Hydrothermal Treatment of Tannin: A Route to Porous Metal Oxides and Metal/Carbon Hybrid Materials
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In the present paper, porous materials were prepared from the hydrothermal treatment of aqueous solutions of tannin, a renewable phenolic resource extracted from tree barks, containing dissolved salts of transition metals: V, Cr, Ni and Fe. Hydrothermal treatment produced carbonaceous particles doped with the aforementioned metals, and such materials were treated according to two different routes: (i) calcination in air in order to burn the carbon and to recover porous oxides; (ii) pyrolysis in inert atmosphere so as to recover porous metal/carbon hybrid materials. The nature of the metal salt was found to have a dramatic impact on the structure of the materials recovered by the first route, leading either to nano-powders (V, Cr) or to hollow microspheres (Ni, Fe). The second route was only investigated with iron, leading to magnetic Fe-loaded micro/mesoporous carbons whose texture, pore volumes and surface areas gradually changed with the iron content.
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Iron ion had a catalytic effect on production of gas, contributing to production of carbon materials with higher porosity and surface area.
“Braghiroli et al. [38] pointed out that the iron ion had a catalytic effect on the production of gas, contributing to the production of carbon materials with higher porosity and surface area.”
From Preparation of Microporous Carbon from <i>Sargassum horneri</i> by Hydrothermal Carbonization and KOH Activation for CO<sub>2</sub> Capture (2018) · cites this paper as [38]
Iron ion can accelerate hydrothermal carbonization reaction and promote formation of pores.
“Secondly, iron ion can accelerate hydrothermal carbonization reaction and promote the formation of pores.”
From Preparation of Microporous Carbon from <i>Sargassum horneri</i> by Hydrothermal Carbonization and KOH Activation for CO<sub>2</sub> Capture (2018) · cites this paper as [38]
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- Authors
- Braghiroli, F., Fierro, V., Szczurek, A., Gadonneix, P., Ghanbaja, J., Parmentier, J., Medjahdi, G., & Celzard, A.
- Affiliations
- Centre National de la Recherche Scientifique (FR)
- Institut Jean Lamour, UMR CNRS—Université de Lorraine n° 7198, ENSTIB, Parc de Saurupt, CS 50840, F-54011 Nancy CEDEX, France
- Corresponding author
- Celzard, Alain
- ORCID
- Venue
- Inorganics
- Publisher
- MDPI AG
- Published
- 2017-01-24
- Volume
- 5
- Issue
- 1
- Pages
- 7
- ISSN
- 2304-6740 (ISSN-L)
- OpenAlex
- W2581058304
- Cited by
- 25
- References
- 66
- Citations by year
- 2026: 4 · 2025: 2 · 2024: 1 · 2022: 3 · 2021: 1 · 2020: 4 · 2019: 6 · 2018: 3 · 2017: 1
- FWCI
- 1.62
- Type
- journal article
- Language
- en
- Open access
- gold
- doi.org
- Licence
- Locations
- Inorganics (publishedVersion, cc-by)
- HAL (submittedVersion, other-oa)
- DOAJ (DOAJ: Directory of Open Access Journals) (submittedVersion, cc-by-sa)
- univOAK (4 institutions : Université de Strasbourg, Université de Haute Alsace, INSA Strasbourg, Bibliothèque Nationale et Universitaire de Strasbourg) (submittedVersion, cc-by)
- Topics
- Physical Sciences › Materials Science › Materials Chemistry › Mesoporous Materials and Catalysis
- Physical Sciences › Materials Science › Materials Chemistry › Chemical and Physical Properties of Materials
- Physical Sciences › Engineering › Biomedical Engineering › Thermochemical Biomass Conversion Processes
- Keywords
- tannins, hydrothermal treatment, porous metal oxides, transition metal salts, vanadium, chromium, nickel, iron, calcination, pyrolysis, hollow microspheres, magnetic carbon, mesoporous carbon
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
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