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Cobalt–Manganese‐Based Spinels as Multifunctional Materials that Unify Catalytic Water Oxidation and Oxygen Reduction Reactions
Abstract
Recently, there has been much interest in the design and development of affordable and highly efficient oxygen evolution reaction (OER) and oxygen reduction reaction (ORR) catalysts that can resolve the pivotal issues that concern solar fuels, fuel cells, and rechargeable metal‐air batteries. Here we present the synthesis and application of porous CoMn 2 O 4 and MnCo 2 O 4 spinel microspheres as highly efficient multifunctional catalysts that unify the electrochemical OER with oxidant‐driven and photocatalytic water oxidation as well as the ORR. The porous materials were prepared by the thermal degradation of the respective carbonate precursors at 400 °C. The as‐prepared spinels display excellent performances in electrochemical OER for the cubic MnCo 2 O 4 phase in comparison to the tetragonal CoMn 2 O 4 material in an alkaline medium. Moreover, the oxidant‐driven and photocatalytic water oxidations were performed and they exhibited a similar trend in activity to that of the electrochemical OER. Remarkably, the situation is reversed in ORR catalysis, that is, the oxygen reduction activity and stability of the tetragonal CoMn 2 O 4 catalyst outperformed that of cubic MnCo 2 O 4 and rivals that of benchmark Pt catalysts. The superior catalytic performance and the remarkable stability of the unifying materials are attributed to their unique porous and robust microspherical morphology and the intrinsic structural features of the spinels. Moreover, the facile access to these high‐performance materials enables a reliable and cost‐effective production on a large scale for industrial applications.
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Metadata
- Authors
- Menezes, P. W., Indra, A., Sahraie, N. R., Bergmann, A., Strasser, P., & Driess, M.
- Venue
- ChemSusChem
- Publisher
- Wiley
- Published
- 2014-11-13
- Volume
- 8
- Issue
- 1
- Pages
- 164-171
- ISSN
- 1864-5631 (ISSN-L)
- 1864-564X
- OpenAlex
- W1964083672
- Cited by
- 267
- References
- 105
- FWCI
- 10.26
- Type
- journal article
- Language
- en
- Open access
- closed
About these checks
Registry, retraction, Cites and statistics results are computed, not judged, with one exception: a printed reference that no index lists is read once by a model before it counts as a citation error. Claims are extracted by a model and kept only when their quote appears verbatim in the text; each cited source is then checked, with a model’s help, for whether it says what the claim relies on. Those verdicts can be wrong — read the claim’s quote and the cited source before relying on one.
Statistics and arithmetic are recomputed, not judged.
Confidence bands are shown only for fields calibrated on our annotated test set. None is calibrated yet, so no band is shown.
What counts as a claim ›How we measure confidence ›How we check this ›
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Data sources
Bibliographic data: Semantic Scholar, OpenAlex, Crossref.
Contains information from the Semantic Scholar Academic Graph Datasets, made available under the ODC Attribution License (ODC-BY 1.0).
Semantic Scholar’s data is described in: Kinney, R., et al. (2023). The Semantic Scholar Open Data Platform. arXiv:2301.10140.
