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π-Conjugated Nickel Bis(dithiolene) Complex Nanosheet
Abstract
A π-conjugated nanosheet comprising planar nickel bis(dithiolene) complexes was synthesized by a bottom-up method. A liquid-liquid interfacial reaction using benzenehexathiol in the organic phase and nickel(II) acetate in the aqueous phase produced a semiconducting bulk material with a thickness of several micrometers. Powder X-ray diffraction analysis revealed that the crystalline portion of the bulk material comprised a staggered stack of nanosheets. A single-layer nanosheet was successfully realized using a gas-liquid interfacial reaction. Atomic force microscopy and scanning tunneling microscopy confirmed that the π-conjugated nanosheet was single-layered. Modulation of the oxidation state of the nanosheet was possible using chemical redox reactions.
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Metadata
- Authors
- Kambe, T., Sakamoto, R., Hoshiko, K., Takada, K., Miyachi, M., Ryu, J.-H., Sasaki, S., Kim, J., Nakazato, K., Takata, M., & Nishihara, H.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2013-02-05
- Volume
- 135
- Issue
- 7
- Pages
- 2462-2465
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2316777255
- Cited by
- 848
- References
- 24
- FWCI
- 15.54
- Type
- journal article
- Language
- en
- Open access
- closed
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