Solidification of floating organic droplet in dispersive liquid-liquid microextraction as a green analytical tool

Mansour, Fotouh R.; Danielson, Neil D.

doi:10.1016/j.talanta.2017.03.084

Cited by 178Analytical chemistry methods developmentAnalytical Chemistry and ChromatographyInnovative Microfluidic and Catalytic Techniques Innovation

Solidification of floating organic droplet in dispersive liquid-liquid microextraction as a green analytical tool

Mansour, Fotouh R., Danielson, Neil D.·2017·Talanta

DOI 10.1016/j.talanta.2017.03.084

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Abstract

Dispersive liquid-liquid microextraction (DLLME) is a special type of microextraction in which a mixture of two solvents (an extracting solvent and a disperser) is injected into the sample. The extraction solvent is then dispersed as fine droplets in the cloudy sample through manual or mechanical agitation. Hence, the sample is centrifuged to break the formed emulsion and the extracting solvent is manually separated. The organic solvents commonly used in DLLME are halogenated hydrocarbons that are highly toxic. These solvents are heavier than water, so they sink to the bottom of the centrifugation tube which makes the separation step difficult. By using solvents of low density, the organic extractant floats on the sample surface. If the selected solvent such as undecanol has a freezing point in the range 10-25°C, the floating droplet can be solidified using a simple ice-bath, and then transferred out of the sample matrix; this step is known as solidification of floating organic droplet (SFOD). Coupling DLLME to SFOD combines the advantages of both approaches together. The DLLME-SFOD process is controlled by the same variables of conventional liquid-liquid extraction. The organic solvents used as extractants in DLLME-SFOD must be immiscible with water, of lower density, low volatility, high partition coefficient and low melting and freezing points. The extraction efficiency of DLLME-SFOD is affected by types and volumes of organic extractant and disperser, salt addition, pH, temperature, stirring rate and extraction time. This review discusses the principle, optimization variables, advantages and disadvantages and some selected applications of DLLME-SFOD in water, food and biomedical analysis.

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The only requirements of a dispersive solvent are to be miscible with both the aqueous sample and the extracting solvent and to efficiently disperse the extracting solvent in water to enhance extraction efficiency.
“The only requirements of a dispersive solvent is to be miscible with both aqueous sample and extracting solvent such as methanol, ethanol, acetone and acetonitrile [22] and efficiently disperse the extracting solvent in water to enhance the extraction efficiency of analytes.”
From Deep eutectic solvent as a novel disperser in dispersive liquid-liquid microextraction based on solidification of floating organic droplet (DLLME-SFOD) for preconcentration of steroids in water samples: Assessment of the method deleterious impact on the environment using Analytical Eco-Scale and Green Analytical Procedure Index (2019) · cites this paper as [22]
DLLME-SFO had not been automated before this work.
“A large number of analytical methods based on manual DLLME-SFO have been reported, but its automation has not yet been reported [23,24].”
From Automated dispersive liquid-liquid microextraction based on the solidification of the organic phase (2018) · cites this paper as [24]
A large number of analytical methods based on manual DLLME-SFO have been reported.
“A large number of analytical methods based on manual DLLME-SFO have been reported, but its automation has not yet been reported [23,24].”
From Automated dispersive liquid-liquid microextraction based on the solidification of the organic phase (2018) · cites this paper as [24]
Despite its undeniable advantages, DLLME-SFOD has significant drawbacks, including the need for at least two organic solvents, the difficulty of automation, and the slowing of the process caused by the freezing step [13,22].
“Despite its undeniable advantages, DLLME-SFOD has significant drawbacks, including the need for at least two organic solvents, the difficulty of automation, and the slowing of the process caused by the freezing step [13,22].”
From Deep Eutectic Solvents as Promising Green Solvents in Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Droplet: Recent Applications, Challenges and Future Perspectives (2021) · cites this paper as [22]

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Asadollahi, T., Dadfarnia, S., Shabani, A. M. H., & Amirkavei, M. (2013) · Journal of Food Science and Technology · doi:10.1007/s13197-013-1077-9 · Cited by 35 · see citing works
Indirect spectrophotometric determination of ultra trace amounts of selenium based on dispersive liquid-liquid microextraction-solidified floating organic drop.
