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Surface Chemistry of Gold Nanoparticles Produced by Laser Ablation in Aqueous Media
Abstract
The femtosecond laser ablation of a gold target in aqueous solutions has been used to produce colloidal Au nanoparticles with controlled surface chemistry. A detailed chemical analysis showed that the nanoparticles formed were partially oxidized by the oxygen present in solution. The hydroxylation of these Au−O compounds, followed by a proton loss to give surface Au−O -, resulted in the negative charging of the nanoparticles. The partial oxidation of the gold nanoparticle surface enhances its chemical reactivity and consequently has a strong impact on its growth. In particular, the oxidized surface reacted efficiently with Cl - and OH - to augment its net surface charge. This limited the coalescence of the particles, due to electrostatic repulsion, and led to a significant reduction of their size. Taking advantage of the repulsion effect, efficient size control was achieved using different salts (7 ± 5 nm for 10 mM KCl, 5.5 ± 4 nm for 10 mM NaCl, 8 ± 5 nm for NaOH, pH 9.4), a considerable improvement comparatively to particles prepared in deionized water, using identical ablation conditions, where particles of 1−250 nm were produced. The partially oxidized gold surface was also suitable for surface modification through both covalent and electrostatic interactions during particle formation. Using solutions of N -propylamine, we showed an efficient control of nanoparticle size (5−8 ± 4−7 nm) by the involvement of these interactions. The results obtained help to develop methodologies for the control of laser-ablation-based nanoparticle growth and the functionalization of nanoparticle surfaces by specific interactions.
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Metadata
- Authors
- Sylvestre, J.-P., Poulin, S., Kabashin, A. V., Sacher, E., Meunier, M., & Luong, J. H. T.
- Venue
- The Journal of Physical Chemistry B
- Publisher
- American Chemical Society (ACS)
- Published
- 2004-10-01
- Volume
- 108
- Issue
- 43
- Pages
- 16864-16869
- ISSN
- 1520-5207 (ISSN-L)
- 1520-6106
- OpenAlex
- W2004664887
- Cited by
- 732
- References
- 6
- FWCI
- 8.58
- Type
- journal article
- Language
- en
- Open access
- closed
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