2-Steps KOH activation of rice straw: An efficient method for preparing high-performance activated carbons
Abstract
Effects of both pre-treatment and number of steps in KOH activation of raw rice straw (RS) on textural and adsorption properties of RS-derived activated carbons (ACs) were investigated. Three pre-treatment protocols were tested: mechanical, chemical by NaOH pulping, and a combination of both. Activation of RS-based materials was investigated, at a constant temperature of 800 degrees C, according to two ways: a 1-step simultaneous carbonisation-activation with KOH, and a 2-steps process: carbonisation followed by activation by KOH. 2-Steps KOH activation was more efficient in producing activated carbons with high surface areas and high methylene blue adsorption than 1-step KOH activation. Additionally, 2-steps KOH activation increased the yield of activated carbons having moderate ash content (8-14%). Surface areas as high as 1917 m(2)/g were obtained when the combined mechanical-chemical pre-treatment method and a 2-steps activation process were carried out.
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The sample prepared with KOH/precursor = 2 showed higher CO2 capacity than the sample prepared with KOH/precursor = 4.
“According to textural properties, the sample prepared with KOH/precursor = 4 represented the larger pore size and the surface area; however, the sample prepared with KOH/precursor = 2 showed higher CO 2 capacity.”
From Biomass/Biochar carbon materials for CO2 capture and sequestration by cyclic adsorption processes: A review and prospects for future directions (2022) · cites this paper as [242]
The sample activated at 600 °C using KOH/precursor = 2 had the maximum CO2 uptake of 4.8 mmol/g at 25 °C and 1 atm.
“In this way, the sample activated at 600 ᵒC using KOH/precursor = 2 had the maximum CO 2 uptake of 4.8 mmol.g -1 at 25 ᵒC and 1 atm.”
From Biomass/Biochar carbon materials for CO2 capture and sequestration by cyclic adsorption processes: A review and prospects for future directions (2022) · cites this paper as [242]
The sample prepared with KOH/precursor = 4 had larger pore size and surface area than the sample prepared with KOH/precursor = 2.
“According to textural properties, the sample prepared with KOH/precursor = 4 represented the larger pore size and the surface area; however, the sample prepared with KOH/precursor = 2 showed higher CO 2 capacity.”
From Biomass/Biochar carbon materials for CO2 capture and sequestration by cyclic adsorption processes: A review and prospects for future directions (2022) · cites this paper as [242]
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- Authors
- Basta, A. H., Fierro, V., El-Saied, H., & Celzard, A.
- Affiliations
- National Research Centre (EG)
- Centre National de la Recherche Scientifique (FR)
- Corresponding author
- Fierro, V.
- Venue
- Bioresource Technology
- Publisher
- Elsevier BV
- Published
- 2009-09
- Volume
- 100
- Issue
- 17
- Pages
- 3941-3947
- ISSN
- 0960-8524 (ISSN-L)
- OpenAlex
- W2089556291
- Cited by
- 312
- References
- 27
- Citations by year
- 2026: 11 · 2025: 17 · 2024: 17 · 2023: 17 · 2022: 25 · 2021: 29 · 2020: 27 · 2019: 29 · 2018: 26 · 2017: 16 · 2016: 17 · 2015: 12 · 2014: 18 · 2013: 15 · 2012: 17
- FWCI
- 12.37
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Bioresource Technology (publishedVersion)
- PubMed (publishedVersion)
- Funders
- Conseil Régional de Lorraine
- Topics
- Physical Sciences › Environmental Science › Water Science and Technology › Adsorption and biosorption for pollutant removal
- Physical Sciences › Engineering › Biomedical Engineering › Thermochemical Biomass Conversion Processes
- Physical Sciences › Engineering › Mechanical Engineering › Carbon Dioxide Capture Technologies
- Keywords
- rice straw, KOH activation, two-step activation, activated carbon, biomass pretreatment, mechanical pretreatment, carbonization, surface area, methylene blue adsorption, ash content
- MeSH terms
- Adsorption, Charcoal, Chemistry, Organic, Hydroxides, Kinetics, Lignin, Methylene Blue, Nitrogen, Oryza, Surface Properties, Temperature, Porosity, Potassium Compounds
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