Versatile, Stable, and Scalable Gel‐Like Aerophobic Surface System (GLASS) for Hydrogen Production
Open accessAbstract
Facile removal of adsorbed gas bubbles from electrode surfaces is crucial to realize efficient and stable energy conversion devices based on electrochemical gas evolution reactions. Conventional studies on bubble removal have limited applicability and scalability due to their reliance on complex and energy/time‐intensive processes. In this study, a simple and versatile method is reported to fabricate large‐area superaerophobic electrodes (up to 100 cm 2 ) for diverse gas evolution reactions using the gel‐like aerophobic surface system (GLASS). GLASS electrodes are readily and uniformly fabricated by simple spin‐coating and cross‐linking of polyallylamine on virtually any kinds of electrodes within 5 min under ambient conditions. Intrinsically hydrophilic gel overlayers with interconnected open pores allow the physical separation of bubble adhesion and catalytic active sites, reducing bubble adhesion strength, and promoting the removal of gas bubbles. As a result, GLASS electrodes exhibit greatly enhanced efficiency and stability for diverse gas evolution reactions, such as hydrogen evolution, hydrazine oxidation, and oxygen evolution reactions. This study provides deeper insights into understanding the effect of the hydrophilic microenvironment on gas evolution reactions and designing practical electrochemical devices.
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Coating polyallylamine hydrochloride hydrogel onto Pt-coated Ni foil makes aerophobicity significantly better than pristine electrode due to hydrophilicity and open pore structure, with bubble adhesion force only 6.87 μN and bubble contact angle 154.61°; during HER the gel-coated electrode exhibits excellent catalytic activity and stability, with average detached bubble diameter only ~50 μm.
“Furthermore, Kang from the same team as Jeon [183] coated polyallylamine hydrochloride (PAH) and gelled it onto the Pt-coated Ni foil (Fig. 16c). The hydrophilicity of PAH hydrogel itself, coupled with the open pore structure on the surface, makes the aerophobicity of the electrode coated with PAH hydrogel significantly better than that of the pristine electrode. The bubble adhesion force is only”
From Advances in Surface/Interface Engineering of Under-Water Superaerophobic Electrodes for Hydrogen Evolution Reaction by Manipulating of Bubbles (2026) · cites this paper as [183]
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- Authors
- Kang, Y., Lee, S., Han, S., Jeon, D., Bae, M., Choi, Y., Lee, D. W., & Ryu, J.
- Affiliations
- Ulsan National Institute of Science and Technology (KR)
- Korea Institute of Geoscience and Mineral Resources (KR)
- Corresponding author
- Ryu, Jungki
- Venue
- Advanced Functional Materials
- Publisher
- Wiley
- Published
- 2023-09-29
- Volume
- 34
- Issue
- 2
- ISSN
- 1616-301X (ISSN-L)
- 1616-3028
- OpenAlex
- W4387220675
- Cited by
- 45
- References
- 54
- Citations by year
- 2026: 16 · 2025: 17 · 2024: 11 · 2023: 1
- FWCI
- 2.15
- Type
- journal article
- Language
- en
- Open access
- Locations
- Advanced Functional Materials (publishedVersion)
- Scholarworks@UNIST (Ulsan National Institute of Science and Technology) (submittedVersion)
- Funders
- National Research Foundation of Korea
- Topics
- Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
- Physical Sciences › Materials Science › Surfaces, Coatings and Films › Surface Modification and Superhydrophobicity
- Physical Sciences › Environmental Science › Water Science and Technology › Minerals Flotation and Separation Techniques
- Keywords
- superaerophobic surfaces, bubble removal, bubble adhesion, polyallylamine, gas evolution reactions, hydrogen evolution reaction, hydrazine oxidation, oxygen evolution reaction, electrocatalyst stability, spin coating, crosslinking
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