Nanoporous Materials from Block Copolymer Precursors

A new family of mesoporous molecular sieves prepared with liquid crystal templates

Beck, J. S., Vartuli, J. C., Roth, W. J., Leonowicz, M. E., Kresge, C. T., Schmitt, K. D., Chu, C. T. W., Olson, D. H., Sheppard, E. W., McCullen, S. B., et al. (1992) · Journal of the American Chemical Society · doi:10.1021/ja00053a020 · Cited by 10,967

Block Copolymer Thermodynamics: Theory and Experiment

Bates, F. S., & Fredrickson, G. H. (1990) · Annual Review of Physical Chemistry · doi:10.1146/annurev.pc.41.100190.002521 · Cited by 3,960

Block Copolymers—Designer Soft Materials

Bates, F. S., & Fredrickson, G. H. (1999) · Physics Today · doi:10.1063/1.882522 · Cited by 3,219

Ultrahigh-Density Nanowire Arrays Grown in Self-Assembled Diblock Copolymer Templates

Thurn-Albrecht, T., Schotter, J., Kästle, G. A., Emley, N., Shibauchi, T., Krusin-Elbaum, L., Guarini, K., Black, C. T., Tuominen, M. T., & Russell, T. P. (2000) · Science · doi:10.1126/science.290.5499.2126 · Cited by 2,104

The Physics of Block Copolymers

Hamley, I. W. (1998) · doi:10.1093/oso/9780198502180.001.0001 · Cited by 1,913

Block Copolymer Lithography: Periodic Arrays of ~10 11 Holes in 1 Square Centimeter

Park, M., Harrison, C., Chaikin, P. M., Register, R. A., & Adamson, D. H. (1997) · Science · doi:10.1126/science.276.5317.1401 · Cited by 1,866

Unifying Weak- and Strong-Segregation Block Copolymer Theories

Matsen, M. W., & Bates, F. S. (1996) · Macromolecules · doi:10.1021/ma951138i · Cited by 1,839

The physics of block copolymers

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Enabling nanotechnology with self assembled block copolymer patterns

Park, C., Yoon, J., & Thomas, E. L. (2003) · Polymer · doi:10.1016/j.polymer.2003.08.011 · Cited by 1,473

Controlling polymer-surface interactions with random copolymer brushes

Mansky, P., Liu, Y., Huang, E., Russell, T. P., & Hawker, C. (1997) · Science · doi:10.1126/science.275.5305.1458 · Cited by 1,291

Highly Oriented and Ordered Arrays from Block Copolymers via Solvent Evaporation

Kim, S. H., Misner, M. J., Xu, T., Kimura, M., & Russell, T. P. (2004) · Advanced Materials · doi:10.1002/adma.200304906 · Cited by 922

Supramolecular Structures from Rod−Coil Block Copolymers

Lee, M., Cho, B.-K., & Zin, W.-C. (2001) · Chemical Reviews · doi:10.1021/cr0001131 · Cited by 758

Local Control of Microdomain Orientation in Diblock Copolymer Thin Films with Electric Fields

Morkved, T. L., Lu, M., Urbas, A. M., Ehrichs, E. E., Jaeger, H. M., Mansky, P., & Russell, T. P. (1996) · Science · doi:10.1126/science.273.5277.931 · Cited by 758

Nanoscopic Templates from Oriented Block Copolymer Films

Thurn-Albrecht, T., Steiner, R., DeRouchey, J., Stafford, C. M., Huang, E., Bal, M., Tuominen, M., Hawker, C. J., & Russell, T. P. (2000) · Advanced Materials · doi:10.1002/(sici)1521-4095(200006)12:11<787::aid-adma787>3.0.co;2-1 · Cited by 646

Complex Optical Surfaces Formed by Replica Molding Against Elastomeric Masters

Xia, Y., Kim, E., Zhao, X.-M., Rogers, J. A., Prentiss, M., & Whitesides, G. M. (1996) · Science · doi:10.1126/science.273.5273.347 · Cited by 643

Block copolymers: synthetic strategies, physical properties, and applications

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Block Copolymers: Past Successes and Future Challenges

Lodge, T. P. (2003) · Macromolecular Chemistry and Physics · doi:10.1002/macp.200290073 · Cited by 567

