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Monodisperse MFe2O4 (M = Fe, Co, Mn) Nanoparticles

Sun, Shouheng, Zeng, Hao, Robinson, David B., Raoux, Simone, Rice, Philip M., Wang, Shan X., Li, Guanxiong·2004·Journal of the American Chemical Society

DOI 10.1021/ja0380852

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Abstract

High-temperature solution phase reaction of iron(III) acetylacetonate, Fe(acac)(3), with 1,2-hexadecanediol in the presence of oleic acid and oleylamine leads to monodisperse magnetite (Fe(3)O(4)) nanoparticles. Similarly, reaction of Fe(acac)(3) and Co(acac)(2) or Mn(acac)(2) with the same diol results in monodisperse CoFe(2)O(4) or MnFe(2)O(4) nanoparticles. Particle diameter can be tuned from 3 to 20 nm by varying reaction conditions or by seed-mediated growth. The as-synthesized iron oxide nanoparticles have a cubic spinel structure as characterized by HRTEM, SAED, and XRD. Further, Fe(3)O(4) can be oxidized to Fe(2)O(3), as evidenced by XRD, NEXAFS spectroscopy, and SQUID magnetometry. The hydrophobic nanoparticles can be transformed into hydrophilic ones by adding bipolar surfactants, and aqueous nanoparticle dispersion is readily made. These iron oxide nanoparticles and their dispersions in various media have great potential in magnetic nanodevice and biomagnetic applications.

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Authors: Sun, S., Zeng, H., Robinson, D. B., Raoux, S., Rice, P. M., Wang, S. X., & Li, G.
Venue: Journal of the American Chemical Society
Publisher: American Chemical Society (ACS)
Published: 2003-12-10
Volume: 126
Issue: 1
Pages: 273-279
ISSN: 0002-7863 (ISSN-L)
1520-5126
DOI: 10.1021/ja0380852
OpenAlex: W2039985275
Cited by: 3,441
References: 37
FWCI: 35.60
Type: journal article
Language: en
Open access: closed

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Monodisperse MFe2O4 (M = Fe, Co, Mn) Nanoparticles

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