The DOI matches its Crossref record; 21 of the 21 references it cites were found in a registry or an index.
A Method for Estimating the Nature and Relative Proportions of Amorphous, Single, and Double-Helical Components in Starch Granules by13C CP/MAS NMR
Abstract
An improved method to analyze the (13)C NMR spectra of native starches, which considers the contribution of the V-type conformation and the nature of the amorphous component, has been developed. Starch spectra are separated into amorphous and ordered subspectra, using intensity at 84 ppm as a reference point. The ordered subspectra of high amylose starches show the presence of both V-type single helices and B-type double helices. Relative proportions of amorphous, single, and double-helical conformations are estimated by apportioning intensity of C1 peak areas between conformational types on the basis of ordered and amorphous subspectra of the native starch. Quantitative analysis shows that the V-type single-helical component increases with amylose content of starches. Different amorphous subspectra are needed to provide a consistent analysis of granular starches from diverse sources. The method of preparation was found to be more important than the starch botanical origin in determining (13)C NMR spectral features of amorphous samples.
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Cites
Official Methods of Analysis: 22nd Edition (2023)
(2023) · Official Methods of Analysis of AOAC INTERNATIONAL · doi:10.1093/9780197610145.002.001 · Cited by 28,007
Morrison, W. R., & Laignelet, B. (1983) · Journal of Cereal Science · doi:10.1016/s0733-5210(83)80004-6 · Cited by 756
The double-helical nature of the crystalline part of A-starch
Imberty, A., Chanzy, H., Pérez, S., Bulèon, A., & Tran, V. (1988) · Journal of Molecular Biology · doi:10.1016/0022-2836(88)90144-1 · Cited by 634
A revisit to the three‐dimensional structure of B‐type starch
Imberty, A., & Perez, S. (1988) · Biopolymers · doi:10.1002/bip.360270803 · Cited by 574
Recent Advances in Knowledge of Starch Structure
Imberty, A., Buléon, A., Tran, V., & Péerez, S. (1991) · Starch - Stärke · doi:10.1002/star.19910431002 · Cited by 550
A Universal Feature in the Structure of Starch Granules from Different Botanical Sources
Jenkins, P. J., Cameron, R. E., & Donald, A. M. (1993) · Starch - Stärke · doi:10.1002/star.19930451202 · Cited by 408
Gidley, M. J., & Bociek, S. M. (1988) · Journal of the American Chemical Society · doi:10.1021/ja00220a016 · Cited by 397
Self-citationMolecular organization in starches: a carbon 13 CP/MAS NMR study
Gidley, M. J., & Bociek, S. M. (1985) · Journal of the American Chemical Society · doi:10.1021/ja00310a047 · Cited by 393
Self-citationBarley sex6 mutants lack starch synthase IIa activity and contain a starch with novel properties
Morell, M. K., Kosar‐Hashemi, B., Cmiel, M., Samuel, M. S., Chandler, P., Rahman, S., Buleon, A., Batey, I. L., & Li, Z. (2003) · The Plant Journal · doi:10.1046/j.1365-313x.2003.01712.x · Cited by 331
Murthy, N. S., & Minor, H. (1990) · Polymer · doi:10.1016/0032-3861(90)90243-r · Cited by 328
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Warren, F. J., Gidley, M. J., & Flanagan, B. M. (2016) · Carbohydrate Polymers · doi:10.1016/j.carbpol.2015.11.066 · Cited by 931
Self-citationLopez‐Rubio, A., Flanagan, B. M., Gilbert, E. P., & Gidley, M. J. (2008) · Biopolymers · doi:10.1002/bip.21005 · Cited by 719
Self-citationRelationship between granule size and in vitro digestibility of maize and potato starches
Dhital, S., Shrestha, A. K., & Gidley, M. J. (2010) · Carbohydrate Polymers · doi:10.1016/j.carbpol.2010.05.018 · Cited by 379
Self-citationXie, F., Halley, P. J., & Avérous, L. (2012) · Progress in Polymer Science · doi:10.1016/j.progpolymsci.2011.07.002 · Cited by 301
Self-citationZhang, B., Chen, L., Li, X., Li, L., & Zhang, H. (2015) · Food Hydrocolloids · doi:10.1016/j.foodhyd.2015.05.002 · Cited by 253
Htoon, A., Shrestha, A. K., Flanagan, B. M., Lopez-Rubio, A., Bird, A. R., Gilbert, E. P., & Gidley, M. J. (2009) · Carbohydrate Polymers · doi:10.1016/j.carbpol.2008.06.016 · Cited by 232
Self-citationEffect of cryo-milling on starches: Functionality and digestibility
Dhital, S., Shrestha, A. K., & Gidley, M. J. (2010) · Food Hydrocolloids · doi:10.1016/j.foodhyd.2009.08.013 · Cited by 144
Self-citationUltrasound-assisted hydration offers a novel approach to anneal in-situ pinto bean starch
Kumar, G., Hooper, J. F., Li, E., Devkota, L., & Dhital, S. (2025) · Carbohydrate Polymers · doi:10.1016/j.carbpol.2025.123602 · Cited by 11
Metadata
- Authors
- Tan, I., Flanagan, B. M., Halley, P. J., Whittaker, A. K., & Gidley, M. J.
- Venue
- Biomacromolecules
- Publisher
- American Chemical Society (ACS)
- Published
- 2007-02-01
- Volume
- 8
- Issue
- 3
- Pages
- 885-891
- ISSN
- 1525-7797 (ISSN-L)
- 1526-4602
- OpenAlex
- W2016527357
- Cited by
- 480
- References
- 21
- FWCI
- 5.11
- Type
- journal article
- Language
- en
- Open access
- closed
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