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Topochemical Synthesis of Sodium Metal Phosphate Olivines for Sodium-Ion Batteries
Abstract
New metastable olivine phases of sodium metal phosphates, Na[Mn 1– x M x ]PO 4 (M = Fe, Ca, Mg), nanorods are synthesized by a simple solid-state reaction at low temperature (≤100 °C) by means of a topotactic molten salt reaction that converts NH 4 [Mn 1– x M x ]PO 4 •H 2 O (M = Fe, Ca, Mg) to Na[Mn 1– x M x ]PO 4 . Their crystal structures are characterized via XRD Rietveld refinement and electron diffraction. A full range of solid solution behavior was observed for olivine Na 1– x Mn 0.5 Fe 0.5 PO 4, in contrast to that of LiMPO 4 (M = Fe, Mn) olivine materials, and is ascribed to ion size effects. The solid solution behavior of NaMn 0.5 Fe 0.5 PO 4 was confirmed by electrochemical characterization.
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Cites
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Metadata
- Authors
- Lee, K. T., Ramesh, T. N., Nan, F., Botton, G., & Nazar, L. F.
- Venue
- Chemistry of Materials
- Publisher
- American Chemical Society (ACS)
- Published
- 2011-07-20
- Volume
- 23
- Issue
- 16
- Pages
- 3593-3600
- ISSN
- 0897-4756 (ISSN-L)
- 1520-5002
- OpenAlex
- W2332110027
- Cited by
- 309
- References
- 9
- FWCI
- 16.93
- Type
- journal article
- Language
- en
- Open access
- closed
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