Extraction, characterization, purification and catalytic upgrading of algae lipids to fuel-like hydrocarbons
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GCMS analysis of the recovered materials indicated a high content of fatty acids, hydrocarbons and phytol isomers, while UV-vis spectroscopic and ICP analyses revealed complete chlorophyll, phosphorus and magnesium removal.
“Gas chromatography-mass spectrometry (GCMS) analysis of the recovered materials indicated a high content of fatty acids, hydrocarbons and phytol isomers, while ultraviolet-visible (UV-vis) spectroscopic and inductively coupled plasma (ICP) analyses revealed complete chlorophyll, phosphorus and magnesium removal.”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
The relative abundance of hydrocarbons in the activated carbon-bleached material was lower than in the K10-bleached material, likely due to the greater hydrophobicity of the activated carbon retaining more of the hydrocarbons.
“Notably, the relative abundance of hydrocarbons in the activated carbon-bleached material was lower than in the K10-bleached material, likely due to the greater hydrophobicity of the activated carbon retaining more of the hydrocarbons.”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
Crocker and co-workers explored deoxygenation of algae oils from Scenedesmus acutus grown on power plant flue gas as a carbon source using nickel-based catalysts.
“Crocker and co-workers explored deoxygenation of algae oils from Scenedesmus acutus grown on power plant flue gas as a carbon source using nickel-based catalysts (71, 89-91).”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
The Ni-Al layered double hydroxide catalyst showed significantly less deactivation at 300°C.
“In particular, the Ni-Al layered double hydroxide catalyst showed significantly less deactivation at 300°C.”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
The lipids used by Crocker and co-workers were purified by column chromatography using either K10 montmorillonite clay or activated carbon with silica gel.
“the lipids were purified by column chromatography using either K10 montmorillonite clay or activated carbon with silica gel, which was effective at removing chlorophyll and other pigments, magnesium and phosphorus.”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
Residual extraction solvent, namely chloroform, was likely the source of chloride detected on the catalyst in post-reaction analysis.
“Santillan-Jimenez et al . (71) also noted that the residual extraction solvent (namely chloroform) was likely the source of chloride detected on the catalyst in post-reaction analysis (71), underscoring the observation that the extraction protocol can impact downstream processes through routes other than influencing the types of lipids extracted.”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
The cleanup procedures were effective at removing chlorophyll and other pigments, magnesium and phosphorus.
“the lipids were purified by column chromatography using either K10 montmorillonite clay or activated carbon with silica gel, which was effective at removing chlorophyll and other pigments, magnesium and phosphorus.”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
A more detailed analysis of impurities suggested that the oil cleanup quantitatively removed phosphorus and magnesium, though a small amount of nitrogen remained.
“A more detailed analysis of impurities also suggested that the oil cleanup quantitatively removed phosphorus and magnesium, though a small amount of nitrogen remained (71).”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
K10 montmorillonite appeared to be a more effective adsorbent than activated carbon, resulting in a greater fraction of products in the diesel range.
“K10 montmorillonite appeared to be a more effective adsorbent than activated carbon, resulting in a greater fraction of products in the diesel range.”
From Catalytic Hydroprocessing of Single-Cell Oils to Hydrocarbon Fuels: Converting microbial lipids to fuels is a promising approach to replace fossil fuels (2021) · cites this paper as [71]
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Umenweke, G. C., & Santillan‐Jimenez, E. (2024) · ACS in focus · doi:10.1021/acsinfocus.7e8011 · Cited by 4 · see citing works
Self-citationSato, C., Alikaram, G., Kolajo, O. O., Dudgeon, J., Hazard, R., Apollon, W., & Kamaraj, S. (2025) · Membranes · doi:10.3390/membranes15100295 · Cited by 3 · see citing works
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Research Highlights – September
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Montero, G. E. R., Zgolicz, P. D., Ballarini, A., Guerra, J. F., & Bocanegra, S. (2026) · Elsevier eBooks · doi:10.1016/b978-0-443-34088-8.00124-5
- Authors
- Santillan-Jimenez, E., Pace, R., Marques, S., Morgan, T., McKelphin, C., Mobley, J., & Crocker, M.
- Affiliations
- University of Kentucky (US)
- Corresponding author
- Crocker, Mark
- Venue
- Fuel
- Publisher
- Elsevier BV
- Published
- 2016-09
- Volume
- 180
- Pages
- 668-678
- ISSN
- 0016-2361 (ISSN-L)
- OpenAlex
- W2343764736
- Cited by
- 58
- References
- 54
- Citations by year
- 2026: 3 · 2025: 7 · 2024: 5 · 2023: 3 · 2022: 4 · 2021: 3 · 2020: 8 · 2019: 8 · 2018: 6 · 2017: 7 · 2016: 4
- FWCI
- 7.41
- Type
- journal article
- Language
- en
- Open access
- bronze
- doi.org
- Licence
- Locations
- Fuel (acceptedVersion)
- Funders
- University of Kentucky Center for Applied Energy Research
- National Science Foundation (1531637)
- Duke Energy
- Topics
- Physical Sciences › Engineering › Mechanical Engineering › Catalysis and Hydrodesulfurization Studies
- Physical Sciences › Energy › Renewable Energy, Sustainability and the Environment › Algal biology and biofuel production
- Physical Sciences › Engineering › Biomedical Engineering › Biodiesel Production and Applications
- Keywords
- algal lipids, Scenedesmus acutus, lipid extraction, lipid purification, adsorption, activated carbon, montmorillonite, in situ transesterification, deoxygenation, NiAl layered double hydroxide, catalyst deactivation, unsaturated lipids, coke formation, biofuel upgrading
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