Ordered Nanoporous Polymers from Polystyrene−Polylactide Block Copolymers

Zalusky, A. S., Olayo-Valles, R., Wolf, J. H., & Hillmyer, M. A. (2002) · Journal of the American Chemical Society · doi:10.1021/ja0278584 · Cited by 553

Integration of self-assembled diblock copolymers for semiconductor capacitor fabrication

Black, C. T., Guarini, K. W., Milkove, K. R., Baker, S. M., Russell, T. P., & Tuominen, M. T. (2001) · Applied Physics Letters · doi:10.1063/1.1383805 · Cited by 351

Ordered Bicontinuous Nanoporous and Nanorelief Ceramic Films from Self Assembling Polymer Precursors

Chan, V. Z.-H., Hoffman, J., Lee, V. Y., Iatrou, H., Avgeropoulos, A., Hadjichristidis, N., Miller, R. D., & Thomas, E. L. (1999) · Science · doi:10.1126/science.286.5445.1716 · Cited by 346

Chemical Approaches to Three-Dimensional Semiconductor Photonic Crystals

Norris, D. J., & Vlasov, Y. A. (2001) · Advanced Materials · doi:10.1002/1521-4095(200103)13:6<371::aid-adma371>3.0.co;2-k · Cited by 346

Bicontinuous Cubic Block Copolymer Photonic Crystals

Urbas, A. M., Maldovan, M., DeRege, P., & Thomas, E. L. (2002) · Advanced Materials · doi:10.1002/adma.200290018 · Cited by 340

Ordered Reactive Nanomembranes/Nanotemplates from Thin Films of Block Copolymer Supramolecular Assembly

Sidorenko, A., Tokarev, I., Minko, S., & Stamm, M. (2003) · Journal of the American Chemical Society · doi:10.1021/ja036085w · Cited by 302

Surface Film Formation on a Graphite Negative Electrode in Lithium-Ion Batteries: Atomic Force Microscopy Study on the Effects of Film-Forming Additives in Propylene Carbonate Solutions

Jeong, S.-K., Inaba, M., Mogi, R., Iriyama, Y., Abe, T., & Ogumi, Z. (2001) · Langmuir · doi:10.1021/la015553h · Cited by 288

2.5-inch disk patterned media prepared by an artificially assisted self-assembling method

Naito, K., Hieda, H., Sakurai, M., Kamata, Y., & Asakawa, K. (2002) · IEEE Transactions on Magnetics · doi:10.1109/tmag.2002.802847 · Cited by 278

Solvent‐Induced Ordering in Thin Film Diblock Copolymer/Homopolymer Mixtures

Kim, S. H., Misner, M. J., & Russell, T. P. (2004) · Advanced Materials · doi:10.1002/adma.200306577 · Cited by 245

A Noncubic Triply Periodic Network Morphology in Poly(isoprene-b-styrene-b-ethylene oxide) Triblock Copolymers

Bailey, T. S., Hardy, C. M., Epps, T. H., & Bates, F. S. (2002) · Macromolecules · doi:10.1021/ma011716x · Cited by 244

Polymorph Selectivity under Nanoscopic Confinement

Ha, J.-M., Wolf, J. H., Hillmyer, M. A., & Ward, M. D. (2004) · Journal of the American Chemical Society · doi:10.1021/ja049724r · Cited by 244

A Simple Route to Metal Nanodots and Nanoporous Metal Films

Shin, K., Leach, K. A., Goldbach, J. T., Kim, D. H., Jho, J. Y., Tuominen, M., Hawker, C. J., & Russell, T. P. (2002) · Nano Letters · doi:10.1021/nl0256560 · Cited by 242

Ordered Network Phases in Linear Poly(isoprene-b-styrene-b-ethylene oxide) Triblock Copolymers

Epps, T. H., Cochran, E. W., Bailey, T. S., Waletzko, R. S., Hardy, C. M., & Bates, F. S. (2004) · Macromolecules · doi:10.1021/ma048762s · Cited by 225

Monolayer films of diblock copolymer microdomains for nanolithographic applications

Mansky, P., haikin, P., & Thomas, E. L. (1995) · Journal of Materials Science · doi:10.1007/bf00353023 · Cited by 214

