Multifunctional Loblolly Pine-Derived Superactivated Hydrochar: Effect of Hydrothermal Carbonization on Hydrogen and Electron Storage with Carbon Dioxide and Dye Removal
Open accessAbstract
Pore modulation via hydrothermal carbonization (HTC) needs investigation due to its crucial effect on surface that influences its multirole utilization of such ultraporous sorbents in applications of energy storage- hydrogen and capacitive- as well as for pollutant abatement- carbon capture and dye removal. Hence, loblolly pine was hydrothermally carbonized followed by KOH activation to synthesize superactivated hydrochars (SAH). The resulting SAHs had specific surface area (SSA) 1462–1703 m2/g, total pore (TPV) and micropore volume (MPV) of 0.62–0.78 cm3/g and 0.33–0.49 cm3/g, respectively. The SAHs exhibit excellent multifunctional performance with remarkably high atmospheric CO2 capture of 145.2 mg/g and high pressure cryogenic H2 storage of 54.9 mg/g. The fabricated supercapacitor displayed substantial specific capacitance value of maximum 47.2 Fg−1 at 1 A g−1 in 6 M KOH and highest MB dye removal of 719.4 mg/g. Higher HTC temperature resulted in increased surface porosity as higher SSA, TPV benefitted H2 storage and MB dye removal while superior MPV favored CO2 capture. Moderate HTC temperature ensured higher mesopore-to-macropore volume ratio favoring electrochemical performance. Isotherm modelling of the adsorbates was compared using models: Langmuir, Freundlich, Langmuir- Freundlich and Temkin.
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The hydrochar predominantly comprises aromatic and aliphatic hydrocarbons, evident in a broad diffraction peak within the 15-21° range characteristic of amorphous carbon.
“The hydrochar predominantly comprises aromatic and aliphatic hydrocarbons61, evident in a broad diffraction peak within the 15–21° range, characteristic of the amorphous carbon diffraction pattern62.”
From Efficient CO2 adsorption by deoiled flaxseed hydrochar (2024) · cites this paper as [62]
Section 3.1 reports the broad 15–21° peak characteristic of amorphous carbon, but only for hydrochar prepared at 260 °C; hydrochars prepared at 180 and 220 °C retained cellulose-related peaks. The aromatic-and-aliphatic composition statement is attached to a different citation in the citing sentence, so this verdict addresses the diffraction claim. (LLM, conf=0.88)
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Giraldo, L., & Moreno‐Piraján, J. C. (2013) · Journal of Analytical and Applied Pyrolysis · doi:10.1016/j.jaap.2013.07.009 · Cited by 15 · see citing works
Molecular insight on unusually high specific hydrogen adsorption over silicon carbide
Yaremov, P. S., Shcherban, N., Aho, A., et al. (2019) · International Journal of Hydrogen Energy · doi:10.1016/j.ijhydene.2019.01.081 · Cited by 8 · see citing works
Flagged first, then by citations
Research works printed but not linked: 1
- [91]Smith J.M. Chemical Engineering Kinetics, 3rd Edition (McGraw-Hill Chemical Engineerin g Series) McGraw-Hill New York, NY, USA 1981 978-0-07-058710-6
Cited by
Sorted by citations
Chambers, C., Saha, S., Grimes, S., Calhoun, J., & Reza, M. T. (2024) · Biomass Conversion and Biorefinery · doi:10.1007/s13399-023-04326-2 · Cited by 14 · see citing works
Self-citationEfficient CO2 adsorption by deoiled flaxseed hydrochar
Arefizadeh, M., Behvandi, D., Shahhosseini, S., & Ghaemi, A. (2024) · Scientific Reports · doi:10.1038/s41598-024-78177-w · Cited by 4 · see citing works
- Authors
- Sultana, A. I., Chambers, C., Ahmed, M. M. N., Pathirathna, P., & Reza, T.
- Affiliations
- Florida Institute of Technology (US)
- Department of Biomedical and Chemical Engineering and Sciences, Florida Institute of Technology, Melbourne, FL 32901, USA
- Venue
- Nanomaterials
- Publisher
- MDPI AG
- Published
- 2022-10-12
- Volume
- 12
- Issue
- 20
- Pages
- 3575
- ISSN
- 2079-4991 (ISSN-L)
- PMC
- PMC9606919
- OpenAlex
- W4304775508
- Cited by
- 17
- References
- 107
- Citations by year
- 2026: 3 · 2025: 2 · 2024: 6 · 2023: 5 · 2022: 1
- FWCI
- 1.32
- Type
- journal article
- Language
- en
- Open access
- gold
- doi.org
- Licence
- Locations
- Nanomaterials (publishedVersion, cc-by)
- PubMed Central (publishedVersion, cc-by)
- PubMed (publishedVersion)
- DOAJ (DOAJ: Directory of Open Access Journals) (submittedVersion, cc-by-sa)
- Funders
- United States Department of Agriculture (2019-67019-31594)
- Topics
- Physical Sciences › Engineering › Mechanical Engineering › Carbon Dioxide Capture Technologies
- Physical Sciences › Environmental Science › Water Science and Technology › Adsorption and biosorption for pollutant removal
- Physical Sciences › Engineering › Biomedical Engineering › Thermochemical Biomass Conversion Processes
- Keywords
- hydrothermal carbonization, Pinus taeda, KOH activation, hydrogen storage, CO2 capture, supercapacitors, pore structure, microporosity, adsorption isotherms, biomass-derived carbon
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
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