Cited by 411Planetary Science and ExplorationAstro and Planetary ScienceGeochemistry and Elemental Analysis

X-ray diffraction results from Mars science laboratory: mineralogy of rocknest at Gale Crater

Open access
Bish, D. L., Blake, D. F., Vaniman, D. T., Chipera, S. J., Morris, R. V., Ming, D. W., Treiman, A. H., Sarrazin, P. +457 more·2013·Science

Abstract

The Mars Science Laboratory rover Curiosity scooped samples of soil from the Rocknest aeolian bedform in Gale crater. Analysis of the soil with the Chemistry and Mineralogy (CheMin) x-ray diffraction (XRD) instrument revealed plagioclase (~An57), forsteritic olivine (~Fo62), augite, and pigeonite, with minor K-feldspar, magnetite, quartz, anhydrite, hematite, and ilmenite. The minor phases are present at, or near, detection limits. The soil also contains 27 ± 14 weight percent x-ray amorphous material, likely containing multiple Fe 3+ - and volatile-bearing phases, including possibly a substance resembling hisingerite. The crystalline component is similar to the normative mineralogy of certain basaltic rocks from Gusev crater on Mars and of martian basaltic meteorites. The amorphous component is similar to that found on Earth in places such as soils on the Mauna Kea volcano, Hawaii.

The claims and statistics of this paper haven’t been checked yet.

Run the check — free, no account needed. It reads the open-access text and checks the sources it cites.

A few free checks a day · papers already verified open instantly · results are public

Integrity signals

Registry

Crossref · 10.1126/science.1238932

Cites

2 of 2 references verified0 citation errors · 0 not checkable

Statistics

Claims the paper makes

The claims and statistics of this paper haven’t been checked yet.

Run the check — free, no account needed. It reads the open-access text and checks the sources it cites.

A few free checks a day · papers already verified open instantly · results are public

Claims other papers make about this one

Each is checked against this paper’s own text: does it say what the citing paper says it does?

  • Rocknest is the best-characterized martian soil to date.

    “Rocknest is the bestcharacterized martian soil to date (Bish et al., 2013; Blake et al., 2013; Leshin et al., 2013; Minitti et al., 2013; Archer et al., 2014; Sutter et al., 2017)”

    From Mars global simulant MGS-1: A Rocknest-based open standard for basaltic martian regolith simulants (2019) · cites this paper as Bish et al., 2013

    The Discussion (page not provided) reports a rich inventory of crystalline and amorphous phases in Rocknest soil and says the XRD results provide critical ground-truth information. This supports Rocknest being well characterized mineralogically, but the paper does not establish that it is the best-characterized Martian soil overall or to date. (LLM, conf=0.83)

    Experimental — accuracy not yet measured
  • Martian soils are a subequal mixture of crystalline and amorphous phases, as revealed by the CheMin instrument on the Mars Science Laboratory.

    “In contrast, martian soils are a subequal mixture of crystalline and amorphous phases, as revealed by the CheMin instrument on the Mars Science Laboratory (MSL) (Bish et al., 2013; Dehouck et al., 2014).”

    From Mars global simulant MGS-1: A Rocknest-based open standard for basaltic martian regolith simulants (2019) · cites this paper as Bish et al., 2013

    The “Amorphous or Poorly Ordered Components” section (page not specified) reports that CheMin found both crystalline and amorphous phases in Rocknest soil, but estimates the amorphous fraction at 27 wt%, leaving roughly 73 wt% crystalline—not a subequal mixture by the central estimates. The Discussion suggests the results may apply to other Martian soils, but does not establish the same proportions for Martian soils generally. (LLM, conf=0.88)

    Experimental — accuracy not yet measured
  • The crystalline fraction of Rocknest is well constrained by X-ray diffraction.

    “The crystalline fraction of Rocknest is well constrained by XRD (Bish et al., 2013).”
  • The detected crystalline phases in Rocknest include plagioclase, pyroxene, olivine, magnetite, anhydrite, hematite, ilmenite, sanidine, and quartz.

    “The detected crystalline phases in Rocknest include plagioclase, pyroxene, olivine, magnetite, anhydrite, hematite, ilmenite, sanidine, and quartz (Bish et al., 2013).”
  • Unit cell parameters for Rocknest minerals indicate ~An57 plagioclase, a mixture of augite and pigeonite, and ~Fo40 olivine.

    “Unit cell parameters for Rocknest minerals indicate ~An57 plagioclase (Bish et al., 2013), a mixture of augite and pigeonite (Bish et al., 2013), and ~Fo40 olivine (Morris et al., 2015).”