Monolithic Catalysts for the Chemical Industry

Boger, T., Heibel, A. K., & Sorensen, C. M. (2004) · Industrial & Engineering Chemistry Research · doi:10.1021/ie030730q · Cited by 209

Core−Shell Gyroid Morphology in a Poly(isoprene-block-styrene-block-dimethylsiloxane) Triblock Copolymer

Shefelbine, T. A., Vigild, M. E., Matsen, M. W., Hajduk, D. A., Hillmyer, M. A., Cussler, E. L., & Bates, F. S. (1999) · Journal of the American Chemical Society · doi:10.1021/ja991442h · Cited by 207

Nanoprocessing Based on Bicontinuous Microdomains of Block Copolymers: Nanochannels Coated with Metals

Hashimoto, T., Tsutsumi, K., & Funaki, Y. (1997) · Langmuir · doi:10.1021/la970967p · Cited by 204

Mesoporous Polystyrene Monoliths

Zalusky, A. S., Olayo-Valles, R., Taylor, C. J., & Hillmyer, M. A. (2001) · Journal of the American Chemical Society · doi:10.1021/ja003936g · Cited by 204

Photonic properties of bicontinuous cubic microphases

Maldovan, M., Urbas, A. M., Yufa, N., Carter, W. C., & Thomas, E. L. (2002) · Physical Review B · doi:10.1103/physrevb.65.165123 · Cited by 203

Nanolithographic templates from diblock copolymer thin films

Mansky, P., Harrison, C. K., Chaikin, P. M., Register, R. A., & Yao, N. (1996) · Applied Physics Letters · doi:10.1063/1.116192 · Cited by 200

New ordered morphologies in ABC triblock copolymers

Auschra, C., & Stadler, R. (1993) · Macromolecules · doi:10.1021/ma00061a005 · Cited by 194

Optimization of Diblock Copolymer Thin Film Self Assembly

Guarini, K. W., Black, C. T., & Yeung, S. H. I. (2002) · Advanced Materials · Cited by 178

Three-Dimensionally Packed Nanohelical Phase in Chiral Block Copolymers

Ho, R.-M., Chiang, Y.-W., Tsai, C.-C., Lin, C.-C., Ko, B.-T., & Huang, B.-H. (2004) · Journal of the American Chemical Society · doi:10.1021/ja039627i · Cited by 178

Nanoscale patterning using self-assembled polymers for semiconductor applications

Guarini, K. W., Black, C. T., Milkove, K. R., & Sandstrom, R. L. (2001) · Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures Processing, Measurement, and Phenomena · doi:10.1116/1.1421551 · Cited by 175

Block Copolymer Surface Reconstuction: A Reversible Route to Nanoporous Films

Xu, T., Stevens, J., Villa, J. A., Goldbach, J. T., Guarini, K. W., Black, C. T., Hawker, C. J., & Russell, T. P. (2003) · Advanced Functional Materials · doi:10.1002/adfm.200304374 · Cited by 175

Large area dense nanoscale patterning of arbitrary surfaces

Park, M., Chaikin, P. M., Register, R. A., & Adamson, D. H. (2001) · Applied Physics Letters · doi:10.1063/1.1378046 · Cited by 172

Polymerization of monomers containing functional silyl groups. 5. Synthesis of new porous membranes with functional groups

Lee, J. S., Hirao, A., & Nakahama, S. (1988) · Macromolecules · doi:10.1021/ma00179a057 · Cited by 168

Combinations of Microphase Separation and Terminal Multiple Hydrogen Bonding in Novel Macromolecules

Yamauchi, K., Lizotte, J. R., Hercules, D. M., Vergne, M. J., & Long, T. E. (2002) · Journal of the American Chemical Society · doi:10.1021/ja020123e · Cited by 158

Network Phases in ABC Triblock Copolymers

Epps, T. H. I., Cochran, E. W., Hardy, C. M., Bailey, T. S., Waletzko, R. S., & Bates, F. S. (2004) · Macromolecules · doi:10.1021/ma0493426 · Cited by 152

A Polystyrene−Oligothiophene−Polystyrene Triblock Copolymer

Hempenius, M. A., Langeveld-Voss, B. M. W., van Haare, J. A. E. H., Janssen, R. A. J., Sheiko, S. S., Spatz, J. P., Möller, M., & Meijer, E. W. (1998) · Journal of the American Chemical Society · doi:10.1021/ja972910v · Cited by 151

