Stereocomplex formation between poly(L‐lactic acid) and poly(D‐lactic acid) with disproportionately low and high molecular weights from the melt
Abstract
Poly( L ‐lactic acid) (PLLA) and poly( D ‐lactic acid) (PDLA) with very different weight‐average molecular weights ( M w ) of 4.0 × 10 3 and 7.0 × 10 5 g mol −1 ( M w (PDLA)/ M w (PLLA) = 175) were blended at different PDLA weight ratios ( X D = PDLA weight/blend weight) and their crystallization from the melt was investigated. The presence of low molecular weight PLLA facilitated the stereocomplexation and thereby lowered the cold crystallization temperature ( T cc ) for non‐isothermal crystallization during heating and elevated the radial growth rate of spherulites ( G ) for isothermal crystallization, irrespective of X D . The orientation of lamellae in the spherulites was higher for the neat PLLA, PDLA and an equimolar blend than for the non‐equimolar blends. It was found that the orientation of lamellae in the blends was maintained by the stereocomplex (SC) crystallites. Although the G values are expected to decrease with an increase in X D or the content of high‐molecular‐weight PDLA with lower chain mobility compared with that of low‐molecular‐weight PLLA, G was highest at X D = 0.5 where the maximum amount of SC crystallites was formed and the G values were very similar for X D = 0.4 and X D = 0.6 with the same enantiomeric excess. This means that the effect of SC crystallites overwhelmed that of chain mobility. The nucleating mechanisms of SC crystallites were identical for X D = 0.1–0.5 in the T c range 130–180 °C. Copyright © 2011 Society of Chemical Industry
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In solution casting processes many parameters can affect crystallization, e.g. the concentration of the polymer in the solution or the evaporation rate of the solvent.
“In solution casting processes many parameters can affect crystallization e.g. the concentration of the polymer in the solution or the evaporation rate of the solvent.76”
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- Authors
- Tsuji, H., & Bouapao, L.
- Affiliations
- Toyohashi University of Technology (JP)
- Corresponding author
- Tsuji, Hideto
- ORCID
- Tsuji, Hideto
- Venue
- Polymer International
- Publisher
- Wiley
- Published
- 2011-12-16
- Volume
- 61
- Issue
- 3
- Pages
- 442-450
- ISSN
- 0959-8103 (ISSN-L)
- 1097-0126
- OpenAlex
- W1970375389
- Cited by
- 59
- References
- 48
- Citations by year
- 2025: 3 · 2024: 4 · 2023: 6 · 2022: 3 · 2021: 5 · 2020: 9 · 2019: 1 · 2018: 6 · 2017: 2 · 2016: 8 · 2015: 5 · 2014: 2 · 2013: 3 · 2012: 2
- FWCI
- 1.91
- Type
- journal article
- Language
- en
- Open access
- closed
- Locations
- Polymer International (publishedVersion)
- Topics
- Physical Sciences › Materials Science › Polymers and Plastics › Polymer crystallization and properties
- Physical Sciences › Materials Science › Biomaterials › biodegradable polymer synthesis and properties
- Physical Sciences › Materials Science › Materials Chemistry › Block Copolymer Self-Assembly
- Keywords
- stereocomplex formation, poly(L-lactic acid), poly(D-lactide), polymer blends, molecular weight effects, cold crystallization, spherulite growth rate, lamellar orientation, nucleation mechanism, chain mobility, enantiomeric excess
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
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