Shabani, A. M. H., Dadfarnia, S., & Nozohor, M. (2013) · Spectrochimica Acta Part A - Molecular and Biomolecular Spectroscopy · doi:10.1016/j.saa.2013.07.004 · Cited by 34 · see citing works
Ultrasound enhanced air-assisted surfactant liquid–liquid microextraction based on the solidification of an organic droplet for the determination of chromium in water, air and biological samples
Ezoddin, M., Abdi, K., & Esmaeili, N. (2016) · Microchemical Journal · doi:10.1016/j.microc.2016.07.005 · Cited by 34 · see citing works
Liquid Chromatographic Determination of NSAIDs in Urine After Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Droplets
Shukri, D. S. M., Sanagi, M. M., Ibrahim, W. A. W., Abidin, N. N. Z., & Aboul-Enein, H. Y. (2015) · Chromatographia · doi:10.1007/s10337-015-2920-0 · Cited by 33 · see citing works
Supramolecular dispersive liquid–liquid microextraction based solidification of floating organic drops for speciation and spectrophotometric determination of chromium in real samples
Abadi, M. D. M., Chamsaz, M., Arbab-Zavar, M. H., & Shemirani, F. (2013) · Analytical Methods · doi:10.1039/c3ay00036b · Cited by 33 · see citing works
Development of Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Drop for the Determination of Trace Nickel
Wang, Y., Zhang, J., Zhao, B., et al. (2011) · Biological Trace Element Research · doi:10.1007/s12011-011-9078-x · Cited by 33 · see citing works
Ligandless-solidified floating organic drop microextraction method for the preconcentration of trace amount of cadmium in water samples
Arpa, Ç., & Durukan, İ. (2011) · Talanta · doi:10.1016/j.talanta.2011.04.044 · Cited by 33 · see citing works
Dispersive liquid-liquid microextraction based on solidification of floating organic drop and high-performance liquid chromatography to the analysis of cocaine’s major adulterants in human urine
Sena, L. C. S., Matos, H. R., Dórea, H. S., Pimentel, M. F., de Santana, D. C. A. S., & de Santana, F. J. M. (2016) · Toxicology · doi:10.1016/j.tox.2016.04.008 · Cited by 32 · see citing works
Preconcentration of organochlorine pesticides in aqueous samples by dispersive liquid–liquid microextraction based on solidification of floating organic drop after SPE with multiwalled carbon nanotubes
Mirzaei, M., & Rakh, M. (2013) · Journal of Separation Science · doi:10.1002/jssc.201301058 · Cited by 30 · see citing works
Room Temperature Ionic Liquid-Based Dispersive Liquid Phase Microextraction for the Separation/Preconcentration of Trace Cd2+ as 1-(2-pyridylazo)-2-naphthol (PAN) Complex from Environmental and Biological Samples and Determined by FAAS
Khan, S., Soylak, M., & Kazi, T. G. (2013) · Biological Trace Element Research · doi:10.1007/s12011-013-9853-y · Cited by 30 · see citing works
Improved dispersive liquid–liquid microextraction based on the solidification of floating organic droplet method with a binary mixed solvent applied for determination of nicotine and cotinine in urine
Wang, X., Wang, Y., Zou, X., & Cao, Y. (2014) · Analytical Methods · doi:10.1039/c3ay42308e · Cited by 29 · see citing works
Preconcentration of valsartan by dispersive liquid–liquid microextraction based on solidification of floating organic drop and its determination in urine sample: Central composite design
Pebdani, A. A., Shabani, A. M. H., Dadfarnia, S., Talebianpoor, M. S., & Khodadoust, S. (2016) · Journal of Separation Science · doi:10.1002/jssc.201600010 · Cited by 29 · see citing works
Determination of the rare earth elements La, Eu, and Yb using solidified floating organic drop microextraction and electrothermal vaporization ICP-MS
Chen, S., Cheng, X., He, Y., Zhu, S., & Lu, D. (2013) · Microchimica Acta · doi:10.1007/s00604-013-1091-7 · Cited by 28 · see citing works
Dispersive liquid–liquid microextraction based on solidification of floating organic droplet for the determination of triazine and triazoles in mineral water samples
Bolzan, C. M., Caldas, S. S., Guimarães, B. D. S., & Prímel, E. G. (2016) · Journal of Separation Science · doi:10.1002/jssc.201600405 · Cited by 28 · see citing works
Ultrasonic-assisted supramolecular solvent-based liquid phase microextraction of mercury as 1-(2-pyridylazo)-2-naphthol complexes from water samples
Aydin, F. A., Yılmaz, E., & Soylak, M. (2016) · International Journal of Environmental & Analytical Chemistry · doi:10.1080/03067319.2016.1253690 · Cited by 28 · see citing works
Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Droplet Followed by Spectrofluorimetry for Determination of Carvedilol in Human Plasma
Zamani-Kalajahi, M., Fazeli-Bakhtiyari, R., Amiri, M., et al. (2013) · Bioanalysis · doi:10.4155/bio.12.326 · Cited by 27 · see citing works
Dispersive solid‐phase extraction followed by vortex‐assisted dispersive liquid–liquid microextraction based on the solidification of a floating organic droplet for the determination of benzoylurea insecticides in soil and sewage sludge
Peng, G., He, Q., Mmereki, D., Lu, Y., Zhong, Z., Liu, H., Pan, W., Zhou, G., & Chen, J. (2016) · Journal of Separation Science · doi:10.1002/jssc.201501347 · Cited by 27 · see citing works
Ultrasound-assisted emulsification solidified floating organic drop microextraction for the determination of trace amounts of copper in water samples
Chang, Q., Zhang, J., Du, X., et al. (2010) · 中国环境科学与工程前沿：英文版 · doi:10.1007/s11783-010-0030-7 · Cited by 26 · see citing works
Dispersive liquid-liquid microextraction based on solidification of floating organic drop for simultaneous separation/preconcentration of nickel, cobalt and copper prior to determination by electrothermal atomic absorption spectrometry
Amirkavei, M., Dadfarnia, S., & Shabani, A. M. H. (2013) · Química Nova · doi:10.1590/s0100-40422013000100012 · Cited by 26 · see citing works
Fiber optic-linear array detection spectrophotometry in combination with dispersive liquid-liquid microextraction for preconcentration and determination of copper
Ezoddin, M., Shemirani, F., & Jamali, M. R. (2010) · Journal of Analytical Chemistry · doi:10.1134/s1061934810020097 · Cited by 25 · see citing works
2-Nitroso-1-naphthol as a selective reagent for preconcentration of cobalt by vortex assisted combined with solidification of organic droplet and its determination by flame atomic absorption spectrometry
Chamsaz, M., Eftekhari, M., Eftekhari, A., et al. (2013) · Environmental Monitoring and Assessment · doi:10.1007/s10661-013-3236-x · Cited by 24 · see citing works
Vortex-assisted surfactant-enhanced emulsification microextraction based on solidification of floating organic drop followed by electrothermal atomic absorption spectrometry for speciation of antimony (ΙΙΙ, V)
Eftekhari, M., Chamsaz, M., Arbab-Zavar, M. H., et al. (2014) · Environmental Monitoring and Assessment · doi:10.1007/s10661-014-4129-3 · Cited by 24 · see citing works
Derivatization and Solidification of Floating Dispersive Liquid‐phase Microextraction for the Analysis of Kanamycin in Wastewater and Soil by HPLC with Fluorescence Detection
Hu, S., Song, Y., Bai, X., Jiang, X., & Yang, X. (2013) · CLEAN - Soil Air Water · doi:10.1002/clen.201200374 · Cited by 24 · see citing works
Determination of four acidic nonsteroidal anti‐inflammatory drugs in wastewater samples by dispersive liquid–liquid microextraction based on solidification of floating organic droplet and high‐performance liquid chromatography
Beldean‐Galea, M. S., Coman, V., Thiébaut, D., et al. (2014) · Journal of Separation Science · doi:10.1002/jssc.201400933 · Cited by 23 · see citing works
Optimization of dispersive liquid–liquid microextraction based on the solidification of floating organic droplets using an orthogonal array design and its application for the determination of fungicide concentrations in environmental water samples
Yang, X., Yang, M., Hou, B., et al. (2014) · Journal of Separation Science · doi:10.1002/jssc.201400075 · Cited by 23 · see citing works
Speciation and determination of iron using dispersive liquid–liquid microextraction based on solidification of organic drop followed by flame atomic absorption spectrometry
Chamsaz, M., Eftekhari, M., Tafreshi, S., et al. (2013) · International Journal of Environmental & Analytical Chemistry · doi:10.1080/03067319.2013.840831 · Cited by 23 · see citing works
Determination of fungicides in sediments using a dispersive liquid–liquid microextraction procedure based on solidification of floating organic drop
Dong, S., Huang, G., Lu, J., & Huang, T. (2014) · Journal of Separation Science · doi:10.1002/jssc.201400010 · Cited by 23 · see citing works
Solid-Phase Extraction Followed by Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Drop for the Determination of Parabens
Hashemi, B., Shamsipur, M., & Fattahi, N. (2015) · Journal of Chromatographic Science · doi:10.1093/chromsci/bmv011 · Cited by 23 · see citing works