Nanoporous Polystyrene Containing Hydrophilic Pores from an ABC Triblock Copolymer Precursor

Rzayev, J., & Hillmyer, M. A. (2004) · Macromolecules · doi:10.1021/ma047870b · Cited by 149

Directed Deposition of Nanoparticles Using Diblock Copolymer Templates

Misner, M. J., Skaff, H., Emrick, T. S., & Russell, T. P. (2003) · Advanced Materials · doi:10.1002/adma.200390050 · Cited by 149

Monolithic Mesophase Silica with Large Ordering Domains

Melosh, N. A., Davidson, P., & Chmelka, B. F. (2000) · Journal of the American Chemical Society · doi:10.1021/ja992801b · Cited by 148

“Hairy Tubes”: Mesoporous Materials Containing Hollow Self-Organized Cylinders with Polymer Brushes at the Walls

Mäki-Ontto, R., de Moel, K., Odorico, W. D., Ruokolainen, J., Stamm, M., ten Brinke, G., & Ikkala, O. T. (2001) · Advanced Materials · Cited by 145

Lithography with a mask of block copolymer microstructures

Harrison, C. K., Park, M. S., Chaikin, P. M., Register, R. A., & Adamson, D. H. (1998) · Journal of Vacuum Science & Technology B Microelectronics and Nanometer Structures Processing Measurement and Phenomena · doi:10.1116/1.589860 · Cited by 143

Process integration of self-assembled polymer templates into silicon nanofabrication

Guarini, K. W., Black, C. T., Zhang, Y., Kim, H., Sikorski, E., & Babich, I. V. (2002) · Journal of Vacuum Science & Technology B Microelectronics and Nanometer Structures Processing Measurement and Phenomena · doi:10.1116/1.1521730 · Cited by 140

Fabrication of Quantum Dot/Polymer Composites: Phosphine-Functionalized Block Copolymers as Passivating Hosts for Cadmium Selenide Nanoclusters

Fogg, D. E., Radzilowski, L. H., Blanski, R. L., Schrock, R. R., & Thomas, E. L. (1997) · Macromolecules · doi:10.1021/ma961103y · Cited by 136

Fabrication and Characterization of Nanoelectrode Arrays Formed via Block Copolymer Self-Assembly

Jeoung, E., Galow, T. H., Schotter, J., Bal, M., Ursache, A., Tuominen, M. T., Stafford, C. M., Russell, T. P., & Rotello, V. M. (2001) · Langmuir · doi:10.1021/la010531g · Cited by 135

Thin Films with Densely, Regularly Packed Nanochannels: Preparation, Characterization, and Applications

Liu, G., Ding, J., Hashimoto, T., Kimishima, K., Winnik, F. M., & Nigam, S. (1999) · Chemistry of Materials · doi:10.1021/cm990184k · Cited by 133

Nanoporous Materials with Spherical and Gyroid Cavities Created by Quantitative Etching of Polydimethylsiloxane in Polystyrene−Polydimethylsiloxane Block Copolymers

Ndoni, S., Vigild, M. E., & Berg, R. H. (2003) · Journal of the American Chemical Society · doi:10.1021/ja0360034 · Cited by 126

Tunable Nanocellular Polymeric Monoliths Using Fluorinated Block Copolymer Templates and Supercritical Carbon Dioxide

Yokoyama, B. H., Li, J., Nemoto, T., & Sugiyama, K. (2004) · Advanced Materials · doi:10.1002/adma.200400072 · Cited by 125

Palladium Nanoparticle Catalyst Prepared in Poly(Acrylic Acid)-lined Channels of Diblock Copolymer Microspheres

Lu, Z., Liu, G., Phillips, H., Hill, J. M., Chang, J. J. S., & Kydd, R. A. (2001) · Nano Letters · doi:10.1021/nl015597a · Cited by 107

Synthesis and Characterization of Model Polyisoprene−Polylactide Diblock Copolymers

Schmidt, S. C., & Hillmyer, M. A. (1999) · Macromolecules · doi:10.1021/ma9900277 · Cited by 106

Spatially Controlled Fabrication of Nanoporous Block Copolymers

Li, M., Douki, K., Goto, K., Li, X., Coenjarts, C. A., Smilgies, D., & Ober, C. K. (2004) · Chemistry of Materials · doi:10.1021/cm0493445 · Cited by 98

