume
- 6
- Issue
- 1
- Pages
- 23352-23352
- ISSN
- 2045-2322 (ISSN-L)
- PMC
- PMC4804215
- OpenAlex
- W2334104499
- Cited by
- 150
- References
- 71
- Citations by year
- 2026: 6 · 2025: 4 · 2024: 22 · 2023: 11 · 2022: 15 · 2021: 15 · 2020: 20 · 2019: 22 · 2018: 12 · 2017: 13 · 2016: 10
- FWCI
- 9.16
- Type
- journal article
- Language
- en
- Open access
- gold
- doi.org
- Locations
- Scientific Reports (publishedVersion, cc-by)
- PubMed Central (publishedVersion, cc-by)
- Repository KITopen (Karlsruhe Institute of Technology) (publishedVersion)
- PubMed (publishedVersion)
- DuEPublico (University of Duisburg-Essen) (submittedVersion, cc-by)
- Universitätsbibliographie, Universität Duisburg-Essen (submittedVersion)
- KITopen (other-oa)
- Funders
- Deutsche Forschungsgemeinschaft (BA 3580/18-1, KI 1263/15-1)
- Bundesministerium für Bildung und Forschung (FKZ03X5523, 03X5523)
- Universität Duisburg-Essen
- Topics
- Physical Sciences › Engineering › Biomedical Engineering › Laser-Ablation Synthesis of Nanoparticles
- Physical Sciences › Materials Science › Electronic, Optical and Magnetic Materials › Gold and Silver Nanoparticles Synthesis and Applications
- Physical Sciences › Materials Science › Materials Chemistry › Advanced Nanomaterials in Catalysis
- Keywords
- core-shell nanoparticles, pulsed laser ablation, phase segregation, acetone, methyl methacrylate, oxidation resistance, magnetic properties, plasmonics, nanoparticle synthesis
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