Ultrasound-assisted emulsification/microextraction based on solidification of trace amounts of thallium prior to graphite furnace atomic absorption spectrometry determination
Afzali, D., Bahadori, B., & Fathirad, F. (2013) · Toxicological & Environmental Chemistry Reviews · doi:10.1080/02772248.2013.856912 · Cited by 22 · see citing works
Speciation of Tl(III) and Tl(I) in hair samples by dispersive liquid–liquid microextraction based on solidification of floating organic droplet prior to flame atomic absorption spectrometry determination
Mohammadi, S. Z., Sheibani, A., Abdollahi, F., & Shahsavani, E. (2012) · Arabian Journal of Chemistry · doi:10.1016/j.arabjc.2012.03.008 · Cited by 22 · see citing works
Dispersive liquid–liquid microextraction based on solidification of floating organic drop combined with field‐amplified sample injection in capillary electrophoresis for the determination of beta(2)‐agonists in bovine urine
Us, M. F., Alshana, U., Lubbad, I., et al. (2013) · Electrophoresis · doi:10.1002/elps.201200348 · Cited by 22 · see citing works
Simultaneous spectrophotometric determination of Fe(III) and Al(III) using orthogonal signal correction–partial least squares calibration method after solidified floating organic drop microextraction
Moghadam, M. R., Shabani, A. M. H., & Dadfarnia, S. (2014) · Spectrochimica Acta Part A Molecular and Biomolecular Spectroscopy · doi:10.1016/j.saa.2014.08.007 · Cited by 22 · see citing works
Ion-pair dispersive liquid–liquid microextraction solidification of floating organic droplets method for the rapid and sensitive detection of phenolic acids in wine samples using liquid chromatography combined with a core–shell particle column
Li, J., Jia, S., Yoon, S. J., et al. (2015) · Journal of Food Composition and Analysis · doi:10.1016/j.jfca.2015.09.016 · Cited by 22 · see citing works
Development and application of chemometric‐assisted dispersive liquid–liquid microextraction for the determination of suspected fragrance allergens in water samples
Tsiallou, T. P., Sakkas, V. A., & Albanis, T. A. (2012) · Journal of Separation Science · doi:10.1002/jssc.201200106 · Cited by 21 · see citing works
Displacement-Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Drop of Trace Amounts of Palladium in Water and Road Dust Samples Prior to Graphite Furnace Atomic Absorption Spectrometry Determination
Ghanbarian, M., Afzali, D., Mostafavi, A., et al. (2013) · Journal of AOAC International · doi:10.5740/jaoacint.11-495 · Cited by 20 · see citing works
DISPERSIVE LIQUID-LIQUID MICROEXTRACTION BASED ON SOLIDIFICATION OF FLOATING ORGANIC DROP COMBINED WITH COUNTER-ELECTROOSMOTIC FLOW NORMAL STACKING MODE IN CAPILLARY ELECTROPHORESIS FOR THE DETERMINATION OF BISPHENOL A IN WATER AND URINE SAMPLES
Alshana, U., Lubbad, I., Göğer, N. G., Çok, İ., Tamer, U., & Ertaş, N. (2013) · Journal of Liquid Chromatography & Related Technologies · doi:10.1080/10826076.2012.725700 · Cited by 19 · see citing works
Vortex-Assisted Solidified Floating Organic Drop Microextraction of Molybdenum in Beverages and Food Samples Coupled with Graphite Furnace Atomic Absorption Spectrometry
Tüzen, M., Shemsi, A. M., & Bukhari, A. A. (2016) · Food Analytical Methods · doi:10.1007/s12161-016-0571-x · Cited by 18 · see citing works
Dispersive Liquid–Liquid Microextraction of Propranolol Enantiomers from Human Plasma Based on The Solidification of A Floating Organic Droplet
Farhadi, K., Hatami, M., Forough, M., et al. (2013) · Bioanalysis · doi:10.4155/bio.13.23 · Cited by 17 · see citing works
DISPLACEMENT-DISPERSIVE LIQUID-LIQUID MICROEXTRACTION BASED ON SOLIDIFICATION FLOATING ORGANIC DROP TRACE AMOUNTS OF LEAD IN WATER SAMPLE PRIOR TO FLAME ATOMIC ABSORPTION SPECTROMETRY DETERMINATION
Afzali, D., Fayazi, M., & FAVI, A. (2013) · Journal of the Chilean Chemical Society · doi:10.4067/s0717-97072013000100020 · Cited by 17 · see citing works
Dispersive Liquid-Liquid Microextraction-Solidified Floating Organic Drop Combined with Spectrophotometry for the Speciation and Determination of Ultratrace Amounts of Selenium
Dadfarnia, S., Shabani, A. M. H., & Nozohor, M. (2013) · Journal of the Brazilian Chemical Society · doi:10.5935/0103-5053.20130287 · Cited by 16 · see citing works
A dispersive liquid-liquid microextraction method based on the solidification of a floating organic drop combined with HPLC for the determination of lovastatin and simvastatin in rat urine.
