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Reporting physisorption data for gas/solid systems with special reference to the determination of surface area and porosity (Recommendations 1984)
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micropore filling.The BET method is unlikely to yield a value of the actual surface area if the isotherm is either Type I or Type III; but both Type II and Type IV isotherms are, in general, amenable to the BET analysis, provided that the value of C is neither too low nor too high and that the BET plot is linear in the region of the isotherm containing Point B.The computation of mesopore size distribution is valid only if the isotherm is of Type IV, but in view of the complexity of most pore systems little is to be gained by the application of an elaborate method of computation.If a Type I isotherm exhibits a nearly constant adsorption at high relative pressure, the micropore volume is given by the amount adsorbed at the plateau.At present there is no reliable procedure available for the computation of the micropore size distribution from a single isotherm.A check list is recommended to assist authors in the measurement of adsorption isotherms and the presentation of the data in the primary literature. CONTENTS SECTION 1.Recent work has drawn attention to the complexity of capillary condensation in pore networks and has indicated that a pore size distribution curve derived from the desorption branch of the loop is likely to be unreliable if pore blocking effects occur.It is significant that a very steep desorption branch is usually found if the lower closure point of the loop is located at the limiting p/p° (see Section 5.3).In particular, the
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“While, the adsorption capacities of the three specimens increase to a limiting value near a straight line when the relative pressures (P/P0) are extremely low, which meets the requirements of the Type I adsorption isotherms [21]”
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“Obtained pigments have an isotherm shape corresponding to types IV and V according to the IUPAC classification [63,64] (Figure 3).”
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“The IeV profile of the Mo-RF electrode in Fig. 6 show similar shape with commercial electrode performance in alkaline electrolysers as reported by Amitava [37].”
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“The cell electrode voltage of the Mo-RF at 298 K in Table 1 are at lower ranges compared with similar IeV profile at 348 K in that report.”
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Metadata
- Authors
- Sing, K. S. W.
- Corresponding author
- Sing, K. S. W.
- Venue
- Pure and Applied Chemistry
- Publisher
- Walter de Gruyter GmbH
- Published
- 1985-01-01
- Volume
- 57
- Issue
- 4
- Pages
- 603-619
- ISSN
- 0033-4545 (ISSN-L)
- 1365-3075
- OpenAlex
- W1980704616
- Cited by
- 24,485
- References
- 0
- Citations by year
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- FWCI
- 16.93
- Type
- journal article
- Language
- en
- Open access
- bronze
- doi.org
- Locations
- Pure and Applied Chemistry (publishedVersion)
- Topics
- Physical Sciences › Chemistry › Physical and Theoretical Chemistry › Adsorption, diffusion, and thermodynamic properties of materials
- Physical Sciences › Materials Science › Materials Chemistry › Mesoporous Materials and Catalysis
- Physical Sciences › Chemistry › Analytical Chemistry › Analytical Chemistry and Chromatography
- Keywords
- physisorption, gas-solid systems, surface area determination, porosity determination, reporting recommendations, adsorption isotherms, BET method
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
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