Cited by 814Polymer Surface Interaction Studiesbiodegradable polymer synthesis and propertiesPolymer crystallization and properties

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FTIR study of polycaprolactone chain organization at interfaces

Elzein, Tamara, Nasser-Eddine, Mohamad, Delaite, Christelle, Bistac, Sophie, Dumas, Philippe·2004·Journal of Colloid and Interface Science

DOI 10.1016/j.jcis.2004.02.001

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Abstract

Polycaprolactone (PCL), extensively known as a biomaterial, is the subject of this paper. Knowing well that some biomaterial applications exhibit specific chain organization, we focused our study on the orientation of PCL chains when this polymer is adsorbed (spin-coated) on inert substrates such as gold-coated glass slides. The main technique allowing adsorbed thin films analysis that we chose is polarization-modulation infrared reflection-absorption spectroscopy (PM-IRRAS), which permits qualitative and quantitative determination of chain anisotropy in the confined layers at the interface. Based on our spectroscopic results, we achieved an adsorption model of PCL chains and we calculated orientation angles with respect to the substrate normal. Calculated values show a quasi-perpendicular deposition of PCL chains on the gold substrate. Moreover, PCL thin films remain highly crystalline, a fact which could be the basis of the important anisotropy of PCL chains.

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Authors: Elzein, T., Nasser-Eddine, M., Delaite, C., Bistac, S., & Dumas, P.
Corresponding author: Elzein, Tamara
ORCID: Elzein, Tamara
Delaite, Christelle
Bistac, Sophie
Venue: Journal of Colloid and Interface Science
Publisher: Elsevier BV
Published: 2004-05
Volume: 273
Issue: 2
Pages: 381-387
ISSN: 0021-9797 (ISSN-L)
DOI: 10.1016/j.jcis.2004.02.001
OpenAlex: W2086588103
Cited by: 814
References: 24
Citations by year: 2026: 42 · 2025: 77 · 2024: 56 · 2023: 64 · 2022: 63 · 2021: 61 · 2020: 68 · 2019: 64 · 2018: 72 · 2017: 45 · 2016: 39 · 2015: 34 · 2014: 25 · 2013: 23 · 2012: 15
FWCI: 3.38
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Journal of Colloid and Interface Science (publishedVersion)
PubMed (publishedVersion)
Topics: Physical Sciences › Materials Science › Surfaces, Coatings and Films › Polymer Surface Interaction Studies
Physical Sciences › Materials Science › Biomaterials › biodegradable polymer synthesis and properties
Physical Sciences › Materials Science › Polymers and Plastics › Polymer crystallization and properties
Keywords: polycaprolactone, polymer chain orientation, interfacial adsorption, polymer thin films, gold substrate, spin-coated films, PM-IRRAS, crystallinity, adsorption modeling, biomaterials

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FTIR study of polycaprolactone chain organization at interfaces

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