Zhao, L.-S., Zhao, P., Wang, L.-L., Ma, X.-W., Hou, X., & Li, F. (2014) · Biomedical chromotography · doi:10.1002/bmc.3205 · Cited by 16 · see citing works
Dispersive Liquid-Liquid Microextraction Based on Solidification of Floating Organic Drop with Central Composite Design for the Determination of Nitrophenols Using High-Performance Liquid Chromatography
Hashemi, B., Shamsipur, M., & Barati, A. (2015) · Journal of the Brazilian Chemical Society · doi:10.5935/0103-5053.20150185 · Cited by 16 · see citing works
Development of a dispersive liquid-liquid microextraction method based on solidification of a floating organic drop for the determination of beta-carotene in human serum
Rahimi, A., & Hashemi, P. (2014) · Journal of Analytical Chemistry · doi:10.1134/s1061934814040078 · Cited by 15 · see citing works
Development of ultrasound‐assisted emulsification microextraction based on solidification of a floating organic droplet for determination of organochlorine pesticides in water samples
Shu, B., Yang, Z., Lee, H., Qiu, B., & Li, H. (2016) · Journal of Separation Science · doi:10.1002/jssc.201501002 · Cited by 15 · see citing works
Analysis of Sudan I in Food by QuEChERS Combined with Ultrasound-assisted Dispersive Liquid-liquid Microextraction with Solidification of Floating Organic Drop (UADLLME-SFO) Prior to HPLC-PAD
He, X., Chen, Y., Li, H., et al. (2015) · Food Science and Technology Research · doi:10.3136/fstr.21.659 · Cited by 15 · see citing works
Determination of boron in water samples by dispersive liquid–liquid microextraction based on the solidification of a floating organic drop coupled with a fluorimetric method
Peng, G., He, Q., Li, H., et al. (2016) · The Analyst · doi:10.1039/c6an00008h · Cited by 14 · see citing works
Application of Solvent Demulsification-Dispersive Liquid-Liquid Microextraction Based on Solidification of Floating Organic Drop Coupled with High Perfomence Liquid Chromatography in Determination of Sulfonylurea Herbicides in Water and Soil
Li, Y., Jing, Z., Lin, R., et al. (2016) · Journal of the Brazilian Chemical Society · doi:10.5935/0103-5053.20160060 · Cited by 14 · see citing works
A Novel Dispersive Liquid-Liquid Microextraction Method Based on Solidification of Floating Organic Drop for Preconcentration of Pd(II) by Graphite Furnace Atomic Absorption Spectrometry after Complexation by a Thienyl Substituted 1,2-Ethanediamine
Ragheb, E., Hashemi, P., Alizadeh, K., & Ganjali, M. R. (2015) · Analytical Sciences · doi:10.2116/analsci.31.119 · Cited by 13 · see citing works
A Simple and Rapid Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Drop Method Combined with Flame Atomic Absorption Spectrometry for Preconcentration and Determination of Copper
Mirzaei, M., & Behzadi, M. (2013) · Journal of AOAC International · doi:10.5740/jaoacint.11-105 · Cited by 13 · see citing works
Directly suspended-solidified floating organic droplets for the determination of fungicides in water and honey samples
Li, S., Yang, X., Hu, L., Cui, X., Zhang, S., Lu, R., Zhou, W., & Gao, H. (2014) · Analytical Methods · doi:10.1039/c4ay00806e · Cited by 12 · see citing works
Dispersive liquid–liquid microextraction based on solidification of floating organic drop for separation and preconcentration of malachite green before its determination by flow injection spectrophotometry
Dadfarnia, S., Shabani, A. M. H., Esfahani, G. S., & Kazemi, E. (2016) · Spectroscopy Letters · doi:10.1080/00387010.2015.1104359 · Cited by 12 · see citing works
A NOVEL METHOD FOR THE DETERMINATION OF TRACE THORIUM BY DISPERSIVE LIQUID-LIQUID MICROEXTRACTION BASED ON SOLIDIFICATION OF FLOATING ORGANIC DROP
Rezaee, M. B., & Khalilian, F. (2016) · Química Nova · doi:10.5935/0100-4042.20160012 · Cited by 12 · see citing works
Solidification of floating organic drop microextraction combined with gas chromatography-flame photometric detection for the analysis of organophosphorus pesticides in water samples