Fluorescent Beads Coated with Polyaniline: A Novel Nanomaterial for Optical Sensing of pH

Pringsheim, E., Zimin, D., & Wolfbeis, O. S. (2001) · Advanced Materials · doi:10.1002/1521-4095(200106)13:11<795::aid-adma795>3.0.co;2-1 · Cited by 92

Volume Contractions Induced by Crosslinking: A Novel Route to Nanoporous Polymer Films

Jeong, U., Ryu, D. Y., Kim, J. K., et al. (2003) · Advanced Materials · doi:10.1002/adma.200304401 · Cited by 90

Potential Skin Layers for Membranes with Tunable Nanochannels

Liu, G., Ding, J., Guo, A., Herfort, M. H., & Bazett‐Jones, D. P. (1997) · Macromolecules · doi:10.1021/ma961530b · Cited by 89

Precise Control of Nanopore Size in Thin Film Using Mixtures of Asymmetric Block Copolymer and Homopolymer

Jeong, U., Ryu, D. Y., Kim, J. K., et al. (2003) · Macromolecules · doi:10.1021/ma034976i · Cited by 89

Nanopatterning with Microdomains of Block Copolymers using Reactive-Ion Etching Selectivity

Asakawa, K., & Hiraoka, T. (2002) · Japanese Journal of Applied Physics · doi:10.1143/jjap.41.6112 · Cited by 88

Synthesis and Thin Film Characterization of Poly(styrene-block-methyl methacrylate) Containing an Anthracene Dimer Photocleavable Junction Point

Goldbach, J. T., Russell, T. P., & Penelle, J. (2002) · Macromolecules · doi:10.1021/ma011940m · Cited by 85

Large area nanolithographic templates by selective etching of chemically stained block copolymer thin films

Olayo‐Valles, R., Lund, M. S., Leighton, C., & Hillmyer, M. A. (2004) · Journal of Materials Chemistry · doi:10.1039/b408639b · Cited by 85

Smart materials based on self‐assembled hydrogen‐bonded comb‐shaped supramolecules

ten Brinke, G., & Ikkala, O. T. (2004) · The Chemical Record · doi:10.1002/tcr.20018 · Cited by 75

Core−Shell Cylinders and Core−Shell Gyroid Morphologies via Blending of Lamellar ABC Triblock and BC Diblock Copolymers

Goldacker, T., & Abetz, V. (1999) · Macromolecules · doi:10.1021/ma990277n · Cited by 74

Core−Shell Double Gyroid Morphologies in ABC Triblock Copolymers with Different Chain Topologies

Hückstädt, H., Goldacker, T., Göpfert, A., et al. (2000) · Macromolecules · doi:10.1021/ma9921551 · Cited by 71

Nano-Patterning for Patterned Media using Block-Copolymer.

Asakawa, K., Hiraoka, T., Hieda, H., Sakurai, M., Kamata, Y., & Naito, K. (2002) · Journal of Photopolymer Science and Technology · doi:10.2494/photopolymer.15.465 · Cited by 69

Template Syntheses of Polypyrrole Nanowires and CdS Nanoparticles in Porous Polymer Monoliths

Johnson, B. J. S., Wolf, J. H., Zalusky, A. S., & Hillmyer, M. A. (2004) · Chemistry of Materials · doi:10.1021/cm0350075 · Cited by 67

Thermotropic Properties of Organic Nanocrystals Embedded in Ultrasmall Crystallization Chambers

Ha, J., Hillmyer, M. A., & Ward, M. D. (2005) · The Journal of Physical Chemistry B · doi:10.1021/jp045488v · Cited by 64

Block copolymer synthesis

Hillmyer, M. A. (1999) · Current Opinion in Solid State and Materials Science · doi:10.1016/s1359-0286(00)00006-1 · Cited by 63

Nanofabrication of integrated magnetoelectronic devices using patterned self-assembled copolymer templates

Bal, M., Ursache, A., Tuominen, M. T., Goldbach, J. T., & Russell, T. P. (2002) · Applied Physics Letters · doi:10.1063/1.1517400 · Cited by 63

