High-Performance Electrocatalysis Using Metallic Cobalt Pyrite (CoS2) Micro- and Nanostructures

Faber, Matthew S.; Dziedzic, Rafal; Lukowski, Mark A.; Kaiser, Nicholas S.; Ding, Qi; Jin, Song

doi:10.1021/ja504099w

Cited by 1,372Electrocatalysts for Energy ConversionCO2 Reduction Techniques and CatalystsAdvanced Photocatalysis Techniques

High-Performance Electrocatalysis Using Metallic Cobalt Pyrite (CoS2) Micro- and Nanostructures

Faber, Matthew S., Dziedzic, Rafal, Lukowski, Mark A., Kaiser, Nicholas S., Ding, Qi, Jin, Song·2014·Journal of the American Chemical Society

DOI 10.1021/ja504099w

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Abstract

The development of efficient and robust earth-abundant electrocatalysts for the hydrogen evolution reaction (HER) is an ongoing challenge. We report metallic cobalt pyrite (cobalt disulfide, CoS2) as one such high-activity candidate material and demonstrate that its specific morphology--film, microwire, or nanowire, made available through controlled synthesis--plays a crucial role in determining its overall catalytic efficacy. The increase in effective electrode surface area that accompanies CoS2 micro- and nanostructuring substantially boosts its HER catalytic performance, with CoS2 nanowire electrodes achieving geometric current densities of -10 mA cm(-2) at overpotentials as low as -145 mV vs the reversible hydrogen electrode. Moreover, micro- and nanostructuring of the CoS2 material has the synergistic effect of increasing its operational stability, cyclability, and maximum achievable rate of hydrogen generation by promoting the release of evolved gas bubbles from the electrode surface. The benefits of catalyst micro- and nanostructuring are further demonstrated by the increased electrocatalytic activity of CoS2 nanowire electrodes over planar film electrodes toward polysulfide and triiodide reduction, which suggests a straightforward way to improve the performance of quantum dot- and dye-sensitized solar cells, respectively. Extension of this micro- and nanostructuring strategy to other earth-abundant materials could similarly enable inexpensive electrocatalysts that lac…

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The overpotential at −10 mA cm−2 for (Ni,Co)Se2-GA is much lower than that for Ni3Se2 nanoforest on Ni foam in 1 M NaOH (203 mV) and CoS2 in 0.5 M H2SO4 (145 mV).
“For example, the overpotential at −10 mA cm−2 is much lower than that for Ni3Se2 nanoforest on Ni foam in 1 M NaOH (203 mV)53 and CoS2 in 0.5 M H2SO4 (145 mV).48”
From Prussian Blue Analogues Derived Penroseite (Ni,Co)Se 2 Nanocages Anchored on 3D Graphene Aerogel for Efficient Water Splitting (2017) · cites this paper as [48]
Based on recent reports on porous HER catalysts, the highly porous morphology of Au aerogel could significantly contribute to HER activity.
“Based on recent reports88,89,90 on porous HER catalysts, the highly porous morphology of Au aerogel could significantly contribute to HER activity”
From Gold aerogel supported on graphitic carbon nitride: an efficient electrocatalyst for oxygen reduction reaction and hydrogen evolution reaction (2015) · cites this paper as [90]

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Authors: Faber, M. S., Dziedzic, R., Lukowski, M. A., Kaiser, N. S., Ding, Q., & Jin, S.
Affiliations: University of Wisconsin–Madison (US)
Corresponding author: Jin, Song
ORCID: Dziedzic, Rafal
Ding, Qi
Jin, Song
Venue: Journal of the American Chemical Society
Publisher: American Chemical Society (ACS)
Published: 2014-06-17
Volume: 136
Issue: 28
Pages: 10053-10061
ISSN: 0002-7863 (ISSN-L)
1520-5126
DOI: 10.1021/ja504099w
OpenAlex: W2331768105
Cited by: 1,372
References: 48
Citations by year: 2026: 34 · 2025: 69 · 2024: 89 · 2023: 82 · 2022: 83 · 2021: 118 · 2020: 128 · 2019: 165 · 2018: 160 · 2017: 197 · 2016: 131 · 2015: 95 · 2014: 19
FWCI: 48.63
Type: journal article
Language: en
Open access: closed
Locations: Journal of the American Chemical Society (publishedVersion)
PubMed (publishedVersion)
Funders: U.S. Department of Energy (DE-FG02-09ER46664)
Topics: Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Electrocatalysts for Energy Conversion
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › CO2 Reduction Techniques and Catalysts
Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Advanced Photocatalysis Techniques
Keywords: cobalt disulfide, CoS2, hydrogen evolution reaction, electrocatalysis, nanowire electrodes, microwire electrodes, nanostructuring, earth-abundant catalysts, polysulfide reduction, triiodide reduction, quantum dot solar cells, dye-sensitized solar cells, catalyst stability, gas bubble release

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High-Performance Electrocatalysis Using Metallic Cobalt Pyrite (CoS2) Micro- and Nanostructures

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