Liu, Y., He, M., Chen, B., & Hu, B. (2015) · Analytical Methods · doi:10.1039/c5ay01181g · Cited by 11 · see citing works
Dispersive Liquid-Liquid Microextraction Based on Solidification of Floating Organic Drop Combined with Flame Atomic Absorption Spectrometry for Preconcentration and Determination of Thallium(III) in Water Samples
Chamsaz, M., Mohadese, H. P. Z., Hossein, A.-Z. M., et al. (2014) · DOAJ (DOAJ: Directory of Open Access Journals) · doi:10.30492/ijcce.2014.7196 · Cited by 11 · see citing works
Determination of Trace Levels of Lead in Water Samples by Graphite Furnace Atomic Absorption Spectrometry After Dispersive Liquid-liquid Microextraction Based on Solidification of Floating Organic Drop
Liang, P. (2014) · Atomic Spectroscopy · doi:10.46770/as.2014.02.005 · Cited by 11 · see citing works
Dispersive Liquid–Liquid Extraction Based on Freezing of the Organic Drop, Followed by GC for the Determination of Methyl Methacrylate in Wastewater
Mokhtari, B., Dalali, N., & Pourabdollah, K. (2013) · Chromatographia · doi:10.1007/s10337-013-2403-0 · Cited by 10 · see citing works
Supramolecular based-ligandless ultrasonic assisted-dispersion solidification liquid–liquid microextraction of uranyl ion prior to spectrophotometric determination with dibenzoylmethane
Shokrollahi, A., & Pili, H. B. (2016) · RSC Advances · doi:10.1039/c5ra23355k · Cited by 10 · see citing works
Application of Chemometrics Methods for the Simultaneous Determination of Zinc and Copper after Preconcentration and Separation by Liquid– Liquid Microextraction Based on Solidification of Floating Organic Drop Coupled to Flow Injection Spectrophotometry
Asadollahi, T., Shabani, A. M. H., Dadfarnia, S., et al. (2012) · Current Analytical Chemistry · doi:10.2174/157341112801264905 · Cited by 10 · see citing works
Solidified Floating Organic Drop Microextraction for the Determination of Trace Dy and Y by Electrothermal Vaporization Inductively Coupled Plasma Mass Spectrometry
Chen, S. (2014) · Atomic Spectroscopy · doi:10.46770/as.2014.01.001 · Cited by 10 · see citing works
Application of dispersive liquid-liquid microextraction based on solidification of floating organic droplet to the analysis of antidepressant drugs in water samples
Sanagi, M. M., Mokhtar, S. U., Ibrahim, W. A. W., et al. (2013) · Sains Malaysiana · Cited by 8 · see citing works
Floating Organic Drop Microextraction Combined with Electrothermal Atomic Absorption Spectrometry for Trace Determination of Cobalt in Oil Refining Wastewaters
Shamsipur, M., Ramezani, M., & Beigi, A. A. M. (2015) · Energy Sources Part A Recovery Utilization and Environmental Effects · doi:10.1080/15567036.2011.592916 · Cited by 6 · see citing works
Simultaneous Determination of Hydrochlorothiazide and Enalapril Maleate in Pharmaceutical Formulations Using Fourier Transform Infrared Spectrometry
Hamid, A. S., Amirzadeh, H., & Reza, S. M. (2016) · Cited by 5 · see citing works
Vortex-assisted surfactant-enhanced-emulsification liquid–liquid microextraction with solidification of floating organic droplet combined with flame atomic absorption spectrometry for the fast determination of cadmium in water samples
Peng, G., Lu, Y. C., He, Q., et al. (2016) · Water Science & Technology · doi:10.2166/wst.2016.063 · Cited by 5 · see citing works
Sensitive analysis In(III) in various matrices by spectrophotometry after dispersive liquid-liquid microextraction based on solidification of floating organic drop
Shadmehri, E. A., Abadi, M. D. M., & Chamsaz, M. (2014) · Russian Journal of Applied Chemistry · doi:10.1134/s1070427214060044 · Cited by 4 · see citing works
Dispersive Liquid-Liquid Microextraction Based on Solidification of Floating Organic Drop Combined with Flame Atomic Absorption Spectrometry for Preconcentration and Determination of Thallium(III) in Water Samples