Anionic living polymerization of monomers with functional silyl groups

Hirao, A., & Nakahama, S. (1992) · Progress in Polymer Science · doi:10.1016/0079-6700(92)90018-t · Cited by 63

Synthesis and Morphological Behavior of Silicon-Containing Triblock Copolymers for Nanostructure Applications

Avgeropoulos, A., Chan, V. Z.-H., Lee, V. Y., Ngo, D., Miller, R. D., Hadjichristidis, N., & Thomas, E. L. (1998) · Chemistry of Materials · doi:10.1021/cm970682y · Cited by 60

An Ordered Nanoporous Monolith from an Elastomeric Crosslinked Block Copolymer Precursor

Cavicchi, K. A., Zalusky, A. S., Hillmyer, M. A., & Lodge, T. P. (2004) · Macromolecular Rapid Communications · doi:10.1002/marc.200300245 · Cited by 59

On the Replication of Block Copolymer Templates by Poly(dimethylsiloxane) Elastomers

Kim, D. H., Lin, Z., Kim, H.-C., Jeong, U., & Russell, T. P. (2003) · Advanced Materials · doi:10.1002/adma.200304581 · Cited by 58

Amphiphiles Coordinated to Block Copolymers as a Template for Mesoporous Materials

Valkama, S., Ruotsalainen, T., Kosonen, H., Ruokolainen, J., Torkkeli, M., Serimaa, R. E., ten Brinke, G., & Ikkala, O. T. (2003) · Macromolecules · doi:10.1021/ma020538k · Cited by 57

Ordered Nanoporous Poly(cyclohexylethylene)

Wolf, J. H., & Hillmyer, M. A. (2003) · Langmuir · doi:10.1021/la0341862 · Cited by 54

Nano- to Macro-Sized Heterogeneities Using Cleavable Diblock Copolymers

Goldbach, J. T., Lavery, K. A., Penelle, J., & Russell, T. P. (2004) · Macromolecules · doi:10.1021/ma0489117 · Cited by 48

Control of pore hydrophilicity in ordered nanoporous polystyrene using an AB/AC block copolymer blending strategy

Mao, H., Arrechea, P. L., Bailey, T. S., Johnson, B. J. S., & Hillmyer, M. A. (2004) · Faraday Discussions · doi:10.1039/b403217a · Cited by 47

Polysulfone-graft-poly(tert-butyl acrylate): Synthesis, Nanophase Separation, Poly(tert-butyl acrylate) Hydrolysis, and pH-Dependent Iridescence

Lu, Z., Liu, G., & Duncan, S. (2003) · Macromolecules · doi:10.1021/ma034980u · Cited by 33

Supramolecular Crystalline Sheets with Ordered Nanopore Arrays from Self‐Assembly of Rigid‐Rod Building Blocks

Lee, M., Park, M., Oh, N., Zin, W., Jung, H., & Yoon, D. K. (2004) · Angewandte Chemie International Edition · doi:10.1002/anie.200460378 · Cited by 24

Nanoscopically Engineered Polyimides

Hedrick, J. L., Labadie, J. W., Volksen, W., et al. (2007) · Springer eBooks · doi:10.1007/3-540-49196-1_2 · Cited by 22

Directing the self-assembly of block copolymers

Darling, S. B. (2007) · Progress in Polymer Science · doi:10.1016/j.progpolymsci.2007.05.004 · Cited by 1,019

Nanoporous Membranes Derived from Block Copolymers: From Drug Delivery to Water Filtration

Jackson, E. A., & Hillmyer, M. A. (2010) · ACS Nano · doi:10.1021/nn1014006 · Cited by 623

Polarity-switching top coats enable orientation of sub-10-nm block copolymer domains

Bates, C. M., Seshimo, T., Maher, M. J., Durand, W. J., Cushen, J. D., Dean, L. M., Blachut, G., Ellison, C. J., & Willson, C. G. (2012) · Science · doi:10.1126/science.1226046 · Cited by 385

Nano-in-Nano Approach for Enzyme Immobilization Based on Block Copolymers

Auriemma, F., De Rosa, C., Malafronte, A., Di Girolamo, R., Santillo, C., Gerelli, Y., Fragneto, G., Barker, R., Pavone, V., Maglio, O., et al. (2017) · ACS Applied Materials & Interfaces · doi:10.1021/acsami.7b08959 · Cited by 29