Self-check

Percentages, sums and reported differences re-computed from the paper’s own numbers.

The self-check needs the paper’s full text.

Cites

Flagged first, then by citations

Research works printed but not linked: 29

  1. R. Gellert et al., Chemistry of rocks and soils in Gusev Crater from the alpha particle x-ray spectrometer. Science 305, 829-832 (2004). doi: 10.1126/ science.1099913; pmid: 15297665 · DOI
  2. A. S. Yen et al., An integrated view of the chemistry and mineralogy of martian soils. Nature 436, 49-54 (2005). doi: 10.1038/nature03637; pmid: 16001059 · DOI · Paper page
  3. I. O. McGlynn, C. M. Fedo, H. Y. McSween Jr., Soil mineralogy at the Mars Exploration Rover landing sites: An assessment of the competing roles of physical sorting and chemical weathering. J. Geophys. Res. 117, E01006 (2012). doi: 10.1029/2011JE003861 · DOI
  4. H. Y. McSween Jr., I. O. McGlynn, A. D. Rogers, Determining the modal mineralogy of Martian soils. J. Geophys. Res. 115, E00F12 (2010). doi: 10.1029/ 2010JE003582 · DOI
  5. R. V. Morris et al., Mössbauer mineralogy of rock, soil, and dust at Gusev Crater, Mars: Spirit's journey through weakly altered olivine basalt on the Plains and pervasively altered basalt in the Columbia Hills. J. Geophys. Res. 111, E02S13 (2006). doi: 10.1029/ 2005JE002584 · DOI
  6. R. V. Morris et al., Mineralogy at Gusev crater from the Mossbauer spectrometer on the Spirit rover. Science 305, 833-836 (2004). doi: 10.1126/science.1100020; pmid: 15297666 · DOI
  7. P. R. Christensen et al., Mineralogy at Meridiani Planum from the Mini-TES Experiment on the Opportunity Rover. Science 306, 1733-1739 (2004). doi: 10.1126/ science.1104909; pmid: 15576609 · DOI
  8. M. Eckert, Max von Laue and the discovery of x-ray diffraction in 1912. Ann. Phys. 524, A83-A85 (2012). doi: 10.1002/andp.201200724 · DOI
  9. R. V. Morris et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 1653; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  10. A. S. Yen et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 2495; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  11. R. Gellert et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 1432; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  12. D. F. Blake et al., Curiosity at Gale crater, Mars: Characterization and analysis of the Rocknest sand shadow. Science 341, 1239505 (2013).
  13. S. M. Morrison et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 1831; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  14. A. H. Treiman et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 1113; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  15. P. D. Archer Jr. et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 2168; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  16. L. A. Leshin et al., Volatile, isotope, and organic analysis of martian fines with the Mars Curiosity rover. Science 341, 1238937 (2013).
  17. S. J. Chipera, D. L. Bish, FULLPAT: A full-pattern quantitative analysis program for x-ray powder diffraction using measured and calculated patterns. J. Appl. Cryst. 35, 744-749 (2002). doi: 10.1107/S0021889802017405 · DOI
  18. F. H. Chung, Quantitative interpretation of x-ray diffraction patterns of mixtures. II. Adiabatic principle of x-ray diffraction analysis of mixtures. J. Appl. Cryst. 7, 526-531 (1974). doi: 10.1107/S0021889874010387 · DOI
  19. R. Yingst et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 1257; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  20. D. F. Blake et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 1289; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  21. W. T. Pike et al., Quantification of the dry history of the Martian soil inferred from in situ microscopy. Geophys. Res. Lett. 38, L24201 (2011). doi: 10.1029/ 2011GL049896 · DOI · Paper page
  22. S. W. Ruff, Spectral evidence for zeolite in the dust on Mars. Icarus 168, 131-143 (2004). doi: 10.1016/j.icarus.2003.11.003 · DOI
  23. D. W. Ming et al., Geochemical and mineralogical indicators for aqueous processes in the Columbia Hills of Gusev crater, Mars. J. Geophys. Res. Planets 111, E02S12 (2006). doi: 10.1029/2005JE002560 · DOI
  24. R. E. Milliken, J. P. Grotzinger, B. J. Thomson, Paleoclimate of Mars as captured by the stratigraphic record in Gale Crater. Geophys. Res. Lett. 37, L04201 (2010). doi: 10.1029/2009GL041870 · DOI
  25. R. V. Morris et al., Phyllosilicate-poor palagonitic dust form Mauna Kea Volcano (Hawaii): A mineralogical analogue for magnetic martian dust? J. Geophys. Res. 106, 5057-5083 (2001). doi: 10.1029/ 2000JE001328 · DOI · Paper page
  26. R. Gellert et al., Alpha Particle X-Ray Spectrometer (APXS): Results from Gusev crater and calibration report. J. Geophys. Res. 111, E02S05 (2006). doi: 10.1029/2005JE002555 · DOI
  27. D. Blake et al., Characterization and calibration of the CheMin mineralogical instrument on Mars Science Laboratory. Space Sci. Rev. 170, 341-399 (2012). doi: 10.1007/s11214-012-9905-1 · DOI
  28. C. N. Achilles, R. V. Morris, S. J. Chipera, D. W. Ming, E. B. Rampe, presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 3072; published on CD by the Lunar and Planetary Institute, Houston, TX (2013).
  29. E. B. Rampe et al., presented at the 44th Lunar and Planetary Science Conference, March 2013, abstract 1188; published on CD by the Lunar and Planetary Institute, Houston, TX (2013). REFERENCES http://science.sciencemag.org/content/341/6153/1238932#BIBL This article cites 21 articles, 6 of which you can access for free PERMISSIONS http://www.sciencemag.org/help/reprints-and-permissions Terms of Service Use of this article is subject to the is a registered trademark of AAAS. Science licensee American Association for the Advancement of Science. No claim to original U.S. Government Works. The title Science, 1200 New York Avenue NW, Washington, DC 20005. 2017 © The Authors, some rights reserved; exclusive (print ISSN 0036-8075; online ISSN 1095-9203) is published by the American Association for the Advancement of Science on September 18, 2018 http://science.sciencemag.org/ Downloaded from

