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Constructing NiCo/Fe3O4 Heteroparticles within MOF-74 for Efficient Oxygen Evolution Reactions
Abstract
Metal–organic frameworks (MOF) have recently emerged as versatile precursors to fabricate functional MOF derivatives for oxygen evolution reactions (OER). Herein, we developed a controlled partial pyrolysis strategy to construct robust NiCo/Fe 3 O 4 heteroparticles within MOF-74 for efficient OER using trimetallic NiCoFe-MOF-74 as precursor. The partial pyrolysis method preserves the framework structure of MOF for effective substrates diffusion while producing highly active nanoparticles. The as-prepared NiCo/Fe 3 O 4 /MOF-74 delivered remarkably stable OER current with an overpotential as low as 238 mV at 10.0 mA cm –2 and an Tafel slop of 29 mV/dec, outperforming those of pristine NiCoFe-MOF-74, totally decomposed MOF derivatives, and most reported non-noble metal based electrocatalysts. The key for the formation of NiCo/Fe 3 O 4 /MOF-74 nanostructures is that the metals can be decomposed from NiCoFe-MOF-74 in the order of Ni, Co, and Fe under controlled heat treatment. Density functional theory calculations reveals that the underlying NiCo promotes the OER activity of Fe 3 O 4 through exchange stabilization of active oxygen species.
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Metadata
- Authors
- Wang, X., Xiao, H., Li, A., Li, Z., Liu, S., Zhang, Q., Gong, Y., Zheng, L., Zhu, Y., Chen, C., Wang, D., Peng, Q., Gu, L., Han, X., Li, J., & Li, Y.
- Venue
- Journal of the American Chemical Society
- Publisher
- American Chemical Society (ACS)
- Published
- 2018-10-23
- Volume
- 140
- Issue
- 45
- Pages
- 15336-15341
- ISSN
- 0002-7863 (ISSN-L)
- 1520-5126
- OpenAlex
- W2898365681
- Cited by
- 422
- References
- 37
- FWCI
- 9.39
- Type
- journal article
- Language
- en
- Open access
- closed
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