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Synthesis, Structure, and Electrochemical Properties of the Layered Sodium Insertion Cathode Material: NaNi1/3Mn1/3Co1/3O2
Abstract
A layered phase, NaNi 1 / 3 Mn 1 / 3 Co 1 / 3 O 2 (NaNMC), isostructural to NaCoO 2 has been synthesized. Stoichiometric NaNMC crystallizes in a rhombohedral R3̅m space group where Na is in an octahedral environment (O3-Type). Galvanostatic cycling on NaNMC vs Na cell indicated a reversible intercalation of 0.5 Na, leading to a capacity of 120 mAh·g –1 in the voltage range of 2–3.75 V and indicating its possible application in Na-ion batteries. The electrochemically driven Na insertion/deinsertion in NaNMC is associated with several phase transitions and solid solution regimes which are studied by in situ X-ray diffraction. Sodium deinsertion in Na x NMC resulted in sequential phase transitions composed of biphasic and monophasic domains. The composition driven structural evolution in Na x NMC follows the sequence O3 ⇒ O1 ⇒ P3 ⇒ P1 phases with an increased ‘ c ’ parameter, while the ‘ a ’ parameter remains almost unchanged.
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Metadata
- Authors
- Sathiya, M., Hemalatha, K., Ramesha, K., Tarascon, J.-M., & Prakash, A. S.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2012-04-30
- Volume
- 24
- Issue
- 10
- Pages
- 1846-1853
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W127421390
- Cited by
- 564
- References
- 15
- FWCI
- 30.73
- Type
- journal article
- Language
- en
- Open access
- closed
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