Cited by

Sorted by citations

Authors
Bish, D. L., Blake, D. F., Vaniman, D. T., Chipera, S. J., Morris, R. V., Ming, D. W., Treiman, A. H., Sarrazin, P., Morrison, S. M., Downs, R. T., Achilles, C. N., Yen, A. S., Bristow, T. F., Crisp, J. A., Morookian, J. M., Farmer, J. D., Rampe, E. B., Stolper, E. M., Spanovich, N., MSL Science Team, Achilles, C., Agard, C., Verdasca, J. A. A., Anderson, R., Anderson, R., Archer, D., Armiens-Aparicio, C., Arvidson, R., Atlaskin, E., Atreya, S., Aubrey, A., Baker, B., Baker, M., Balic-Zunic, T., Baratoux, D., Baroukh, J., Barraclough, B., Bean, K., Beegle, L., Behar, A., Bell, J., Bender, S., Benna, M., Bentz, J., Berger, G., Berger, J., Berman, D., Bish, D., Blake, D. F., Avalos, J. J. B., Blaney, D., Blank, J., Blau, H., Bleacher, L., Boehm, E., Botta, O., Böttcher, S., Boucher, T., Bower, H., Boyd, N., Boynton, B., Breves, E., Bridges, J., Bridges, N., Brinckerhoff, W., Brinza, D., Bristow, T., Brunet, C., Brunner, A., Brunner, W., Buch, A., Bullock, M., Burmeister, S., Cabane, M., Calef, F., Cameron, J., Campbell, J. "., Cantor, B., Caplinger, M., Rodríguez, J. C., Carmosino, M., Blázquez, I. C., Charpentier, A., Chipera, S., Choi, D., Clark, B., Clegg, S., Cleghorn, T., Cloutis, E., Cody, G., Coll, P., Conrad, P., Coscia, D., Cousin, A., Cremers, D., Crisp, J., Cros, A., Cucinotta, F., d'Uston, C., Davis, S., Day, M. "., Juarez, M. D. L. T., DeFlores, L., DeLapp, D., DeMarines, J., DesMarais, D., Dietrich, W., Dingler, R., Donny, C., Downs, B., Drake, D., Dromart, G., Dupont, A., Duston, B., Dworkin, J., Dyar, M. D., Edgar, L., Edgett, K., Edwards, C., Edwards, L., Ehlmann, B., Ehresmann, B., Eigenbrode, J., Elliott, B., Elliott, H., Ewing, R., Fabre, C., Fairén, A., Farley, K., Farmer, J., Fassett, C., Favot, L., Fay, D., Fedosov, F., Feldman, J., Feldman, S., Fisk, M., Fitzgibbon, M., Flesch, G., Floyd, M., Flückiger, L., Forni, O., Fraeman, A., Francis, R., François, P., Franz, H., Freissinet, C., French, K. L., Frydenvang, J., Gaboriaud, A., Gailhanou, M., Garvin, J., Gasnault, O., Geffroy, C., Gellert, R., Genzer, M., Glavin, D., Godber, A., Goesmann, F., Goetz, W., Golovin, D., Gómez, F. G., Gómez-Elvira, J., Gondet, B., Gordon, S., Gorevan, S., Grant, J., Griffes, J., Grinspoon, D., Grotzinger, J., Guillemot, P., Guo, J., Gupta, S., Guzewich, S., Haberle, R., Halleaux, D., Hallet, B., Hamilton, V., Hardgrove, C., Harker, D., Harpold, D., Harri, A.-M., Harshman, K., Hassler, D., Haukka, H., Hayes, A., Herkenhoff, K., Herrera, P., Hettrich, S., Heydari, E., Hipkin, V., Hoehler, T., Hollingsworth, J., Hudgins, J., Huntress, W., Hurowitz, J., Hviid, S., Iagnemma, K., Indyk, S., Israël, G., Jackson, R., Jacob, S., Jakosky, B., Jensen, E., Jensen, J. K., Johnson, J., Johnson, M., Johnstone, S., Jones, A., Jones, J., Joseph, J., Jun, I., Kah, L., Kahanpää, H., Kahre, M., Karpushkina, N., Kasprzak, W., Kauhanen, J., Keely, L., Kemppinen, O., Keymeulen, D., Kim, M.