Three-dimensional Nitrogen-Doped Graphene Supported Molybdenum Disulfide Nanoparticles as an Advanced Catalyst for Hydrogen Evolution Reaction

Dong, Haifeng; Liu, Conghui; Ye, Haitao; Hu, Linping; Fugetsu, Bunshi; Dai, Wenhao; Cao, Yu; Qi, Xueqiang; Lu, Huiting; Zhang, Xueji

doi:10.1038/srep17542

Cited by 188Electrocatalysts for Energy ConversionFuel Cells and Related MaterialsAdvanced Photocatalysis Techniques

Three-dimensional Nitrogen-Doped Graphene Supported Molybdenum Disulfide Nanoparticles as an Advanced Catalyst for Hydrogen Evolution Reaction

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Dong, Haifeng, Liu, Conghui, Ye, Haitao, Hu, Linping, Fugetsu, Bunshi, Dai, Wenhao, Cao, Yu, Qi, Xueqiang +2 more·2015·Scientific Reports

DOI 10.1038/srep17542PMC PMC4670999

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Abstract

An efficient three-dimensional (3D) hybrid material of nitrogen-doped graphene sheets (N-RGO) supporting molybdenum disulfide (MoS 2) nanoparticles with high-performance electrocatalytic activity for hydrogen evolution reaction (HER) is fabricated by using a facile hydrothermal route. Comprehensive microscopic and spectroscopic characterizations confirm the resulting hybrid material possesses a 3D crumpled few-layered graphene network structure decorated with MoS 2 nanoparticles. Electrochemical characterization analysis reveals that the resulting hybrid material exhibits efficient electrocatalytic activity toward HER under acidic conditions with a low onset potential of 112 mV and a small Tafel slope of 44 mV per decade. The enhanced mechanism of electrocatalytic activity has been investigated in detail by controlling the elemental composition, electrical conductance and surface morphology of the 3D hybrid as well as Density Functional Theory (DFT) calculations. This demonstrates that the abundance of exposed active sulfur edge sites in the MoS 2 and nitrogen active functional moieties in N-RGO are synergistically responsible for the catalytic activity, whilst the distinguished and coherent interface in MoS2/N-RGO facilitates the electron transfer during electrocatalysis. Our study gives insights into the physical/chemical mechanism of enhanced HER performance in MoS 2/N-RGO hybrids and illustrates how to design and construct a 3D hybrid to maximize the catalytic efficiency.

