Cited by 152MXene and MAX Phase MaterialsAdvancements in Battery MaterialsSupercapacitor Materials and Fabrication

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Synthesis and Electrochemical Properties of Two-Dimensional RGO/Ti3C2Tx Nanocomposites

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Shen, Changjie, Wang, Libo, Zhou, Aiguo, Wang, Bo, Wang, Xiaolong, Lian, Weiwei, Hu, Qianku, Qin, Gang, Liu, Xuqing·2018·Nanomaterials

DOI 10.3390/nano8020080PMC PMC5853712

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Abstract

MXene is a new type of two-dimensional layered material. Herein, a GO/Ti3C2Tx nanocomposite was prepared by a simple liquid phase method, and the obtained GO/Ti3C2Tx was transformed into RGO/Ti3C2Tx under high temperature with Ar/H2. The prepared samples were characterized using X-ray diffraction (XRD), Raman measurement, scanning electron microscopy (SEM), energy disperse spectroscopy (EDS), and X-ray photoelectron spectroscopy (XPS). As an electrode material in lithium-ion batteries, the RGO/Ti3C2Tx nanocomposite exhibited an excellent electrochemical performance and an excellent rate performance. Compared to pure Ti3C2Tx, the nanocomposite had a better reversible capacity at different current densities and had no attenuation after 200 cycles, which is one time higher than pure Ti3C2Tx. The improvement in the specific capacity was due to the excellent electrical conductivity and the unique structure of RGO, in which a charge transfer bridge was built among the Ti3C2Tx flakes. Such a bridge shortened the transmission distance of the electrons and ions and effectively controlled the restacking of the laminated materials.

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Figure 1 (a) X-ray diffraction (XRD) patterns and (b) Raman spectrum of Ti3AlC2, Ti3C2Tx, and GO/Ti3C2Tx, and RGO/Ti3C2Tx nanocomposites.CC BY · PubMed Central

Figure 2 Scanning electron microscopy (SEM) image of Ti3AlC2 (a), Ti3C2Tx (b), GO/Ti3C2Tx (c), and RGO/Ti3C2Tx (d). Element area profile and linear scanning of RGO/Ti3C2Tx (e,f).CC BY · PubMed Central

Figure 3 TEM image of Ti3C2Tx (a), RGO (b), and RGO/Ti3C2Tx (c).CC BY · PubMed Central

Figure 4 The survey spectrum (a) and high-resolution XPS spectra of the C1s (b), Ti2p (c), and O1s (d) peaks of the RGO/Ti3C2 nanocomposite.CC BY · PubMed Central

Figure 5 Charge–discharge profiles of (a) Ti3C2Tx and (b) the RGO/Ti3C2Tx nanocomposite electrode at different cycles with a current density of 50 mA/g.CC BY · PubMed Central

Figure 6 Rate performance of Ti3C2Tx and the RGO/Ti3C2Tx nanocomposite at different current densities.CC BY · PubMed Central

Figure 7 Cycling performance of (a) Ti3C2Tx and (b) the RGO/Ti3C2Tx nanocomposite at a current density of 500 mA/g.CC BY · PubMed Central

Figure 8 Cyclic voltammetry (CV) curves of the RGO/Ti3C2Tx nanocomposite from 3.0 to 0.01 V at a scan rate of 0.2 mV/s.CC BY · PubMed Central

Figure 9 Electrochemical impedance spectroscopy (EIS) plots of the Ti3C2Tx and RGO/Ti3C2Tx.CC BY · PubMed Central

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“As a result, a large number of hydrogen bonds between the surface of modified CC and MXene make them tightly combine together and thus increase the stability of CMCM electrodes.(29) CV curves of CC, OPMCC, and CMCC in the sulfuric acid electrolyte are shown in Figure S1.”
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“These peaks are attributed to the presence of oxygen-containing functional groups on the RGO in the In2O3/RGO NCs, as reported in previous studies [46,47].”
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Authors: Shen, C., Wang, L., Zhou, A., Wang, B., Wang, X., Lian, W., Hu, Q., Qin, G., & Liu, X.
Affiliations: Henan Polytechnic University (CN)
Chinese Academy of Sciences (CN)
University of Manchester (GB)
Corresponding author: Wang, Libo
ORCID: Wang, Libo
Zhou, Aiguo
Wang, Bo
Hu, Qianku
Qin, Gang
Liu, Xuqing
Venue: Nanomaterials
Publisher: MDPI AG
Published: 2018-01-31
Volume: 8
Issue: 2
Pages: 80
ISSN: 2079-4991 (ISSN-L)
DOI: 10.3390/nano8020080
PMC: PMC5853712
OpenAlex: W2785719750
Cited by: 152
References: 56
Citations by year: 2026: 15 · 2025: 9 · 2024: 19 · 2023: 35 · 2022: 25 · 2021: 12 · 2020: 21 · 2019: 15 · 2018: 1
FWCI: 4.57
Type: journal article
Language: en
Open access: gold
doi.org
Licence: cc-by
creativecommons.org/licenses/by/4.0/ (vor)
Locations: Nanomaterials (publishedVersion, cc-by)
Europe PMC (PubMed Central) (publishedVersion, cc-by)
PubMed Central (publishedVersion, cc-by)
PubMed (publishedVersion)
DOAJ (DOAJ: Directory of Open Access Journals) (submittedVersion, cc-by-sa)
Research Explorer (The University of Manchester) (submittedVersion, cc-by)
Funders: National Natural Science Foundation of China (51403056, 51472075, 134100510008, 51772077, T2013-4)
Henan Polytechnic University (T2013‐4)
Henan Province Science and Technology Innovation Talent Program
Topics: Physical Sciences › Materials Science › Materials Chemistry › MXene and MAX Phase Materials
Physical Sciences › Engineering › Electrical and Electronic Engineering › Advancements in Battery Materials
Physical Sciences › Materials Science › Electronic, Optical and Magnetic Materials › Supercapacitor Materials and Fabrication
Keywords: MXene, Ti3C2Tx, reduced graphene oxide, lithium-ion battery anodes, electrochemical performance, rate capability, reversible capacity, two-dimensional layered materials

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Synthesis and Electrochemical Properties of Two-Dimensional RGO/Ti3C2Tx Nanocomposites

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