-H., Kinch, K., King, P., Kirkland, L., Kocurek, G., Koefoed, A., Köhler, J., Kortmann, O., Kozyrev, A., Krezoski, J., Krysak, D., Kuzmin, R., Lacour, J. L., Lafaille, V., Langevin, Y., Lanza, N., Lasue, J., Le Mouélic, S., Lee, E. M., Lee, Q.-M., Lees, D., Lefavor, M., Lemmon, M., Malvitte, A. L., Leshin, L., Léveillé, R., Lewin-Carpintier, É., Lewis, K., Li, S., Lipkaman, L., Little, C., Litvak, M., Lorigny, E., Lugmair, G., Lundberg, A., Lyness, E., Madsen, M., Mahaffy, P., Maki, J., Malakhov, A., Malespin, C., Malin, M., Mangold, N., Manhes, G., Manning, H., Marchand, G., Jiménez, M. M., García, C. M., Martin, D., Martin, M., Martínez-Frías, J., Martín-Soler, J., Martín-Torres, F. J., Mauchien, P., Maurice, S., McAdam, A., McCartney, E., McConnochie, T., McCullough, E., McEwan, I., McKay, C., McLennan, S., McNair, S., Melikechi, N., Meslin, P.-Y., Meyer, M., Mezzacappa, A., Miller, H., Miller, K., Milliken, R., Ming, D., Minitti, M., Mischna, M., Mitrofanov, I., Moersch, J., Mokrousov, M., Jurado, A. M., Moores, J., Mora-Sotomayor, L., Morookian, J. M., Morris, R., Morrison, S., Mueller-Mellin, R., Muller, J.-P., Caro, G. M., Nachon, M., López, S. N., Navarro-González, R., Nealson, K., Nefian, A., Nelson, T., Newcombe, M., Newman, C., Newsom, H., Nikiforov, S., Niles, P., Nixon, B., Dobrea, E. N., Nolan, T., Oehler, D., Ollila, A., Olson, T., Owen, T., Hernández, M. Á. D. P., Paillet, A., Pallier, E., Palucis, M., Parker, T., Parot, Y., Patel, K., Paton, M., Paulsen, G., Pavlov, A., Pavri, B., Peinado-González, V., Pepin, R., Peret, L., Perez, R., Perrett, G., Peterson, J., Pilorget, C., Pinet, P., Pla-García, J., Plante, I., Poitrasson, F., Polkko, J., Popa, R., Posiolova, L., Posner, A., Pradler, I., Prats, B., Prokhorov, V., Purdy, S. W., Raaen, E., Radziemski, L., Rafkin, S., Ramos, M., Rampe, E., Raulin, F., Ravine, M., Reitz, G., Rennó, N., Rice, M., Richardson, M., Robert, F., Robertson, K., Manfredi, J. A. R., Romeral-Planelló, J. J., Rowland, S., Rubin, D., Saccoccio, M., Salamon, A., Sandoval, J., Sanin, A., Fuentes, S. A. S., Saper, L., Sarrazin, P., Sautter, V., Savijärvi, H., Schieber, J., Schmidt, M., Schmidt, W., Scholes, D. "., Schoppers, M., Schröder, S., Schwenzer, S., Martinez, E. S., Sengstacken, A., Shterts, R., Siebach, K., Siili, T., Simmonds, J., Sirven, J.-B., Slavney, S., Sletten, R., Smith, M., Sánchez, P. S., Spanovich, N., Spray, J., Squyres, S., Stack, K., Stalport, F., Steele, A., Stein, T., Stern, J., Stewart, N., Stipp, S. L. S., Stoiber, K., Stolper, E., Sucharski, B., Sullivan, R., Summons, R., Sumner, D., Sun, V., Supulver, K., Sutter, B., Szopa, C., Tan, F., Tate, C., Teinturier, S., ten Kate, I., Thomas, P., Thompson, L., Tokar, R., Toplis, M., Redondo, J. T., Trainer, M., Treiman, A., Tretyakov, V., Urqui-O'Callaghan, R., Van Beek, J., Van Beek, T., VanBommel, S., Vaniman, D., Varenikov, A., Vasavada, A., Vasconcelos, P., Vicenzi, E., Vostrukhin, A., Voytek, M., Wadhwa, M., Ward, J., Webster, C., Weigle, E., Wellington, D., Westall, F., Wiens, R. C., Wilhelm, M. B., Williams, A., Williams, J., Williams, R., Williams, R. B. "., Wilson, M., Wimmer-Schweingruber, R., Wolff, M., Wong, M., Wray, J., Wu, M., Yana, C., Yen, A., Yingst, A., Zeitlin, C., Zimdar, R., & Mier, M.-P. Z.