Chamsaz, & Mahmoud (2014) · Cited by 4 · see citing works
Optimization of Dispersive Liquid-Liquid Microextraction Based on Solidification of Floating Organic Drop of Endocrine Disrupting Compounds in Liquid Food Samples Using Response Surface Plot Method
Li, Y., & Zhang, C. (2014) · Asian Journal of Chemistry · doi:10.14233/ajchem.2014.16259 · Cited by 3 · see citing works
Mixed Extractant-Dispersive Liquid Phase Microextraction Based on Solidification of Floating Organic Drop for Determination of S-phenylmercapturic Acid in Urine
Xiao, Z. (2013) · CHINESE JOURNAL OF ANALYTICAL CHEMISTRY (CHINESE VERSION) · Cited by 2 · see citing works
Mixed Extractant-Dispersive Liquid Phase Microextraction Based on Solidification of Floating Organic Drop for Determination of S -phenylmercapturic Acid in Urine
Wang, Y., Zou, X., Zhang, W., et al. (2013) · CHINESE JOURNAL OF ANALYTICAL CHEMISTRY (CHINESE VERSION) · doi:10.3724/sp.j.1096.2013.20940 · Cited by 2 · see citing works

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A new tool for the evaluation of the analytical procedure: Green Analytical Procedure Index
Płotka-Wasylka, J. (2018) · Talanta · doi:10.1016/j.talanta.2018.01.013 · Cited by 2,328 · see citing works
Liquid–phase microextraction: A review of reviews
Rutkowska, M., Płotka-Wasylka, J., Sajid, M., & Andruch, V. (2019) · Microchemical Journal · doi:10.1016/j.microc.2019.103989 · Cited by 244 · see citing works
Selecting an extraction solvent for a greener liquid phase microextraction (LPME) mode-based analytical method
Kokosa, J. M. (2019) · TrAC Trends in Analytical Chemistry · doi:10.1016/j.trac.2019.05.012 · Cited by 145 · see citing works
In matrix formation of deep eutectic solvent used in liquid phase extraction coupled with solidification of organic droplets dispersive liquid-liquid microextraction; Application in determination of some pesticides in milk samples
Jouyban, A., Farajzadeh, M. A., & Afshar Mogaddam, M. R. (2020) · Talanta · doi:10.1016/j.talanta.2019.120169 · Cited by 122 · see citing works
Deep eutectic solvent as a novel disperser in dispersive liquid-liquid microextraction based on solidification of floating organic droplet (DLLME-SFOD) for preconcentration of steroids in water samples: Assessment of the method deleterious impact on the environment using Analytical Eco-Scale and Green Analytical Procedure Index
El-Deen, A. K., & Shimizu, K. (2019) · Microchemical Journal · doi:10.1016/j.microc.2019.103988 · Cited by 92 · see citing works
Hydrophobic Deep Eutectic Solvents in Developing Microextraction Methods Based on Solidification of Floating Drop: Application to the Trace HPLC/FLD Determination of PAHs
Yousefi, S. M., Shemirani, F., & Ghorbanian, S. A. (2018) · Chromatographia · doi:10.1007/s10337-018-3548-7 · Cited by 87 · see citing works
Emulsification microextraction of amphetamine and methamphetamine in complex matrices using an up-to-date generation of eco-friendly and relatively hydrophobic deep eutectic solvent
Rajabi, M., Ghassab, N., Hemmati, M., & Asghari, A. (2018) · Journal of Chromatography A · doi:10.1016/j.chroma.2018.07.040 · Cited by 76 · see citing works
Solvent-terminated dispersive liquid-liquid microextraction: a tutorial
Mansour, F. R., & Danielson, N. D. (2018) · Analytica Chimica Acta · doi:10.1016/j.aca.2018.02.005 · Cited by 64 · see citing works
Self-citation
Deep Eutectic Solvents as Promising Green Solvents in Dispersive Liquid–Liquid Microextraction Based on Solidification of Floating Organic Droplet: Recent Applications, Challenges and Future Perspectives
El-Deen, A. K., & Shimizu, K. (2021) · Molecules · doi:10.3390/molecules26237406 · Cited by 58 · see citing works
“Despite its undeniable advantages, DLLME-SFOD has significant drawbacks, including the need for at least two organic solvents, the difficulty of automation, and the slowing of the process caused by the freezing step [13,22].”
