Green ultrasound-assisted extraction of carotenoids based on the bio-refinery concept using sunflower oil as an alternative solvent
Abstract
A green, inexpensive and easy-to-use method for carotenoids extraction from fresh carrots assisted by ultrasound was designed in this work. Sunflower oil was applied as a substitute to organic solvents in this green ultrasound-assisted extraction (UAE): a process which is in line with green extraction and bio-refinery concepts. The processing procedure of this original UAE was first compared with conventional solvent extraction (CSE) using hexane as solvent. Moreover, the UAE optimal conditions for the subsequent comparison were optimized using response surface methodology (RSM) and ultra performance liquid chromatography--diode array detector--mass spectroscopy (UPLC-DAD-MS). The results showed that the UAE using sunflower as solvent has obtained its highest β-carotene yield (334.75 mg/l) in 20 min only, while CSE using hexane as solvent obtained a similar yield (321.35 mg/l) in 60 min. The green UAE performed under optimal extraction conditions (carrot to oil ratio of 2:10, ultrasonic intensity of 22.5 W cm(-2), temperature of 40 °C and sonication time of 20 min) gave the best yield of β-carotene.
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Li et al. [115] found that the highest yield of β-carotene (334.75 mg/L) using sunflower as solvent was achieved by UAEE within 20 min, while hexane extraction obtained a similar yield (321.35 mg/L) but required 60 min.
“According to the findings, the highest yield of β-carotene (334.75 mg/L) using sunflower as a solvent was achieved by the UAEE within a short duration of 20 min. In contrast, the extraction using hexane as the solvent obtained a similar yield (321.35 mg/L) but required a longer extraction time of 60 min.”
From A comprehensive review of ultrasonic assisted extraction (UAE) for bioactive components: Principles, advantages, equipment, and combined technologies (2023) · cites this paper as [115]
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- Authors
- Li, Y., Fabiano-Tixier, A. S., Tomao, V., Cravotto, G., & Chemat, F.
- Affiliations
- Université d'Avignon et des Pays de Vaucluse (FR)
- University of Turin (IT)
- Corresponding author
- Chemat, Farid
- Venue
- Ultrasonics Sonochemistry
- Publisher
- Elsevier BV
- Published
- 2013-01
- Volume
- 20
- Issue
- 1
- Pages
- 12-18
- ISSN
- 1350-4177 (ISSN-L)
- OpenAlex
- W2010406025
- Cited by
- 259
- References
- 21
- Citations by year
- 2026: 17 · 2025: 13 · 2024: 20 · 2023: 22 · 2022: 26 · 2021: 18 · 2020: 22 · 2019: 23 · 2018: 15 · 2017: 37 · 2016: 17 · 2015: 12 · 2014: 13 · 2013: 4
- FWCI
- 14.23
- Type
- journal article
- Language
- en
- Open access
- closed
- Licence
- Locations
- Ultrasonics Sonochemistry (publishedVersion)
- PubMed (publishedVersion)
- HAL (submittedVersion)
- Topics
- Life Sciences › Agricultural and Biological Sciences › Food Science › Agricultural and Biological Research
- Health Sciences › Medicine › Biochemistry › Phytochemicals and Antioxidant Activities
- Physical Sciences › Materials Science › Materials Chemistry › Ultrasound and Cavitation Phenomena
- Keywords
- ultrasound-assisted extraction, carotenoids, beta-carotene, carrot, sunflower oil, green extraction, biorefinery, extraction optimization, response surface methodology
- MeSH terms
- Sunflower Oil, Carotenoids, Chemical Fractionation, Hexanes, Plant Oils, Solvents, Time Factors, Ultrasonics, Green Chemistry Technology
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