Cited by 530CO2 Reduction Techniques and CatalystsElectrocatalysts for Energy ConversionCatalysts for Methane Reforming

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Selective and Efficient Reduction of Carbon Dioxide to Carbon Monoxide on Oxide‐Derived Nanostructured Silver Electrocatalysts

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Ma, Ming, Trześniewski, Bartek J., Xie, Jie, Smith, Wilson A.·2016·Angewandte Chemie International Edition

DOI 10.1002/anie.201604654

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Abstract

In this work, the selective electrocatalytic reduction of carbon dioxide to carbon monoxide on oxide‐derived silver electrocatalysts is presented. By a simple synthesis technique, the overall high faradaic efficiency for CO production on the oxide‐derived Ag was shifted by more than 400 mV towards a lower overpotential compared to that of untreated Ag. Notably, the Ag resulting from Ag oxide is capable of electrochemically reducing CO 2 to CO with approximately 80 % catalytic selectivity at a moderate overpotential of 0.49 V, which is much higher than that (ca. 4 %) of untreated Ag under identical conditions. Electrokinetic studies show that the improved catalytic activity is ascribed to the enhanced stabilization of COOH . intermediate. Furthermore, highly nanostructured Ag is likely able to create a high local pH near the catalyst surface, which may also facilitate the catalytic activity for the reduction of CO 2 with suppressed H 2 evolution.

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Authors: Ma, M., Trześniewski, B. J., Xie, J., & Smith, W. A.
Affiliations: China University of Petroleum, East China (CN)
Delft University of Technology (NL)
Eindhoven University of Technology (NL)
Corresponding author: Smith, Wilson A.
ORCID: Ma, Ming
Trześniewski, Bartek J.
Xie, Jie
Smith, Wilson A.
Venue: Angewandte Chemie International Edition
Publisher: Wiley
Published: 2016-07-05
Volume: 55
Issue: 33
Pages: 9748-9752
ISSN: 1433-7851 (ISSN-L)
1521-3773
DOI: 10.1002/anie.201604654
OpenAlex: W2470317005
Cited by: 530
References: 43
Citations by year: 2026: 17 · 2025: 34 · 2024: 49 · 2023: 50 · 2022: 43 · 2021: 72 · 2020: 81 · 2019: 78 · 2018: 62 · 2017: 38 · 2016: 6
FWCI: 16.65
Type: journal article
Language: en
Open access: green
research.tue.nl
Licence: other-oa
onlinelibrary.wiley.com/termsAndConditions#vor (vor)
Locations: Angewandte Chemie International Edition (publishedVersion)
PubMed (publishedVersion)
TU/e Research Portal (publishedVersion, other-oa)
TU/e Research Portal (submittedVersion)
TU/e Research Portal (submittedVersion, other-oa)
Funders: CSC
NWO VENI
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › CO2 Reduction Techniques and Catalysts
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Chemical Engineering › Catalysis › Catalysts for Methane Reforming
Keywords: electrochemical CO2 reduction, carbon monoxide production, silver electrocatalyst, silver nanostructures, COOH intermediate, Faradaic efficiency, overpotential, local pH, hydrogen evolution suppression, CO selectivity

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Selective and Efficient Reduction of Carbon Dioxide to Carbon Monoxide on Oxide‐Derived Nanostructured Silver Electrocatalysts

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