Affiliations
  • Department of Geological Sciences, Indiana University, Bloomington, IN 47405, USA.
  • Ames Research Center (US)
  • Planetary Science Institute (US)
  • Chesapeake Energy, Oklahoma City, OK 73154, USA.
  • NASA Johnson Space Center, Houston, TX 77058, USA.
  • Johnson Space Center (US)
  • Lunar and Planetary Institute, Houston, TX 77058, USA.
  • In-Xitu, Campbell, CA 95008, USA.
  • University of Arizona (US)
  • Engineering and Science Contract Group/United Technologies Corporation Aerospace Systems, Houston, TX 77058, USA.
  • Jet Propulsion Laboratory (US)
  • NASA Ames Research Center, Moffett Field, CA 94035, USA.
  • Jet Propulsion Laboratory/California Institute of Technology, Pasadena, CA 91109, USA.
  • Arizona State University (US)
  • California Institute of Technology (US)
  • Indiana University Bloomington (US)
  • GeoRessources (FR)
  • Lunar and Planetary Institute (US)
ORCID
Venue
Science
Published
2013-09-27
Volume
341
Issue
6153
Pages
1238932-1238932
ISSN
  • 0036-8075 (ISSN-L)
  • 1095-9203
OpenAlex
W1981028812
Cited by
411
References
2
Citations by year
2026: 13 · 2025: 27 · 2024: 23 · 2023: 26 · 2022: 22 · 2021: 28 · 2020: 20 · 2019: 26 · 2018: 27 · 2017: 35 · 2016: 81 · 2015: 42 · 2014: 30 · 2013: 11
FWCI
28.01
Type
journal article
Language
en
Open access
Locations
  • Science (publishedVersion)
  • PubMed (publishedVersion)
  • elib (German Aerospace Center) (acceptedVersion)
  • Smithsonian Digital Repository (Smithsonian Institution) (submittedVersion)
  • CaltechAUTHORS (California Institute of Technology) (submittedVersion)
  • HAL (submittedVersion)
  • Utrecht University Repository (Utrecht University) (submittedVersion)
  • elib (German Aerospace Center) (submittedVersion)
  • UCL Discovery (University College London) (submittedVersion)
Topics
  • Physical Sciences › Physics and Astronomy › Astronomy and Astrophysics › Planetary Science and Exploration
  • Physical Sciences › Physics and Astronomy › Astronomy and Astrophysics › Astro and Planetary Science
  • Physical Sciences › Earth and Planetary Sciences › Geochemistry and Petrology › Geochemistry and Elemental Analysis
Keywords
Gale Crater, Curiosity rover, plagioclase, forsteritic olivine, augite, pigeonite, K-feldspar, magnetite, hisingerite, basaltic meteorites, Gusev Crater

About these checks

Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.

Statistics and arithmetic are recomputed, not judged.

Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.

What counts as a claim ›How we measure confidence ›How we check this ›

Are you an author, or do you see a problem with this page? Request a review