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Zhang et al. reported an effective electrocatalytic activity for HER when graphene oxide is doped with nitrogen, resulting in a low overpotential of 112 mV.
“Zhang et al. reported an effective electrocatalytic activity for HER when graphene oxide (GO) is doped with nitrogen, resulting in a low overpotential of 112 mV.18”
From Three-Dimensional Printed MoS2/Graphene Aerogel Electrodes for Hydrogen Evolution Reactions (2022) · cites this paper as [18]
The Results (Electrochemical activity and durability) report a 112 mV HER onset potential for a MoS₂/N-RGO hybrid, not for nitrogen-doped graphene oxide alone. The Discussion says N-RGO without MoS₂ showed little HER activity compared with the hybrid. The claim captures the reported value but omits the MoS₂ nanoparticles essential to the tested catalyst. (LLM, conf=0.89)
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Highly enhanced hydrogen sensing properties of sericin-induced exfoliated MoS2 nanosheets at room temperature
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Photocatalytic H2 Evolution from Oxalic Acid: Effect of Cocatalysts and Carbon Dioxide Radical Anion on the Surface Charge Transfer Mechanisms
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Controllable Insertion Mechanism of Expanded Graphite Anodes Employing Conversion Reaction Pillars for Sodium-Ion Batteries
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MoS 2 ‐TiO 2 Nanocomposite with Excellent Adsorption Performance and High Antibacterial Activity
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Porous Nitrogen-Doped Crumpled Graphene Nanoparticles: A Metal-Free Nanozyme for Selective Detection of Dopamine in Aqueous Medium and Human Serum
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Three-Dimensional Printed MoS2/Graphene Aerogel Electrodes for Hydrogen Evolution Reactions
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Active Basal Plane Catalytic Activity via Interfacial Engineering for a Finely Tunable Conducting Polymer/MoS2 Hydrogen Evolution Reaction Multilayer Structure
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Synthesis and tribological properties of WS2/MoS2 micro-nano composite lubricant
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Simultaneously Engineering Electron Conductivity, Site Density and Intrinsic Activity of MoS 2 via the Cation and Anion Codoping Strategy
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Graphite oxide and molybdenum disulfide composite for hydrogen evolution reaction
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Synthesis of CoAl-LDH nanosheets and N-doped graphene nanocomposite via Successive Ionic Layer Deposition method and study of their electrocatalytic properties for hydrogen evolution in alkaline media
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Construction of Hierarchical SnO2@NC@MoS2/C Nanotubes for Ultrastable Lithium- and Sodium-Ion Batteries
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A multifunctional nanostructured molybdenum disulphide (MoS 2 ): an overview on synthesis, structural features, and potential applications
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Improved resistive switching performance in Cu-cation migrated MoS2 based ReRAM device incorporated with tungsten nitride bottom electrode
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Relevant photovoltaic effect in N-doped CQDs/MoS2 (0D/2D) quantum dimensional heterostructure
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Boron Doped Graphene Quantum Structure and MoS2 Nanohybrid as Anode Materials for Highly Reversible Lithium Storage
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P-doped 3D graphene network supporting uniformly vertical MoS2 nanosheets for enhanced hydrogen evolution reaction
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Oxygen doped MoS2 quantum dots for efficient electrocatalytic hydrogen generation
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Evaluation of N doped rGO-ZnO-CoPc(COOH)8 nanocomposite in cyanide degradation and its bactericidal activities
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Tailoring of 1T Phase-Domain MoS2 Active Sites with Bridging S22–/Apical S2– Phase-Selective Precursor Modulation for Enriched HER Kinetics
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Symmetric Supercapacitors with layer-by-layer Molybdenum disulfide - reduced graphene oxide structures and poly(3,4-ethylenedioxythiophene) nanoparticles nanohybrid electrode
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Transition metal (Ni, co)‐doped graphitic carbon nitride/ MoS2 heterojunctions as efficient photocatalysts for hydrogen evolution reaction under visible light
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Authors: Dong, H., Liu, C., Ye, H., Hu, L., Fugetsu, B., Dai, W., Cao, Y., Qi, X., Lu, H., & Zhang, X.
Affiliations: University of Science and Technology Beijing (CN)
Aston University (GB)
Chongqing University (CN)
The University of Tokyo (JP)
Corresponding author: Dong, Haifeng
Zhang, Xueji
ORCID: Dong, Haifeng
Liu, Conghui
Ye, Haitao
Hu, Linping
Fugetsu, Bunshi
Dai, Wenhao
Cao, Yu
Qi, Xueqiang
Lu, Huiting
Zhang, Xueji
Venue: Scientific Reports
Publisher: Springer Science and Business Media LLC
Published: 2015-12-07
Volume: 5
Issue: 1
Pages: 17542-17542
ISSN: 2045-2322 (ISSN-L)
DOI: 10.1038/srep17542
PMC: PMC4670999
OpenAlex: W2240019802
Cited by: 188
References: 63
Citations by year: 2026: 7 · 2025: 13 · 2024: 7 · 2023: 13 · 2022: 17 · 2021: 19 · 2020: 30 · 2019: 29 · 2018: 26 · 2017: 19 · 2016: 8
FWCI: 5.22
Type: journal article
Language: en
Open access: gold
doi.org
Licence: cc-by
creativecommons.org/licenses/by/4.0 (tdm)
creativecommons.org/licenses/by/4.0 (vor)
Locations: Scientific Reports (publishedVersion, cc-by)
Europe PMC (PubMed Central) (publishedVersion, cc-by)
PubMed Central (publishedVersion, cc-by)
PubMed (publishedVersion)
Aston Publications Explorer (Aston University) (acceptedVersion)
Figshare (submittedVersion, cc-by)
Leicester Research Archive (University of Leicester) (submittedVersion, cc-by)
Funders: National Natural Science Foundation of China (21275017, 21305008, 21127007, 21475008, 11175039)
Ministry of Education of the People's Republic of China (06199045, 11170197)
University of Science and Technology Beijing
Fundamental Research Funds for the Central Universities (06199045)
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Engineering › Electrical and Electronic Engineering › Fuel Cells and Related Materials
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Advanced Photocatalysis Techniques
Keywords: hydrogen evolution reaction, molybdenum disulfide nanoparticles, nitrogen-doped graphene, reduced graphene oxide, electrocatalysis, acidic electrocatalysis, nitrogen active sites, electron transfer, hydrothermal synthesis, DFT calculations

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Three-dimensional Nitrogen-Doped Graphene Supported Molybdenum Disulfide Nanoparticles as an Advanced Catalyst for Hydrogen Evolution Reaction

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