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Characterization of Polydopamine Thin Films Deposited at Short Times by Autoxidation of Dopamine
Abstract
Current interest in melanin films derived from the autoxidation of dopamine stems from their use as a universal adhesion layer. Here we report chemical and physical characterization of polydopamine films deposited on gold surfaces from stirred basic solutions at times ranging from 2 to 60 min, with a focus on times ≤10 min. Data from Fourier transform infrared (FTIR), X-ray photoelectron spectroscopy (XPS), and electrochemical methods suggest the presence of starting (dopamine) and intermediate (C=N-containing tautomers of quinone and indole) species in the polydopamine films at all deposition times. A uniform overlayer analysis of the XPS data indicates that film thickness increased linearly at short deposition times of ≤10 min. At deposition times ≥10 min, the films appeared largely continuous with surface roughness ≈ ≤ 2 nm, as determined by atomic force microscopy (AFM). Pinhole-free films, as determined by anionic redox probe measurements, required deposition times of 60 min or greater.
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Metadata
- Authors
- Zangmeister, R. A., Morris, T. A., & Tarlov, M. J.
- Venue
- Langmuir
- Publisher
- American Chemical Society (ACS)
- Published
- 2013-06-27
- Volume
- 29
- Issue
- 27
- Pages
- 8619-8628
- ISSN
- 0743-7463 (ISSN-L)
- 1520-5827
- OpenAlex
- W1995646011
- Cited by
- 983
- References
- 45
- FWCI
- 17.62
- Type
- journal article
- Language
- en
- Open access
- closed
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