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Oxygen Tolerance Study of Photoinduced Electron Transfer–Reversible Addition–Fragmentation Chain Transfer (PET-RAFT) Polymerization Mediated by Ru(bpy)3Cl2

Xu, Jiangtao, Jung, Kenward, Boyer, Cyrille·2014·Macromolecules

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Abstract

This study reports a highly efficient photoredox catalyst, Ru(bpy) 3 Cl 2, capable of controlling the polymerization of methacrylates, acrylates, and acrylamides in the presence of thiocarbonylthio compounds via a photoinduced electron transfer–reversible addition–fragmentation chain (PET-RAFT) process. This polymerization technique was performed in a closed vessel in the presence or absence of air. Online Fourier transform near-infrared spectroscopy (FTNIR) was employed to monitor the monomer conversions of methyl methacrylate, methyl acrylate, and N,N ′-dimethylacrylamide in the presence or absence of air. Interestingly, after an induction period, the polymerization proceeded in the presence of air to yield well-defined polymers (PDI < 1.20). The polymers were characterized by 1 H NMR, UV–vis spectroscopy, and gel permeation chromatography. Excellent end-group retention was also demonstrated by NMR, UV–vis, and successive chain extensions of the resulting homopolymers to yield diblock and multiblock copolymers (decablock copolymers).

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See all 304

Authors: Xu, J., Jung, K., & Boyer, C.
Venue: Macromolecules
Publisher: American Chemical Society (ACS)
Published: 2014-06-20
Volume: 47
Issue: 13
Pages: 4217-4229
ISSN: 0024-9297 (ISSN-L)
1520-5835
DOI: 10.1021/ma500883y
OpenAlex: W2313595743
Cited by: 304
References: 80
FWCI: 14.74
Type: journal article
Language: en
Open access: closed

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Oxygen Tolerance Study of Photoinduced Electron Transfer–Reversible Addition–Fragmentation Chain Transfer (PET-RAFT) Polymerization Mediated by Ru(bpy)3Cl2

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