Background
Automated dispersive liquid-liquid microextraction based on the solidification of the organic phase
Medina, D. A. V., Santos-Neto, Á. J., Cerdà, V., & Maya, F. (2018) · Talanta · doi:10.1016/j.talanta.2018.06.081 · Cited by 55 · see citing works
Liquid-phase microextraction: update May 2016 to December 2018
Campillo, N., Gavazov, K., Viñas, P., Hagarova, I., & Andruch, V. (2020) · Applied Spectroscopy Reviews · doi:10.1080/05704928.2019.1604537 · Cited by 45 · see citing works
Evaporation-assisted dispersive liquid–liquid microextraction based on the solidification of floating organic droplets for the determination of triazole fungicides in water samples by high-performance liquid chromatography
Jing, X., Yang, L., Zhao, W., Wang, F., Chen, Z., Ma, L., Jia, L., & Wang, X. (2019) · Journal of Chromatography A · doi:10.1016/j.chroma.2019.03.040 · Cited by 44 · see citing works
Liquid phase microextraction techniques combined with chromatography analysis: a review
Dugheri, S., Mucci, N., Bonari, A., Marrubini, G., Cappelli, G., Ubiali, D., Campagna, M., Montalti, M., & Arcangeli, G. (2020) · Acta Chromatographica · doi:10.1556/1326.2019.00636 · Cited by 41 · see citing works
Method for the determination of carboxylic acids in industrial effluents using dispersive liquid-liquid microextraction with injection port derivatization gas chromatography–mass spectrometry
Makoś, P., Fernandes, A., & Boczkaj, G. (2017) · Journal of Chromatography A · doi:10.1016/j.chroma.2017.08.045 · Cited by 31 · see citing works
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Authors: Mansour, F. R., & Danielson, N. D.
Affiliations: Tanta University (EG)
Miami University (US)
Corresponding author: Mansour, Fotouh R.
ORCID: Mansour, Fotouh R.
Danielson, Neil D.
Venue: Talanta
Publisher: Elsevier BV
Published: 2017-08
Volume: 170
Pages: 22-35
ISSN: 0039-9140 (ISSN-L)
DOI: 10.1016/j.talanta.2017.03.084
OpenAlex: W2603218211
Cited by: 178
References: 143
Citations by year: 2026: 8 · 2025: 16 · 2024: 27 · 2023: 13 · 2022: 19 · 2021: 27 · 2020: 20 · 2019: 23 · 2018: 20 · 2017: 5
FWCI: 2.16
Type: journal article
Language: en
Open access: closed
Licence: www.elsevier.com/tdm/userlicense/1.0/ (tdm)
Locations: Talanta (publishedVersion)
PubMed (publishedVersion)
Topics: Physical Sciences › Chemistry › Analytical Chemistry › Analytical chemistry methods development
Physical Sciences › Chemistry › Spectroscopy › Analytical Chemistry and Chromatography
Physical Sciences › Engineering › Biomedical Engineering › Innovative Microfluidic and Catalytic Techniques Innovation
Keywords: dispersive liquid-liquid microextraction, solidification of floating organic droplet, green analytical chemistry, undecanol, extraction efficiency optimization, water analysis, food analysis, biomedical analysis

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Solidification of floating organic droplet in dispersive liquid-liquid microextraction as a green analytical tool

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