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Cationic Ring-Opening Polymerization(CROP) major mechanistic phenomena
Abstract
Lipase-catalyzed ring-opening polymerization of 10-fluorodecan-9-olide (1a), 11-fluoroundecan-10-olide (1b), 12-fluorododecan-11-olide (1c) and 14-fluorotetradecan-13-olide (1d) gave optically active products with Mw of 3.000 to 8.000, while 10-fluoroundecan-11-olide (3a) gave an optically inactive polymer with Mw = 11.000. On the other hand, Candida antarctica lipase-catalyzed polymerization of 10- to 14-membered ω-fluoro-(ω-1)-hydroxyalcanoic acids gave optically inactive oligomers with Mw of 3.000 to 11.000 in the presence of molecular sieves, while reactions without molecular sieves gave oligomers with lower molecular weight, but with small optical rotations. 9-Fluoro-10-hydroxydecanoic acid, on the other hand, gave an optically inactive polyester with Mw = 7400. © 2000 John Wiley & Sons, Inc. J Polym Sci A: Polym Chem 38: 2004–2012, 2000
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“Finally, from even more detailed studies it was found that ring-expansion is favored at low monomer concentrations and the open chain mechanism dominates the propagation at higher monomer concentration [45] (see also [5]).”
From Ring-Opening Polymerization—An Introductory Review (2013) · cites this paper as [45]
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Metadata
- Authors
- Penczek, S.
- Venue
- Journal of Polymer Science Part A: Polymer Chemistry
- Published
- 2000
- References
- 10
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